共查询到19条相似文献,搜索用时 78 毫秒
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单点滴定法和双点滴定法是近年来发展起来的两种具有推广前景的分析方法。本文介绍这两种方法的基本内容、发展状况及影响准确度的因素,并将它们与电位滴定法、标准加入法及线性滴定法进行了比较 相似文献
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导出了沉淀单点滴定法与双点滴定法计算式。以银电极为指示电极 ,Ag 标准溶液为滴定剂 ,对Cl-、Br-、I-及SCN-等离子的测定进行了研究 ;对影响测定结果准确度的因素进行了讨论。实验发现 ,在α =1 .0~ 1 .1的条件下 ,单点滴定法有较高的准确度 ;在α1 ≈ 1 .0~ 1 .1、ΔV =0 .5~ 1 .0mL的条件下 ,双点滴定法有较高的准确度 相似文献
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本文提出以离子选择性电极为指示电极的库仑双点滴定的实验方法,推导出定量公式和相对误差公式,探讨了影响准确度的主要因素。 相似文献
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酸碱电位双点滴定法在药物分析中的应用 总被引:1,自引:0,他引:1
探讨酸碱电位双点滴定法在药物分析中的应用。提出测定药片中的盐酸麻黄碱和烟酸的实验方法及其实验参数。该法简便快速。对2种样品的测定结果令人满意。 相似文献
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High-performance thin-layer chromatography has been used for separation and quantification of nitroguanidine and guanidine
nitrate, for online and off-line quality control of synthesis. The compounds were separated on silica gel 60 F254 layers with dioxane–tetrahydrofuran 1:1 (v/v), as mobile phase. UV detection was performed at 210 and 265 nm for guanidine nitrate and nitroguanidine, respectively. Quantitative
analysis was performed by absorbance densitometry and use of peak area. Validation was performed taking into consideration
the special features of the method. 相似文献
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土壤硝态氮反映土壤短期氮素供应水平,实时了解土壤硝态氮的含量为精准农业和农业面源污染防控提供支撑,因此,在线实时检测土壤硝态氮方法突破就显得十分迫切。土壤硝态氮中的硝酸根离子在土壤中的高水溶性和流动性为全固态硝酸根离子选择电极高敏感检测土壤中硝态氮提供了条件,固态硝态氮离子选择电极的离子选择膜反应硝酸根离子在被测溶液中的浓度。采用全固态硝酸根离子选择电极ELIT NO3-,且与温度电极和pH电极融合组成电极阵列对土壤饱和溶液中的硝酸根离子进行检测。设计了高输入阻抗运算放大电路对电极信号进行采集,并通过微处理控制蠕动泵完成土壤硝态氮待测溶液连续流动测定及实时传输结果。实验结果表明,电极响应时间≤15 s,斜率-51.63 mV/decade,线性范围10-5~10-2.2 mol/L,最低检测限10-5.23 mol/L。相对标准差在0.78%~4.5%,加标回收率均在90.0%~110%。与紫外可见分光光度法测试结果相比,相关系数(R2)为0.9952,为土壤硝态氮在现场检测奠定技术基础。 相似文献
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《Analytical letters》2012,45(5):343-346
Abstract An argentometric potentiometric method for the precise determination of formaldehyde using an iodide -ion electrode is described. Formaldehyde was determined by titrating the iodide-ion generated by the reaction with iodine in an alkaline medium. The accuracy and precision were better than 0.1% under the optimum condition. 相似文献
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主成分分析同时单点R滴定法研究 总被引:3,自引:1,他引:3
将主成分分析用于单点R滴定法中,同时测定了镍矿中Ni,Cu,Co含量,讨论了方法原理,指定电位的选择,建立了主成分分析常数矩阵,对20个模拟样和矿样进行了分析,均获得满意结果。 相似文献
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During the outbreak of novel coronavirus pneumonia, 84 Disinfectant has been widely used. It is very important to determine the available chlorine content in 84 Disinfectant. A new method to rapidly determine the available chlorine content in 84 Disinfectant by automatic potentiometric titration was established. Statistically, there is no significant difference in results between automatic potentiometric titration and manual titration. Combined the principles of analytical chemistry and the application to the determination of anti-epidemic material, this experiment has theoretical and practical significance, and can be used as an experiment in analytical chemistry laboratory for sophomore students. 相似文献