Determination of embedded layer properties using adaptive time-frequency domain analysis

A general model for determination of the complete set of acoustical and geometrical properties of an isotropic layer embedded between isotropic or anisotropic multilayered solids is developed. These properties include density, longitudinal and shear elastic moduli, layer thickness, and loss factors, simultaneously determined from two measurements, one at normal and one at oblique incidence. The inversion model is an extension of the method proposed by Lavrentyev and Rokhlin [J. Acoust. Soc. Am. 102, 3467 (1997)] which is applicable to thick substrates. In this new method, the inversion model mimics an experiment by using the same time-domain gating of the signal reflected from the embedded layer. This allows application of this method to layered solids when reflections from different layers overlap in the time domain. The sensitivity of the method, its stability against data scatter, and the effect of the oblique incident angle are evaluated. The effect of plane-wave approximation versus beam approximation in the inverse algorithm is discussed. Experimental results are given to demonstrate examples of adhesive layer property reconstruction.     

An ultrasonic method for determination of elastic moduli, density, attenuation and thickness of a polymer coating on a stiff plate

An ultrasonic method proposed by us for determination of the complete set of acoustical and geometrical properties of a thin isotropic layer between semispaces (J. Acoust. Soc. Am. 102 (1997) 3467) is extended to determination of the properties of a coating on a thin plate. The method allows simultaneous determination of the coating thickness, density, elastic moduli and attenuation (longitudinal and shear) from normal and oblique incidence reflection (transmission) frequency spectra. Reflection (transmission) from the coated plate is represented as a function of six nondimensional parameters of the coating which are determined from two experimentally measured spectra: one at normal and one at oblique incidence. The introduction of the set of nondimensional parameters allows one to transform the reconstruction process from one search in a six-dimensional space to two searches in three-dimensional spaces (one search for normal incidence and one for oblique). Thickness, density, and longitudinal and shear elastic moduli of the coating are calculated from the nondimensional parameters determined. The sensitivity of the method to individual properties and its stability against experimental noise are studied and the inversion algorithm is accordingly optimized. An example of the method and experimental measurement for comparison is given for a polypropylene coating on a steel foil.     

Dielectric susceptibility of a ferroelectric bilayer film with surface transition layers

Using the transverse Ising model within the framework of the mean-field theory, we investigate a ferroelectric bilayer film with the surface transition layer within each constituent slab and an antiferroelectric interfacial coupling between two slabs. The combined influence of the surface transition layer and antiferroelectric interfacial coupling on the dielectric susceptibility of a bilayer film is discussed in detail. The results show that the surface transition layer plays a crucial role in dielectric susceptibility of a bilayer film.     

套管-水泥界面微间隙厚度的低频超声反演方法

研究了应用低频超声垂直入射反射波实现套管-水泥界面流体微间隙薄层厚度的反演方法。应用灵敏度函数比较分析了分层系统反射谱各阶谐振频率处的相位跳变量较之各阶谐振频率作为反演特征量的优势。通过目标函数分析,选取分层系统3~10阶谐振频率处相位跳变量作为特征量,利用BP神经网络实验获得0.1~1.0 mm内不同间隙层厚度的反演结果。反演结果与真实值的平均相对误差为4.6%,最小反演厚度仅为波长的18%。所选取的相位特征量也可用于其它层状高声阻抗介质下的薄层厚度反演。      

Calculating acoustical properties of cells: influence of surface topography and liquid layer between cell and substrate.

In this paper, a mathematical formulation is presented to compute the V(z) of a tapering layered solid and applying this formulation to the determination of acoustic properties of biological cells and tissues. The formulation is adopted in the simplex inversion algorithm to obtain the acoustic properties of a tapering cell from its V(z) values. The influence of two parameters had been considered: The tapering angle and the presence of a thin liquid layer present between cells and the substratum to which they adhere. Up to a tapering angle less than 10 degrees, it can be safely neglected. However, if a larger angle is neglected, then the acoustic wave velocity in the cell is overestimated. Cell thickness estimation is not affected significantly when the tapering angle is ignored. The calculations of acoustic properties of cells are considerably influenced by the introduction of a thin fluid layer between the solid substratum and the overlying cell, neglecting the presence of at least a very thin layer (20-30 nm), in general, results in a considerable overestimation of sound velocity. The reliability of the data calculated from V(z) values was ascertained using an independent method to determine cell thickness by calculating it from the interference fringe pattern obtained with the reflection-interference light microscope. The shape of the glutaraldehyde-fixed cells was similar to fried eggs. The highest sound velocities were found close to the periphery of the dome-shaped cell center. In the very center and over most of the area of the thin periphery, sound velocity was close to that in saline.     

Note: Interfacial layer and phase inversion behavior in the blend of polyethersulfone and polycarbonate

A blend of polyethersulfone (PES) and polycarbonate (PC) with a ratio of 40/ 60 was studied by scanning electron microscopy (SEM), dynamic mechanical analysis, and transmission electron microscopy (TEM). It was found that the PES-PC blend is a partially miscible, two-phase system, and an interfacial layer exists between the phases of PES and PC. Specific interaction resulting from the n-complex between PES and PC provides the driving force for formation of the interfacial layer. In addition, phase inversion behavior was also observed for the 40/60 composition.     

三层介质超声谐振模式随材料和界面粘接性能变化的演变规律

在用超声波谐振对粘接材料的粘接强度进行无损评估时, 不同模式对粘接强度的敏感程度受到众多因素和参数的影响, 对检测结果的可靠性至关重要. 基于多层介质中声传播和界面弱粘接边界条件的理论模型, 将一个上下非对称的金属-粘接剂-金属三层结构的平面波反射系数函数中的谐振模式看作是上下铝金属层各自的Lamb波频散模式通过夹心粘接剂层相互耦合后叠加组成. 改变影响结构粘接强度的因素, 即粘接剂的性能参数(声阻抗、密度、厚度)和界面切向劲度系数k_t来分析三层结构谐振模式耦合方式的变化,得出结论: 粘接结构粘接性能的变化基本上不改变与被粘铝层相关的固有部分的Lamb波模式, 而它们的耦合模式则在谐振频率上产生平移并会与固有模式进行交换和替代; 不同参数的变化引起的模式演变有各自的规律, 大多可彼此区分.     

Electrostatic coupling with interfacial free charge in ferroelectric-paraelectric bilayers and superlattices

Based on a thermodynamic model, we studied the interfacial free charge effect on the polarization, spatial inversion symmetry, and dielectric response in ferroelectric-paraelectric bilayer. The broken spatial inversion symmetry and imprint due to free charge are not found. Effect of free charge on the dielectric constant is not monotonic. Contradiction between the equilibrium polarization and non-linear field-induced dielectric polarization in paraelectric layer is found. Our study reveals that treating coupling strength as an “input” parameter taken dependent of the polarization is inappropriate to describe electrostatic coupling with interfacial free charge.     

Characterization of various aluminium oxide layers by means of spectroscopic ellipsometry

This paper reports the characterization of both barrier type and porous type anodic oxide films on aluminium by means of spectroscopic ellipsometry (SE). In order to show the capabilities of the technique for quantitative determination of the layer characteristics, results based on ellipsometric data are correlated with complementary information from the analytical techniques transmission electron microscopy (TEM) and Auger electron spectroscopy (AES). It is concluded that ellipsometry yields an accurate characterization for the thicknesses and the interfacial properties of both the barrier layer and the porous layer. The porosity of the porous layer, determined with SE, is found to be in good agreement with the results obtained from TEM.     

The hysteresis loops of a ferroelectric bilayer film with surface transition layers

Based on the transverse Ising model in the framework of the mean field approximation,this paper discusses a ferroelectric bilayer film with the surface transition layers within each constituent slab and an antiferroelectric interfacial coupling between two slabs.The hysteresis loop of a bilayer film is investigated.The results show that the surface transition layer in a ferroelectric bilayer film plays a significant role in realizing the multiple-state memory.     

外场作用下铁电/铁磁双层膜的极化磁化性质

建立了铁电/铁磁双层膜模型,铁电层的电矩用连续标量描述,而铁磁层的自旋应用经典矢量描述.利用蒙特卡罗方法模拟了体系的热力学性质和极化、磁化行为.给出了零场下体系的内能、比热、极化和磁化随温度变化的关系,并分别研究了体系在外磁场和外电场下的极化和磁化行为.模拟结果表明,双层膜体系的内能、比热、极化和磁化性质因层间耦合系数的不同而明显不同,当界面耦合较弱时,双层膜表现出各自的热力学性质,当层间耦合增强到一定程度时,双层膜耦合为一个整体,表现出统一的热力学性质.该双层膜在外场中形成电滞回线和磁滞回线,并表现出偏置特性,界面耦合强度和温度影响滞后回线和偏置现象.     

Transverse acoustoelectric voltage inversion and its application to semiconductor surface study: CdS

The transverse acoustoelectric voltage inversion has been observed in CdS. It is found to be due to the inversion of the semiconductor surface. The inversion layer results from a high magnitude of the dc transverse acoustoelectric voltage developed on the semiconductor surface. The acoustoelectric voltage inversion is strongly dependent on the wavelength and intensity of light illuminating the semiconductor surface, and the power input of the SAW. The sub bandgap spectral response of the transverse acoustoelectric voltage determines the positions of the surface states in the energy gap. The above bandgap spectrum determines the photon energy in which transition from bulk to surface absorption takes place and the photon energy for complete surface absorption.     

Characterization methods for liquid interfacial layers

Liquid interfaces are met everywhere in our daily life. The corresponding interfacial properties and their modification play an important role in many modern technologies. Most prominent examples are all processes involved in the formation of foams and emulsions, as they are based on a fast creation of new surfaces, often of an immense extension. During the formation of an emulsion, for example, all freshly created and already existing interfaces are permanently subject to all types of deformation. This clearly entails the need of a quantitative knowledge on relevant dynamic interfacial properties and their changes under conditions pertinent to the technological processes. We report on the state of the art of interfacial layer characterization, including the determination of thermodynamic quantities as base line for a further quantitative analysis of the more important dynamic interfacial characteristics. Main focus of the presented work is on the experimental possibilities available at present to gain dynamic interfacial parameters, such as interfacial tensions, adsorbed amounts, interfacial composition, visco-elastic parameters, at shortest available surface ages and fastest possible interfacial perturbations. The experimental opportunities are presented along with examples for selected systems and theoretical models for a best data analysis. We also report on simulation results and concepts of necessary refinements and developments in this important field of interfacial dynamics.     

Damped vibration analysis of an elastically connected complex double-string system

The main purpose of the present paper is to consider theoretically damped transverse vibrations of an elastically connected double-string system. This system is treated as two viscoelastic strings with a Kelvin-Voigt viscoelastic layer between them. A theoretical analysis has been made for a simplified model of the system, in which assumed physical parameters make it possible to decouple the governing equations of motion by introducing the principal co-ordinates. Applying the method of separation of variables and the modal expansion method, exact analytical solutions for damped free and forced responses of the system subjected to arbitrarily distributed transverse continuous loads are determined in the case of arbitrary magnitude of linear viscous damping. It is important to note that the solutions obtained are explicitly expressed in terms of parameters characterizing the physical properties of the system under discussion. For the sake of completeness of the analysis, solutions for undamped free and forced vibrations are also formulated.     

High field magnetoconductivity of Si inversion layers

The transverse magnetoconductivity (σ_χχ) of electron inversion layers on (100) Si is measured in magnetic fields up to 220 kG at temperatures from 4.2 to 1.6 K. The dependence of σ_χχ on T, H, and the electric field along the inversion layer suggests that immobile electrons between two Landau subbands are to a large extent localized out of the top of the lower subband. Fine structure, which may be indicative of inhomogeneities of electronic origin, is observed in σ_χχ vs electron density.     

Vibration analysis and design optimization of viscoelastic sandwich cylindrical shell

Damping properties of viscoelastic sandwich structure can be improved by changing some parameters such as thickness of the layers, distribution of partial treatments, slippage between layers at the interfaces, cutting and its distribution at the top and core layers. Since the optimization problem may result in a thick core layer, for achieving more accuracy a new higher-order Taylor's expansion of transverse and in-plane displacement fields is developed for the core layer of sandwich cylindrical shell in which the displacement fields at the core layer are compatibly described in terms of the displacement fields at the elastic faces. The presented model includes fewer parameters than the previously developed models and therefore decreases the number of degree of freedom in the finite element modeling. The transverse normal stress in the core layer is also considered. The formulations are developed to consider the slippage between layers at the interfaces. Finally, by combining the finite element method and the optimization algorithms based on the genetic algorithm and sequential quadratic programming technique, a design optimization methodology has been formulated to maximize the damping characteristics using the optimal number and location of cuts and partial treatments with optimal thicknesses of top and core layers.     

铁电双层膜的反转动力学行为

基于Landau-Khalatnikov运动方程,本文研究了含有表面过渡层和铁电界面耦合的反转动力学行为(包括平均极化、反转时间、反转电流和矫顽场).研究结果表明:在铁电双层膜系统中存在一个竞争的机理,即表面过渡层与界面耦合的竞争作用.我们发现在双层膜反转过程中出现了反常行为,这些反常行为归因于表面过渡层与界面耦合之间的竞争.表面过渡层与界面耦合的共同行为对铁电双层膜的动力学特性起到了决定性的作用.     

Procedure for retrieving the optical properties of a two-layered medium from time-resolved reflectance measurements

A procedure for retrieving the optical properties of a two-layered diffusive medium based on an exact analytical solution of the diffusion equation and on relative multidistance time-resolved reflectance measurements is presented. The method overcomes some limitations of previously developed procedures. Five parameters of the medium have been fitted: the absorption and the reduced scattering coefficients of both layers and the thickness of the first layer. The actual values of the parameters are correctly retrieved by the procedure. The inversion procedure does not require an initial guess for the unknown optical properties, but the starting value for the thickness of the first layer needs to be estimated with an error smaller than 50%.     

Assessment of interface deformation and fracture in metal matrix composites under transverse loading conditions

The transverse properties of unidirectional metal matrix composites (MMCs) are dominated by the fiber/matrix interfacial properties, residual stresses and matrix mechanical response. In order to monitor and study, in situ, the failure of interfaces in titanium-based composites subjected to transverse loading conditions, an ultrasonic imaging technique has been developed. The interface was imaged ultrasonically and the change in ultrasonic amplitude with the transverse loading was monitored, indicating the sensitivity of the technique to fracture and deformation of interfaces. This change in amplitude has been explained in terms of the multiple reflection theory of ultrasonic waves. The multiple reflection theory enabled estimation of the interfacial deformation and debonding as a function of loading. The ultrasonic technique was also used in conjunction with finite element modeling in order to quantify the fiber/matrix interfacial transverse strength in situ in MMCs.