共查询到20条相似文献,搜索用时 31 毫秒
1.
Crystallography Reports - The Schiff base, 3-(2-(2-hydroxybenzylidene)hydrazinyl)quinoxalin-2(1H)-one has been synthesized by condensation of 3-hydrazinyl quinoxalin-2(1H)-one and salicylaldehyde... 相似文献
2.
Crystallography Reports - Two complexes with V-shaped ligands, [(L1)2Mn(H2O)4](HSA)2] (1), {[(L1)2Zn(H2O)2](HSA)2}n (2) (L1 = bis(4-(1H-imidazol-1-yl)phenyl)methanone, H2SA = salicylic acid), have... 相似文献
3.
Crystallography Reports - The title complex, {[Co4(DPT)4(bdc)4] · DPT · DMF · H2O} n (1) was prepared under hydrothermal condition (dimethylformamide and water) based on mixed... 相似文献
4.
Crystallography Reports - Two coordination polymers, {[L1Zn(adc)]2⋅5H2O}n (1), {[L1Cd(adc)]2⋅2.75H2O}n (2) (L1 = bis(4-(1H-imidazol-1-yl)phenyl)methanone, H2adc =... 相似文献
5.
Crystallography Reports - Two novel complexes, {[L1Ni(ipa)(H2O)]2(DMF)}n (1) and {[L1Zn(pa)]4(H2O)}n (2), (L1 = bis(4-(1H-benzo[d]imidazol-1-yl)phenyl)methanone, H2ipa = isophthalic acid, H2pa =... 相似文献
6.
Crystallography Reports - A cobalt coordination polymer, {[Co(L1)2(H2O)2] · (HCOO)2 · H2O}n, where L1 is a bis(4-(1H-imidazol-1-yl)phenyl)methanone, has been synthesized and characterized... 相似文献
7.
Crystallography Reports - The title compound, 1-(4-(5,6-dihydropyridazin-1(4H)-yl)phenyl)-N-methylmethanesulfonamide (C12H17N3O2S), was isolated as an impurity during the preparation of sumatriptan... 相似文献
8.
Crystallography Reports - 6,6'-(1E,1'E)-(ethane-1,2-diylbis(azan-1-yl-1-ylidene))bis(phenylmethan-1-yl-1-ylidene)bis(3-(octyloxy)phenol) has been synthesized and characterized by FTIR, 1H,... 相似文献
9.
Mao-Lin Hu Ping Yin Zhi-Cheng Ma Ali Morsali 《Journal of chemical crystallography》2008,38(11):807-813
Abstract Two new peptide compounds, 2(s)-(5-fluorouracil-1-aceto)amino-2-isopropyl acetate hemihydrate (1:1/2H
2
O) and 2(s)-(5-fluorouracil-1-aceto)amino-2-isopropyl acetic acid (2), have been synthesized and characterized by elemental analysis, IR, 1H- and 13C NMR spectroscopy. Two new compounds were structurally characterized by single-crystal X-ray diffraction. The thermal stabilities
of compounds 1:1/2H
2
O and 2 were studied by DSC-TGA techniques. The result of the biological test showed that the compounds 1:1/2H
2
O and 2 have certain antitumor activities.
Index Abstract Two new peptide compounds, 2(s)-(5-fluorouracil-1-aceto)amino-2-isopropyl acetate hemihydrate (1:1/2H2O) and 2(s)-(5-fluorouracil-1-aceto)amino-2-isopropyl
acetic acid (2), have been synthesized and characterized by elemental analysis, IR, 1H-, and 13C NMR spectroscopy. Two new
compounds were structurally characterized by single-crystal X-ray diffraction. The thermal stabilities of compounds 1:1/2H2O
and 2 were studied by DSC-TGA techniques. The result of the biological test showed that the compounds 1:1/2H2O and 2 have
certain antitumor activities.
相似文献
10.
Crystallography Reports - A cobalt coordination polymer with V-shaped ligands, {[Co0.5(L1) ⋅ (C4H2O4)0.5] ⋅ 0.25H2O}n, (L1 = 4-(1H-imidazol-1-yl)phenyl)methanone, C4H2O4 =... 相似文献
11.
Frans G. Moers Sandip K. Nayak René de Gelder Jan M.M. Smits Lambertus Thijs Binne Zwanenburg 《Journal of chemical crystallography》1999,29(9):1053-1056
The crystal and molecular structure of 2-{(R)-1-Hydroxy-1-[(2S)-1-tritylaziridin-2-y1] methy1}acrylate is described. Crystal data: C26H25NO3, orthorhombic, space group P212121, a = 9.6954(5), b = 13.1458(5), c = 16.7885(7) Å, V = 2139.8(2) Å3, Z = 4. The (R,S) diastereomer shows an intramolecular hydrogen bonding N···H—O under formation of a five-membered ring with N···O distance of 2.664 Å. IR, 1H NMR and 13C NMR data are discussed. The 1H NMR of the (R,S) diastereomer shows a singlet- whereas the (S,S) diastereomer exhibits a doublet-pattern for the hydroxyl proton. 相似文献
12.
Crystallography Reports - The title compound, C13H14BrN3O2, was synthesized by click chemistry (CuAAC) using 4-bromobut-1-yne and ethyl 4-azidobenzoate. Its molecular structure was determined by 1H... 相似文献
13.
14.
Li Zhong-Lin Feng Rui Fan Sheng-Qing Zhang De-Shuai Yang Qing-Qing Zhao Fang-Hua 《Journal of chemical crystallography》2022,52(1):97-104
Journal of Chemical Crystallography - Two new coordination polymers (CPs), namely, {[Zn(tib)(SO4)]·2H2O}n (1) and {[Cd(tib)(2,6-pydc)(H2O)]·H2O}n (2), have been hydrothermally synthesized... 相似文献
15.
16.
17.
Khajuria Rajni Sharma Suresh Kapoor Kamal K. Gupta Vivek K. 《Crystallography Reports》2017,62(7):1144-1147
Crystallography Reports - The title compound 6-phenyl-4-(p-tolyl)pyridin-2(1H)-one was synthesized via one-pot, three component reaction of (E)-1-phenyl-3-(p-tolyl)-2-propen-1-one, ethyl... 相似文献
18.
Crystallography Reports - Compound 1-(3-amino-4-morpholino-1H-indazole-1-carbonyl)-N-(4-methoxyphenyl)cyclopropane-1-carboxamide (C22H23N5O3, Mr = 870.96) was synthesized by condensation of... 相似文献
19.
Héctor Novoa de Armas Norbert M. Blaton Oswald M. Peeters Camiel J. De Ranter Margarita Suárez Estael Ochoa Yamila Verdecia Esperanza Salfrán 《Journal of chemical crystallography》2000,30(4):237-243
The synthesis and structural characterization of Methyl 6-chloro-4-(2-chlorophenyl)-5-formyl-2-methyl-1,4-dihydropyridine-3-carboxylate is described. The structure was refined to R1 = 0.0470 for 2665 reflections (with I > 2(I)). Crystal data: C15H13C12NO3, monoclinic,space group P21/c, a = 11.163(9), b = 14.484(8), c = 9.422(7) Å, V = 1512.9(19) Å3, Z = 4. The results of crystallographic and molecular modeling (AM1) were compared. The Cl atom attached to the phenyl group has two possible orientations, having 75% (sp) and 25% (ap) occupancy, respectively. The molecules in the crystal are held together by means of intermolecular hydrogen bonds of the type N=H...O and by C=H...O interactions. 相似文献
20.
Crystallography Reports - (E)-4-(2-(4-Cyanobenzylidene)hydrazinyl)benzonitrile dimethyl sulfoxide hemisolvate, C15H10N4 ⋅ 0.5C2H6OS is synthesized following a green protocol and its crystal... 相似文献