Evolution of triple junction defect structure at plastic deformation of metallic polycrystals

A method for the determination of the components of the Frank vector of disclinations in triple junctions (TJ) of real polycrystalline aggregates has been proposed. Using this method we found that real polycrystals contain junction disclinations (JD), the nature of which is related to their thermo-mechanical history. One of the elements of the evolution of the network of initial junction disclinations is the formation of disclination dipole configurations in the adjacent TJ. The influence of the types of boundaries forming the junctions on JD Frank vector power is discussed.     

Mesoscale plastic deformation of aluminum polycrystals

A study is made of the mechanism of plastic deformation at the mesoscale level in flat specimens of aluminum polycrystals. The mechanism is examined with the use of high-resolution optical-television system TOMSC-1. It is shown that a multilevel mesoscale structure is formed in the specimen as it is deformed. The formation of this structure leads to the appearance of two types of stationary waves 120 μm and 4.8 mm long. The results are interpreted within the framework of a hierarchy of mesoscale levels of deformation and are linked with the decisive role of surface oxide films in the formation of the mesoband structure and stationary waves associated plastic flow. Institute of the Physics of Strength and Materials Science, Siberian Branch of the Russian Academy of Sciences. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 1, pp. 31–39, January, 1997.     

Stress relaxation in the region of microplastic deformation of polycrystals

Stress relaxation equations are derived to predict the relaxation capacity of a material on the basis of studies of microplastic deformation under static loading. The approach was checked experimentally on spring steels LANKMts, ÉI702, ÉP637, and 50KhFA.Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 7, pp. 37–41, July, 1987.     

A model of grain refinement and strengthening of Al alloys due to cold severe plastic deformation

This paper presents a model which quantitatively predicts grain refinement and strength/hardness of Al alloys after very high levels of cold deformation through processes including cold rolling, equal channel angular pressing (ECAP), multiple forging (MF), accumulative roll bonding (ARB) and embossing. The model deals with materials in which plastic deformation is exclusively due to dislocation movement within grains, which is in good approximation the case for many metallic alloys at low temperature, for instance aluminium alloys. In the early stages of deformation, the generated dislocations are stored in grains and contribute to overall strength. With increase in strain, excess dislocations form and/or move to new cell walls/grain boundaries and grains are refined. We examine this model using both our own data as well as the data in the literature. It is shown that grain size and strength/hardness are predicted to a good accuracy.     

Grain boundary role and behaviour during high-temperature deformation of polycrystals

Data concerning the phenomenology and nature of some grain boundary (GB) processes — dynamic recovery at GB and GB sliding during high temperature deformation of polycrystals are given. On the basis of these data a new model of superplasticity (SP) is discussed. The possibility of realization of SP at relatively low temperatures is shown.     

Dislocation structure of plastic relaxation waves in polycrystals and alloys under intense shock wave loading

The influence of the structure factors (sizes of grains and precipitates) on the dislocation structure formed in polycrystals and alloys behind the shock wave front (elastic precursor) has been theoretically discussed in terms of the dislocation kinetic relationships and kinetic equation for the dislocation density. The critical conditions of the transition from the cellular dislocation structure to a uniform dislocation distribution have been formulated. These conditions are used to determine the dependences of the critical pressure, above which the dislocation distribution becomes uniform, on the grain size and precipitate volume density.     

On the annealing of junction disclinations in deformed polycrystals

The kinetics of relaxation of disclination quadrupoles formed within triple junctions of grains during plastic deformation are studied. The calculations are made using the discrete dislocation model for disclinations by simulating the climb of dislocations. Exponential relationships are obtained for the relaxation of the strength and elastic energy of disclination quadrupoles with a characteristic time proportional to the cube of grain size. The distribution of vacancy fluxes along grain boundaries (GBs) during the relaxation of a disclination quadrupole is studied in detail. The relation between continuum and discrete dislocation approaches to a study of the GB recovery process is considered. Characteristics of each relaxation stage are studied. A hierarchy of characteristic relaxation times for dimerent grain size ranges is constructed and it is show that in nanocrystalline materials the spreading time of trapped lattice dislocations can depend on the grain size.     

Investigation of relaxation processes in nanocrystalline cobalt produced by severe plastic deformation

It has been shown that the dependence of the width of X-ray diffraction lines of plastically deformed cobalt on the annealing temperature is described by the exponential function. Characteristic temperature regions corresponding to the processes of recovery and recrystallization have been established. It has been shown that the values of the activation energy of recrystallization determined from the experimental data are comparable with the activation energy of the grain-boundary diffusion in metals. The activation energy for the recovery region is considerably lower than the activation energy of migration of nonequilibrium grain boundaries in nanocrystalline metals. The X-ray diffraction data have been confirmed by the investigations of the microstructure and microhardness.     

Elastic and plastic deformation of NaCl and Ni3Al polycrystals during compression in a multi-anvil apparatus

Abstract

The compression behaviour in a multi-anvil apparatus of pure NaCl and of a foil of Ni₃Al embedded in a pressure medium of NaCl has been studied by energy-dispersive X-ray diffraction. At ambient temperature, the pressure and stresses, determined from line positions of NaCl, were constant throughout the sample chamber. Line positions and line widths of NaCl reflections were reversible on pressure release. A saturation of microstrains observed in NaCl at 2 GPa is thus attributed to brittle fracture setting in at uniaxial stresses of around 0.3 GPa. Ni₃Al polycrystals, in contrast, undergo extensive (ductile) plastic deformation above 4 GPa. The compression behaviour of both Ni₃Al and NaCl is identical to that previously determined in a diamond anvil cell. While a multi-anvil device thus has the advantage, compared with a diamond anvil cell, of constant pressure and stress throughout the sample chamber, microstrains in poly-crystalline samples arise in both devices. Samples in a multi-anvil apparatus thus need to be mixed with a pressure medium and to consist of essentially single crystals just as in a diamond anvil cell. Annealing experiments at high pressures confirm that the release of the uniaxial stress component in the pressure medium does not cause a release of microstrains in the embedded sample if the latter has been plastically deformed. Annealing for the purpose of attaining hydrostatic conditions in compression studies thus has to be carried out with care.     

Surface size effects under plastic deformation of microcrystals and nanocrystals

The size effects associated with the crystal surface as an effective sink for moving dislocations in a thin crystal and as a barrier for these dislocations in the presence of a high-strength film or a special hardened layer on the surface, which favor the accumulation of dislocations in the crystal, have been considered theoretically in terms of the kinetic equation for the density of dislocations concentrated in the crystal in the critical lengths of single-ended (unipolar) dislocation sources. The theoretical results have been illustrated by the experimental data available in the literature for microcrystals and nanocrystals of copper and aluminum. It has been found in accordance with these data that the dependence of the yield stress ??_2% of the crystal on the crystal transverse size D has the form ??_2% ?? D ^?0.75 when there is a free crystal surface for the escape ofthe dislocations and ??_2% ?? D ^?0.5 when there is a high-strength layer on the lateral surface of the crystal..     

Grain boundary sliding and lattice dislocation emission in nanocrystalline materials under plastic deformation

A theoretical model is proposed to describe the physical mechanisms of hardening and softening of nanocrystalline materials during superplastic deformation. According to this model, triple interface junctions are obstacles to glide motion of grain boundary dislocations, which are carriers of grain boundary glide deformation. Transformations of an ensemble of grain boundary dislocations that occur at triple interface junctions bring about the formation of partial dislocations and the local migration of triple junctions. The energy characteristics of these transformations are considered. Pileups of partial dislocations at triple junctions cause hardening and initiate intragrain lattice sliding. When the Burgers vectors of partial dislocations reach a critical value, lattice dislocations are emitted and glide into adjacent grains, thereby smoothing the hardening effect. The local migration of triple interface junctions (caused by grain boundary sliding) and the emission of lattice dislocations bring about softening of a nanocrystalline material. The flow stress is found as a function of the total plastic strain, and the result agrees well with experimental data.     

Contribution from dislocation to deformation resistance in polycrystals of copper-based solid solutions

The evolution of dislocation structure in solid solutions of Cu-Al and Cu-Mn systems with different grain sizes and at different test temperatures is studied by means of transmission electron diffraction microscopy. The scalar density of dislocations is measured and its relationship to the flow stress of alloys is determined. Changes in the contribution from dislocation hardening to deformation resistance upon variations in the contributions associated with changes in grain size, solid-solution hardening, and test temperature are analyzed.     

Characteristics of the relaxation to steady-state deformation in solids

The characteristics of the transient process of relaxation to steady-state deformation in solids are investigated theoretically. Various loading regimes are modeled by the method of mobile cellular automata. It is shown that the stressed state in a material is highly inhomogeneous in the relaxation stage; this property, in turn, can produce stable structures in the velocity field of the material particles and influence the evolution of deformation in later stages. Zh. Tekh. Fiz. 67, 34–37 (September 1997)