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钕钇异核谷氨酸配合物的合成及晶体结构 总被引:3,自引:1,他引:3
在水溶液中合成发钕钇异核谷氨酸配合物[(Nd4/3Y2/3(Glu)2(H2O)8)4](ClO4)16.10H2O的单晶,并测定其结构。晶体属单斜晶系,P21空间群,晶胞参数:a=1.1037(5)nm,b=1.6710(5)nm,c=2.0086(10)nm,β=102.80(4)°,V=3.612(3)nm^3,Z=1,Dc=2.079g/cm^3。最终偏差因子R=0.058。钕和钇对中心位 相似文献
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警惕锌剂治疗的毒性和副作用 总被引:1,自引:0,他引:1
临床实践证明某些疾病补锌治疗有效,但也发现1%左右的人出现副作用,人类对锌过量虽具有耐受性,但据报道不管是急性中毒量,治疗量,还是常用的自选补充量,均可出现中毒症状。原因是锌与其它元素间有相互作用,特别是与铜的拮抗作用,所以用锌剂一定要严格掌握适应症、剂量、疗程,以免引起不良反应,影响儿童健康。 相似文献
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酶是生物催化剂,在数以千计的酶中,第一大类以烟酰胺腺嘌呤核苷酸(NAD/NADH)为辅酶的多种氧化-还原酶需要金属离子作为辅助因子而发生独特的催化功能。其中含锌的醇脱氨酶(ADH)是目前研究得最多的一种。本文用电化学分析法研究稀土离子对乳酸脱氢酶(LDH)和谷氨酸脱氢酶(GDH)两体系的作用时也探讨了Zn2+在此两体系中的作用。结果指出在LDH体系中不需要 Zn2+;在 GDH(牛肝中提取)体系中, Zn2+是一种强抑制剂,Eu3+可以缓解它的抑制作用,但是在黄瓜根系提取的粗GDH体系中,Zn2+必需存在于反介质中起激活酶的催化作用。 相似文献
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腹泻病患儿发锌测定与补锌的疗效观察 总被引:3,自引:1,他引:3
测定了110名急性腹泻病患儿的发锌,并对52名急性腹泻病患儿补锌治疗。结果表明,腹泻患儿缺锌率高于健康儿,而补锌可使该病的退热和止泻时间明显缩短。 相似文献
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锌磷酸铝分子筛ZAPO—34的合成 总被引:1,自引:0,他引:1
硅磷酸铝分子筛SAPO-34是SAPO-n系列分子筛中的一员,结构类型与菱沸石(Cbabazite)相当,属小孔沸石类,孔口大小为4.3(?),孔体积为0.42cm~2/g。1985年我们合成了这种分子筛,作为甲醇转化制低碳烯烃的催化剂,它具有较高的活性和较好 相似文献
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Both zinc and the amino acid cysteine play important roles in biological function, including antioxidant protection and tissue repair. We attempted to prepare a (1:l) zinc‐cysteine complex using L‐cysteine and zinc metal. Zinc metal was added to a solution of L‐cysteine and refluxed with constant stirring. The product was selected by filtration and, after evaporation precipitation, was subjected to elemental analysis, 1H NMR, and mass spectroscopy. The novel compound has one molecule of zinc conjugated to one molecule of cysteine. 相似文献
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Molecular precursors phthalimidomethyl phthalic acid and phthalimidomethyl phthalonitrile were synthesized for the first time and both were able to condensation to form tetra-phthalimidomethyl phthalocyanine zinc through “ammomium molybdate method” and “DBU method ”respectively. The precursors and title compounds were char-acterized by element analysis, IR, UV/Vis as well as NMR. The two synthesis methods were compared, the result indicated that using the phthalimidomethyl phthalic acid as precursor through the former method, the product was an isomer with C4h symmetry, while using phthalimidomethyl phthalonitrile as precursor through the latter method, the products were a mixture of different isomers. 相似文献
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D. Mruga Dr. O. Soldatkin K. Paliienko A. Topcheva Dr. N. Krisanova D. Kucherenko Prof. Dr. T. Borisova Dr. S. Dzyadevych Dr. A. Soldatkin 《Electroanalysis》2021,33(5):1299-1307
Today, the concentration of glutamate in the patient′s blood is an important indicator in medical diagnostics; therefore, it is necessary to have a simple, accurate, and fast tool to obtain the data. Here, a recently developed amperometric glutamate-sensitive biosensor was optimized to improve its characteristics. The platinum disk electrode was used as a transducer. As a bioselective element we used the enzyme glutamate oxidase, covalently crosslinked with bovine serum albumin by glutaraldehyde. Circumstances of enzyme immobilization on the transducer‘s surface were optimized (enzyme and glutaraldehyde concentrations and immobilization duration). To test the ability of this biosensor to work in biological environments containing complex biological substances, the influence of the working solution was investigated (concentration of the working buffer, its temperature, presence of the protein in the analyzed sample). The linear range of biosensor was from 5 to 600 μM of glutamate and the sensitivity was 150–200 nA/mM. Measurements of glutamate concentrations in the blood plasma were performed by biosensor and glutamate dehydrogenase assay. The linear correlation between the methods was found in a range of 50.4–182.5 μM (R2=0.99). Thus, it has been shown that the developed biosensor makes it possible to measure the concentration of glutamate in blood plasma. 相似文献
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HPLC法测定鸡精中谷氨酸钠的含量 总被引:3,自引:0,他引:3
以邻苯二甲醛与谷氨酸钠中的氨基进行柱前在线衍生化反应,采用C18色谱柱分离、荧光检测器(激发340nm,发射450nm)进行测定,建立了柱前衍生反相高效液相色谱测定鸡精中谷氨酸钠含量的方法。该方法相对标准偏差为0.69%,加标回收率为99.1%~101%,在0.10~50.0mg/L范围内,谷氨酸钠的峰面积和浓度之间的相关系数为0.9999,保留时间和峰面积的相对标准偏差分别为1.22%和0.71%,鸡精中谷氨酸钠定量下限为0.2μg/g。 相似文献
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锌与甲壳胺络合物的制备 总被引:10,自引:2,他引:10
甲壳胺是甲壳素(2-乙酰氨基-1,4-个葡聚糖)脱乙酰基后的产物,学名为2-氨基-l.4-个葡聚糖,目前主要从虾、蟹壳中提取.这的用途很广,涉及诸多领域[1].甲壳胺有杀菌、抑菌、消炎、促进伤口愈合的功能,有降低胆固醇,增强免疫力,体内排毒,防治胃溃疡和胃酸过多等功能,它对人体细胞无毒,且有亲和性,不与体液反应,也无抗原抗体反应,国内外已有许多报道[2].本文报道克服甲壳胺只能溶于弱酸溶液的缺点,将其氧化降解成水溶性低聚物后,作为锌的配体,探讨二者络合的条件及所形成络合物的一些性质,以期能为人体补锌提供新的途… 相似文献
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碱性锌锰电池用化学二氧化锰的研制 总被引:2,自引:0,他引:2
以直接氧化法生成的初级二氧化锰经饱和水蒸汽处理后,进行重质化处理,制成碱性锌锰电池用化学二氧化锰,所研制样品表现出n-型半导体特征,从X射线衍射、热重分析的测试,发现成品的理化性能和结合水含量有较大的改进,电化学活性也有较大提高,所制成LR03实体电池电性能优良. 相似文献
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