基于SM-NCF反射光谱辨识的液体折射率监测方法

针对分子生物学与环境监测领域高灵敏度特异性检测需求,提出一种基于反射光谱特征辨识的单端反射式光纤折射率传感器模型,并给出了这种基于多模干涉原理的单模光纤-无芯光纤(Single mode fiber-No core fiber, SM-NCF)串接结构传感机理及其理论模型。无芯光纤实质上是一种结构特殊的多模光纤,在实际应用中无芯光纤结构本身作为纤芯,外界环境介质当作包层,构成光波导结构。这与普通多模光纤相比,不需要采用氢氟酸对多模光纤的包层进行化学腐蚀,不会降低光纤的机械性能,也不会破坏芯模传输条件,可以更好的实现对周围环境折射率的传感监测。当无芯光纤所处外界环境折射率发生改变时,其波导结构和包层有效折射率均会发生改变,从而引起传输光信号的纵向传播常数和模场分布也会随之发生改变,最终导致不同波长对应传输光功率的变化。上述效应反映在反射光谱上,即干涉波谷对应的谐振波长、波谷峰值强度以及半波宽度发生相应变化,通过辨识该反射光谱特征就可实现对外界环境折射率的测量。借助光束传播法(BPM),数值模拟得到无芯光纤长度分别为自映像距离和非自映像距离时的SM-NCF内部光场能量分布规律,并制作了无芯光纤长度分别为自映像距离和非自映像距离的SM-NCF光纤折射率传感探头,将作为传感区域的无芯光纤一端与标准单模光纤熔接,采用磁控溅射技术在无芯光纤另一端面镀上金膜,用以提升反射光谱强度。在此基础上,搭建了基于SM-NCF终端反射型的光纤折射率试验系统,并开展了相关实验研究。研究结果表明,当无芯光纤长度是15 mm(自映像距离)时,随着液体折射率从1.331 5依次增大至1.390 2,SM-NCF反射光谱逐渐向长波方向偏移,其反射峰谐振波长对应的折射率灵敏度约为197.57 nm·RIU-1,相关系数为0.93;反射峰值强度也呈现逐渐降低趋势,其折射率灵敏度约为-62.80 dB·RIU-1。当无芯光纤长度是20 mm(非自映像距离)时,随着液体折射率依次增大,SM-NCF反射光谱呈现明显双峰现象,且均逐渐向长波方向偏移,dip2谐振峰波长折射率灵敏度约为133 nm·RIU-1,相关系数为0.96;反射峰值强度也呈现逐渐降低趋势,其折射率灵敏度约为-31.66 dB·RIU-1。对比分析可知,不论是从反射峰谐振波长偏移的角度,还是从反射峰值强度的角度,自映像距离长度对应的 SM-NCF终端反射型光纤传感器均具有较高灵敏度。对于相同折射率液体环境,非自映像距离长度对应的SM-NCF反射光谱半波宽度与自映像距离长度相比,呈现显著变窄趋势。相对于SMS透射型传感结构,当传感区域长度相同时,SM-NCF反射型结构能够实现对光波信号的往返两次调节。这种终端反射型SM-NCF传感器改进了传统透射型折射率传感器不便与待测液体相接触的缺点,具有结构简单、易于制作、抗电磁干扰能力强以及便于远程遥测等优点,能够为后续生化与环保监测领域研究应用提供有益支持。     

Relative humidity sensor based on SMS fiber structure with polyvinyl alcohol coating

A novel relative humidity (RH) sensor based on single-mode–multimode–single-mode (SMS) fiber structure is presented. The sensors are created through coating a thin layer of polyvinyl alcohol (PVA) on the multimode fiber deleted the cladding trough HF solution cauterization as the sensitive cladding film, whose refractive index varies as a function of humidity level. Due to the SMS fiber structure's sensitivity to ambient refractive index, the transmission spectra of SMS fiber structure coated PVA film are modified under exposure to different ambient humidity levels ranging from 30% to 80% RH. The related numerical simulations of transmission spectra of SMS fiber structure with different surrounding refractive index are also proposed. The sensitive of the RH measurement of 0.09 nm/% RH in the range from 30% to 80% RH is experimentally achieved. Meanwhile the intensity of wavelength at 1543 nm is decreasing as the humidity increasing. The experimental results obtained are consistent with the conclusion obtained by numerical simulating.     

Refractive index profiling of a GRIN optical fiber using a modulated speckled sheet of light

A method for calculating the refractive index of GRIN optical fiber from its transverse interference pattern is presented.In this method the transverse interference fringe pattern through an optical fiber using a sheet of light is applied to get the refractive index profile of it. The optical fiber is not immersed in a matching liquid as used in different techniques [Barakat N, El-Hennawi HA, El-Zaiat SY, Hassan R. Pure Appl Opt 1996;5:27].In this method a sheet of He–Ne laser light is allowed to illuminate the fiber. The light sheet is divided into two parts, the first is refracted through the fiber while the second is used as a reference beam. Interference pattern will be obtained between these two rays displaying the refractive index variation along the fiber radius.The fringe shift of such interference pattern has been measured and used to calculate the deflection angle of light refracted by the fiber and the cladding. An equation is derived to calculate the refractive index profile difference ratio δn at different positions across the fiber cross section in terms of the corresponding deflection angle and is verified experimentally.The optical path difference between these two rays (refracted and reference beam divided by the fiber) has been derived and the fringe shift obtained has been used to calculate the refractive index profile of the fiber.Introducing a ground glass screen on the passage of the two light beams (refracted and reference beam divided by the fiber), two superimposed identical speckle patterns are formed leading to the formation of a third speckle pattern modulated by a grid structure displaying the optical thickness of the fiber.     

超细低水峰抗弯损光纤的设计及制作

采用全合成预制棒制造法（VAD＋OVD）和改进的G.652.D光纤拉制法制造光纤.研究了工艺中光纤芯径的大小、第一包层的厚度、芯包折射率差、芯包比等参量与光纤弯曲性能的关系,并据此制作了几种超细低水峰抗弯损光纤.该光纤的裸光纤直径约80 μm,涂覆后成品光纤直径约140 μm,当弯曲半径不小于7.5 mm时,能够在1 260～1 625 nm整个波段内满足DWMD的传输要求.     

Compact optical fiber curvature sensor based on concatenating two tapers

A low-loss, compact, and highly sensitive optical fiber curvature sensor is presented. The device consists of two identical low-loss fused fiber tapers in tandem separated by a distance L. When the optical fiber is kept straight and fixed, no interference pattern appears in the transmitted spectrum. However, when the device is bent, the symmetry of the straight taper is lost and the first taper couples light into the cladding modes. In the second taper, a fraction of the total light guided by the cladding modes will be coupled back to the fundamental mode, producing an interference pattern in the transmitted spectrum. As the fiber device is bent, visibility of the interference fringes grows, reaching values close to 1. The dynamic range of the device can be tailored by the proper selection of taper diameter and separation between tapers. The effects of temperature and refractive index of the external medium on the response of the curvature sensor is also discussed.     

振幅掩膜紫外写入的长周期光纤光栅特性研究

振幅掩膜紫外写入的长周期光纤光栅的纤芯折射率分布函数为矩形波。以三层阶跃折射率光波导结构基础，用弱导标量近似和标量耦合模理论分析折射率调制类型为矩形波的长周期光纤光栅的特性。详细地给出耦合模方程近似处理的方法，并说明了其合理性。用数学软件Matlab进行了数值模拟计算，发现折射率调制类为矩形波的光栅传输谱不是由它的各次余弦光栅谱的线性叠加而成的。还研究了外部环境折射率、包层半径、栅占空比等光栅结构参量对矩形折射率调制的光栅传输谱的影响。同时指出了每阶包层模的双谐振峰位置随栅参量的变化规律。刊■刊『_型，刿j1     

Simplified coupling power model for fibers fusion

Fiber coupler fabrication used for an optical waveguide requires lossless power for an optimal application. The previous research coupled fibers were successfully fabricated by injecting hydrogen flow at 1 bar and fused slightly by unstable torch flame in the range of 800–1350°C. Optical parameters may vary significantly over wide range physical properties. Coupling coefficient and refractive index are estimated from the experimental result of the coupling ratio distribution from 1% to 75%. The change of geometrical fiber affects the normalized frequency V even for single mode fibers. V is derived and some parametric variations are performed on the left and right hand side of the coupling region. A partial power is modelled and derived using V, normalized lateral phase constant u, and normalized lateral attenuation constant, w through the second kind of modified Bessel function of the l order, which obeys the normal mode and normalized propagation constant b. Total power is maintained constant in order to comply with the energy conservation law. The power is integrated through V, u, and w over the pulling length of 7500 μm for 1-D. The core radius of a fiber significantly affects V and power partially at coupling region rather than wavelength and refractive index of core and cladding. This model has power phenomena in transmission and reflection for an optical switch and tunable filter.     

Design and performance of a plastic optical fiber leakage sensor

In this article design and operation of a plastic optical fiber (POF) sensor based on the unconventional light leakage from one fiber to another one causing intensity modulation are presented. The dominant loss mechanism was found to be the evanescent loss and based on this phenomenon the optical fiber sensor was designed. The penetration depth of evanescent wave as a function of different refractive index of cladding was calculated. Operation of this sensor was tested as a liquid level sensor for different liquids and the experimental results are compared. The dry (air interface layer) and wet output (liquid interface layer) signals for this probe were measured for a series of measurements and important factors concerning sensor operation are described. The precision of measured values, reproducibility of the results (1.35% error), and the stability of sensing operation as a function of time at different launching powers are also reported (0.85% error). The reported results for this design are promising and verify the successful operation of such a device as a liquid level probe and also as an on/off level switch.     

基于高折射率液体填充的花瓣形微结构光纤可调滤模特性

提出一种新型的可调滤模光纤结构,利用纤芯模式与微结构包层形成的超模群之间的耦合实现选择性滤模,采用花瓣形包层结构使包层中传输的模式更容易产生高的泄漏损耗;提出以液体填充包层介质柱,使包层形成的超模群有效折射率区间可以通过环境温度来调节,从而达到可调选择性滤模目的.利用液体柱的LP11模所形成的超模群,有效增大了其工作带宽和温度调谐范围.数值模拟结果表明,采用长度仅为71.4 mm的滤模光纤,可以使特定的抑制模式损耗达到20 dB以上,而其他模式损耗均在1 dB以下.提出的光纤可以在少模光纤传输系统中作为滤模器使用,以降低模式转换器、复用器/解复用器以及光开关和光路由等的模式串扰.     

Study on magnetic fluid optical fiber devices for optical logic operations by characteristics of superparamagnetic nanoparticles and magnetic fluids

We propose two optical fiber-based schemes using two magnetic fluid optical fiber modulators in series or in parallel for optical logic signal processing and operation. Here, each magnetic fluid optical fiber modulator consists of a bare multimode fiber surrounded by magnetic fluid in which the refractive index is adjustable by applying external magnetic fields amplifying the input electrical signal to vary the transmission intensity of the optical fiber-based scheme. The physical mechanisms for the performances of the magnetic fluid optical fiber devices, such as the transmission loss related to Boolean number of the logic operation as well as the dynamic response, are studied by the characteristics of superparamagnetic nanoparticles and magnetic fluids. For example, in the dynamic response composed of the retarding and response sub-procedures except the response times of the actuation coil, the theoretical evaluation of the retarding time variation with cladding magnetic fluids length has good agreement with the experimental results.     

Monitoring some liquid cladding layer properties using LED beam transmittance coefficients through the fiber itself

We report work on the adaptation of a conventional optical fiber assembly to monitor the properties of liquid. An LED¹ was used in conjunction with a home-made fiber cell fitted with glass fiber rods to monitor some of the physical properties of liquid samples. The technique discriminates between different liquids using their light transmittance ability as cladding layer to the glass fiber. Discrimination between liquids according to their transmission coefficients is partly dependant on refractive index of liquids; therefore, samples were also tested with a refractometer for comparison. Results show that the technique is superior to the refractometer in distinguishing between liquids of different indexes.     

复合纺丝法制备聚合物瓣状光纤的研究

瓣状光纤(SCF)由高折射率均匀芯层和高低折射率区域交替的皮层组成, 可有效地实现大纤芯单模运行。提出了采用复合纺丝法一步制备瓣状光纤。采用聚碳酸酯(PC)和聚甲基丙烯酸甲酯(PMMA)成功地制备截面符合设计要求的聚合物瓣状光纤。所制光纤的纤芯直径为40 μm。并用白光作为光源, 考察了所制光纤在500～1000 nm波段范围的出射光谱。从出射光谱可以看出, 所制光纤在730～830 nm波段范围内透射率比较高。通过截断法对所得光纤在500～1000 nm波段范围的传输损耗进行测试, 结果表明所制光纤的传输损耗比较大, 最大为30 dB/m。采用532 nm绿色激光作为光源, 通过CCD采集60 cm所得光纤的光斑。     

Influence of uniaxial crystal material cladding on reflectivity and dispersion of uniform fiber Bragg grating

The fiber Bragg grating with cladding made of uniaxial crystal material whose optical axis is parallel to the axis of fiber Bragg grating proposed in the paper published in 2003 was investigated again and an error was corrected in the calculation, its effective index, reflectivity and dispersion were examined using coupled-mode theory and numeric solution. The calculated results indicate that no low frequency cutoff phenomenon exists in the HE₁₁ mode, more power is transmitted by the core of the fiber with cladding made of isotropic material, the reflectivity of the fiber Bragg grating with cladding made of uniaxial crystal material is much higher than that with cladding made of isotropic material, the parameter K_cl, i.e., the ratio of the extraordinary to the ordinary ray refractive index, has a stronger impact on the reflectivity, Bragg wavelength and the dispersion of this kind of fiber Bragg grating when it varied from 1.00 to 1.01 than in other regions. This means that the characteristics of the fiber Bragg grating with uniaxial crystal cladding can be changed through adjusting K_cl while keeping its length, periodicity and the other parameters as constants.     

Determination of the refractive index profile of a symmetric fiber preform by the transport of intensity equation

The refractive index profile of an axially symmetric fiber preform is determined by using the transport of intensity equation. In this method the preform is immersed in an index-matching liquid, and a collimated light beam impinges on it laterally. The intensity distributions of the transmitted light are measured on two close parallel planes inside the preform core. From the recorded intensity distributions, the deflection function is calculated by the transport of intensity equation. The refractive index profile is obtained by means of Abel inversion. Also, for comparison, the refractive index profile of the preform is measured by the focusing method and the results are in agreement with less than 3% error.     

基于白光扫描干涉法的光纤折射率分布的测量

提出了一种光纤折射率分布的测量方法,采用白光扫描干涉技术,并在参考镜上构造与光纤样品相同的结构来克服白光相干长度短的限制,优化了光路,提高了干涉条纹间的对比度。采用与白光干涉信号的包络线呈高斯分布的Morlet小波作为小波变换的母小波进行拟合处理,得到光纤与已知折射率的匹配液之间的相对高度。通过计算获得光纤的折射率分布,并对获得的数据采用光纤折射率分布的经典函数进行拟合,得到多模光纤和单模光纤的决定系数分别为0.997 2和0.996 4。最后将实验获得的结果与官方参数进行比较,误差为0.01%,表明该种方法测量的精度较高,完全可以用来测量光纤的折射率。     

电光聚合物波导中的锥形结构

提出并设计了一种基于电光聚合物的锥形波导,可用于单模光纤与电光聚合物波导器件之间的连接.锥形波导中采用了宽度锥形和折射率锥形结构.宽度锥形采用劈形形状,通过宽度和折射率的缓慢变化实现模场转换.劈形形状的宽度锥形具有较小的损耗且易于制作,折射率锥形可采用灰度掩膜光刻技术制作.研究了锥形波导的传输损耗与锥形波导的长度、波导宽度和厚度、材料吸收损耗等参数的关系及其优化,分析了锥形波导中的功率传输、模场分布与模式转换效率.结果显示锥形波导的传输损耗小于0.37 dB,光纤-波导-光纤的连接损耗优于1.62 dB,对插入损耗的改善达到8.78 dB,模场转换效率达到了83.7%.     

侧边抛磨光纤中传输光功率变化的实验研究

针对轮式光纤侧边抛磨法制备的侧边抛磨光纤,研究了在侧边抛磨区覆盖不同折射率的材料时,侧边抛磨光纤传输光功率随覆盖材料折射率变化的特性.研究表明,侧边抛磨光纤中传输光功率会随抛磨区覆盖材料折射率的变化而改变.当覆盖材料的折射率小于1.437 8时,光功率损耗近似为零；而当覆盖材料的折射率逐渐增大接近1.452 1时,光功率损耗迅速增大至最大值.当覆盖材料的折射率由1.453 2逐渐增大时,光功率损耗由最大值逐渐减小,最终维持在某个确定的值.侧边抛磨光纤并不是抛磨深度越深,损耗就越大.侧边抛磨光纤中传输的光功率存在波长相关损耗(WDL）.实验结果与理论结论符合较好.     

染料掺杂液晶可调谐光纤荧光光源的研究

本文提出了染料掺杂液晶填充空心光纤构造荧光可调谐光源.基于染料分子能级结构理论分析B4400荧光光谱依赖温度的变化特性,采用脉宽8 ns,波长为532 nm YAG倍频脉冲激光器抽运,向列相液晶作基体,实验分析染料B4400掺杂液晶填充空心光纤荧光光谱选择性荧光放大规律及温度调谐特性.结果表明:通过控制染料浓度可控制荧光输出功率水平;当温度升高时,中心波长发生红移,中心波长调谐范围为590—605 nm;荧光谱宽呈单调展宽,调制范围为228—236 nm;染料掺杂液晶填充空心光纤荧光光源可实现一定范围内的温度调谐.     

全光纤干涉式结构中传感模式仿真分析

全光纤干涉式传感结构中包层模场与外界物理量作用,携带被感测信息,因此对包层模的研究是设计制作和提高该类传感器传感性能的关键.利用有限差分光束传播法获得传感光纤不同长度和不同芯径比时传感器对应的光谱,通过傅里叶变换获得其干涉频谱,计算出各主要参与干涉的包层模组的有效折射率,利用色散方程确定对应包层模.理论仿真结果显示,随着传感部分光纤长度增加,参与干涉的包层模式随之增加,并且向高阶模式变化,光谱变得稠密,是多阶包层模干涉的叠加,传感器输出干涉谱的自由光谱范围变小.随着输入光纤与传感光纤芯径比变化,会明显改变纤芯包层功率分布,同时,芯径比增大也会增加参与干涉的包层模种类和阶数.     

The measurement of sucrose concentration by two-tapered all-fiber Mach–Zehnder interferometer employing different coupling structures and manufacture processes

The sucrose concentration measurement and characteristics of light coupling taper structure on sensitivity with various fabrication processes of taper structure for all-fiber Mach–Zehnder interferometer (AFMZI) are presented. Using fusion splicer with electrical discharge, the standard single-mode fiber is employed to be fabricated as conical coupling/decoupling taper structure. The basic two fabrication processes are designed as single fusion-stretching (SFS), multiple fusions without stretching (MF). The third advanced process is composed of SFS and multiple fusions without stretching processes, and called multiple fusions with single stretching (MFSS). Various types of coupling/decoupling taper structures were fabricated based on the three kinds of fabrication processes. The effects of geometry shape including taper waist, taper angle, and sensing length on sensing sensitivity of AFMZIs are estimated. The modifications of fiber core and cladding induced by thermal effect affect the refractive index distributions and shapes of taper structure. The effects of refractive index changes of fiber core and cladding on sensing sensitivity are also discussed. The AFMZI was tested by measuring aqueous sucrose solution of refractive index unit (RIU) from 1.333 to 1.420 RIU. The optical spectrums are measured by a spectrometer. The spectrum dip shifts and sensing sensitivity was measured and calculated, respectively. As shown in results, sensing sensitivities of AFMZIs of taper structure fabricated by MFSS and multiple fusions without stretching processing are generally higher than SFS. The reasons could be aimed on materials modification through thermal effect on blurring fiber core-cladding interface and proper taper angle of taper structure. The more homogeneous refractive index distribution on fiber core-cladding interface, the more detecting light power decoupled through core-cladding interface to interact with exterior environment and enhance the sensing sensitivity. Similarly, an appropriate taper angle also provides a better coupling/decoupling performance. The optimal sensitivities relative to low refractive index, high refractive index, and full refractive index range are 87.62, 133.55, and 104.20 nm/RIU, respectively, and the corresponding sensing length are 30, 50, and 30 mm, respectively, with taper angle of 25° and taper waist of 40 μm.