High sensitivity measurements of normal force under large amplitude oscillatory shear

The two aims of this publication are to introduce a new and rheometer-independent rheometric tool for measuring the axial normal force in oscillatory shear rheology and to study the normal forces of polyolefin melts under large amplitude oscillatory shear (LAOS). A new plate geometry with an incorporated highly sensitive piezoelectric normal force sensor was designed for a rotational rheometer. The new geometry was used to investigate normal forces of polyethylene (PE) melts under LAOS. The resulting stress and normal force data was compared with the data from measurements in commercial high performance rotational rheometers. The stress and the normal force response were Fourier-transformed and their resulting spectra were analysed. The non-linear contributions to the FT-magnitude spectra (i.e. the intensities of the higher harmonics) were analysed using the framework of the Q-parameter, \(Q=I_{3/1}/{\gamma ^{2}_{0}}\) for both the stress spectrum and the normal force spectrum, resulting in the strain-dependent \(Q\left (\gamma _{0}\right )\) and \(Q_{NF}\left (\gamma _{0}\right )\), respectively. The newly designed normal force geometry had a sensitivity in the measurement starting from \(5\times 10^{-5}\) N up to 20 N, and respectively a signal-to-noise ratio (SNR) of \(1:\) 16.000, which is about a factor of 1.8 times better than the best performing commercial rheometers. The new geometry was used to determine \(Q\left (\gamma _{0}\right )\) and \(Q_{NF}\left (\gamma _{0}\right )\), to characterize the shear rheological behaviour of the PE melts. Even rather simple rheometers, those without normal force detection, can be extended utilizing the here presented tools for high sensitive FT-rheology analysing the normal forces.     

An instrumented vehicle for offroad dynamics testing

The paper presents an instrumented vehicle that was equipped with measuring systems to perform complete dynamics tests, especially in off-road conditions. The equipment consists of four wheel dynamometers, a steering robot, and a differential GPS system together with an inertial platform, a non-contact vehicle speed sensor, and an on-board computer with software to control the devices and collect experimental data. The four wheel dynamometers measure six elements; based on strain gage force transducers, it measures three orthogonal forces and three moments. The steering robot can control the steering wheel of the vehicle at a variety of excitation modes; it can carry out typical vehicle dynamics tests (ISO 7401, ISO 4138, ISO/TR3888, etc.) as well as custom engineered tests at a wide range of setting parameters (steer angle rate up to 1600 deg/s). The differential GPS system gives true time vehicle kinematics data (velocities, accelerations, angles, etc.) at 10-ns sample rate and 20-mm accuracy. The base vehicle, a Suzuki Vitara 4 × 4, required no special modifications or changes to install the measuring equipment. The paper also describes typical tests performed with the use of the instrumented vehicle together with sample results.     

剪力公式的论证与应用

在结构力学中对梁和刚架绘制内力图时一般是先绘制弯矩图,再绘制剪力图. 根据上述特点,寻求了一种应用弯矩图绘制剪力图的数值方法,即剪力公式. 该公式主要特点是：把剪力计算的平衡问题转化为几何问题. 并且通过例题的应用,叙述了剪力公式的使用方法.适用于静定结构和超静定结构.     

Two-component hot-film probe for measurements of wall shear stress

A two-component, hot-film probe has been developed, to measure the wall shear stress as a vector quantity in time-dependent flows. The probe has been applied for the measurements of the bottom shear stress in a flow generated by combined waves and current in a water basin where the magnitude and the direction of the bottom shear stress varied periodically with respect to time. The probe has also been used to measure the bottom shear stress around a vertical cylinder exposed to water waves generated in a wave flume.     

Velocity profiles in shear force driven wall films

A wind tunnel experiment was carried out to investigate the structure, thickness and velocity profiles of a shear force driven liquid film. The local, time resolved film thickness was measured by means of a fluorescence technique, and a dedicated LDA system enabled the measurement of velocity profiles inside the thin and wavy film. The application of both techniques is briefly described.     

Effect of non-persistent joints distribution on shear behavior

The particle flow code 2D (PFC2D) is used to establish a coplanar, non-persistent joint model. Three joint distribution types, namely, both-side (type a), scattered (type b), and central (type c), are set according to their position. Numerical simulations of the direct shear test are conducted to investigate the effect of non-persistent joint distribution and connectivity on shear mechanical behavior. Simulation results are in good agreement with the analytical solutions to Jennings' criterion, and show: (1) type-c and type-b joints have high strength, whereas type-a joints have low strength. Shear strength and modulus increase with a decrease in joint persistency, and the shear displacement that correspond to shear strength increases with a decrease in persistency. (2) The brittle failure characteristics of the sample are evident when the intact rock bridge area is large. Reinforcement at both ends of the joint limits shear deformation, and shear strength can be effectively improved when joint persistency is large. The small-area dispersed reinforcement joint method cannot effectively improve shear strength. (3) The comprehensive shear strength parameters and the shear strength of the non-persistent joints can be predicted well using Jennings' criterion. Cohesion is the dominant factor that controls shear strength.     

Novel load cell for measuring axial force,shear force,and bending movement in large-scale structural experiments

This paper describes the design, construction and testing of a load cell to measure the axial force, shear force, and bending moment at the end of a structural beam. The capacities of the load cell are 780 kN in axial load, 350 kN in shear, and 200 kNm in bending. These magnitudes, together with the requirement that the load cell should be kept as slim as possible, necessitated a novel design comprising three steel double-spring elements machined with semicircular channels to provide localized strain amplification. The load cell was designed with the aid of detailed finite element analysis and was machined from grade 55 steel. After strain gaging, it was subjected to an extensive series of calibration tests. Results from these tests are reported, together with those from some early experiments in which two load cells were used to measure the behavior of structural steel knee elements.     

An engineering failure envelope for adhesive joints

An engineering failure envelope (EFE) for adhesive joints is presented and discussed. It is based on local nominal deformation parameters near the free edge of the bond where delamination may start. Tested on a double CLS specimen, this EFE exhibits an easy-to-apply failure envelope. Linear-fracture-mechanics tools show limited capability of predicting the failure load, since the singular region, especially for the interlaminar peeling stresses, is very small. Tests include simultaneous bending and stretching at different ratios in order to simulate realistic loading conditions.     

Base strain effects on force measurements

Force transducers directly interact with their environment. In this study, a force transducer is attached to the midpoint of a free-free beam and is used to measure the force on a rigid mass that vibrates with the beam. The ratio of force to mass times acceleration is measured for several different masses over a frequency range that includes the first four odd natural frequencies of the beam. Then the force transducer is mounted so that the beam's strain is isolated from the transducer. The tests are repeated. The results dramatically illustrate the effects of base strain on the force measurements. A simple theoretical model is developed that explains the vertical axis shift in the calibration curve. Paper was presented at SEM 1994 Spring Conference and Exhibits.     

Chemical analysis by force measurements in electric fields

A method is presented measuring the force acting on a sample in the inhomogeneous part of the electric field of a condensor. The possibilities for using this method in automatic chemical analysis of liquids or in liquid chromatography are discussed.     

Analytical solutions for adhesive composite joints considering large deflection and transverse shear deformation in adherends

This paper presents a novel formulation and analytical solutions for adhesively bonded composite single lap joints by taking into account the transverse shear deformation and large deflection in adherends. On the basis of geometrically nonlinear analysis for infinitesimal elements of adherends and adhesive, the equilibrium equations of adherends are formulated. By using the Timoshenko beam theory, the governing differential equations are expressed in terms of the adherend displacements and then analytically solved for the force boundary conditions prescribed at both overlap ends. The obtained solutions are applied to single lap joints, whose adherends can be isotropic adherends or composite laminates with symmetrical lay-ups. A new formula for adhesive peel stress is obtained, and it can accurately predict peel stress in the bondline. The closed-form analytical solutions are then simplified for the purpose of practical applications, and a new simple expression for the edge moment factor is developed. The numerical results predicted by the present full and simplified solutions are compared with those calculated by geometrically nonlinear finite element analysis using MSC/NASTRAN. The agreement noted validates the present novel formulation and solutions for adhesively bonded composite joints. The simplified shear and peel stresses at the overlap ends are used to derive energy release rates. The present predictions for the failure load of single lap joints are compared with those available in the literature.     

Error estimation of temperature measurements in non-isothermal shear layers

A simple analytical model has been developed to estimate the error of an invasive temperature measurement technique in a non-isothermal environment. The error depends significantly on the sensor geometry and the temperature distribution of the surrounding fluid. The problem is described in such a way that the model can easily be adapted to other sensor geometries.     

The shear gage: For reliable shear modulus measurements of composite materials

A special strain gage called the shear gage was developed for composite materials testing with notched shear specimens. The shear-gage records the average shear strain across the entire test section between the notches of the losipescu and compact shear specimens rather than just sampling the shear strain over a small region in the center of the test section. Hence, the shear stress/strain response is obtained by dividing the average shear stress (load divided by the cross-sectional area between the notches) by the average shear strain. By placing gages on both faces of the specimen, accurate and repeatable shear-modulus measurements can be made without prior knowledge of the shear strain or stress distributions. This scheme essentially integrates the shear strain through the entire test section. Knowledge of other material properties is not required to accurately determine shear modulus values. The shear gage was tested on a variety of composite and isotropic materials resulting in more reliable shear modulus determination and less scatter than previously possible.     

Lift force acting on single bubbles in linear shear flows

Lift coefficients, C_L, of single bubbles in linear shear flows are measured to investigate effects of the bubble shape, the liquid velocity gradient and the fluid property on C_L. The range of the Morton number, M, tested is from logM = − 6.6 to − 3.2. The shapes of bubbles are spherical and ellipsoidal. A correlation of bubble aspect ratio for single bubbles in infinite stagnant liquids proposed in our previous study can give good evaluations for bubbles in the linear shear flows. The C_L of spherical bubbles at low bubble Reynolds numbers, Re, depend on the dimensionless shear rate Sr and Re and decrease with increasing Re. These characteristics agree with the Legendre-Magnaudet correlation. The use of a single dimensionless group such as Re, the Eötvös number, the Weber number and the Capillary number cannot correlate C_L of non-spherical bubbles. The trend of the critical Re for the reversal of the sign of C_L is the same as that for the onset of oscillation of bubble motion, which supports the mechanism proposed by Adoua et al., at least within the range of −6.6 ≤ logM ≤ −3.2. An experimental database of C_L is provided for validation of available C_L models and CFD.     

An instrumented drive axle to measure tire tractive performance

An instrumented drive axle is introduced for a prototype tractor using in field research on tractor and implement performance. This mechanism was developed to determine whether such an instrumented drive axle is practical. The drive axle was equipped with a set of transducers to measure wheel angular velocity, rear axle torque and dynamic weight, as well as tire side forces. Measuring the drawbar pull acting on the tractor provides data for calculating net traction, motion resistance and chassis resistance for each driven wheel.     

Tire slip-angle force measurements on winter surfaces

Tire lateral force data on winter surfaces cannot be obtained with the traditional laboratory test technique of an instrumented tire on a moving belt surface. Furthermore, changing snow and ice conditions can drastically change the tire/surface interaction. In this study the Cold Regions Research and Engineering Laboratory’s (CRREL’s) Instrumented Vehicle (CIV) was used in a unique configuration to measure tire lateral force versus slip-angle data on ice and snow at various temperatures, moisture contents, depths, and densities. The vehicle is instrumented to record longitudinal, lateral, and vertical force at the tire contact patch of each wheel as well as vehicle speed, tire speed, and front tire slip angle. The tests were conducted at the Keweenaw Research Center (KRC) in northern Michigan in February 2005 and March 2006. Tests were conducted on ice, packed snow from 0.50 to 0.58 g/cc, remixed snow depths of 2.5–20.3 cm at 0.43 to 0.48 g/cc and freshly fallen snow with depths of 0.5–17 cm at 0.07 to 0.23 g/cc. Surface air temperatures during testing ranged from −14 to 1.6 °C. The data collected show that peak lateral force and the shape of the lateral force versus slip-angle curve are related to snow properties and depths.     

Dynamic stall behavior from unsteady force measurements

A direct force measurement technique employing piezoelectric load cells is used to experimentally investigate a two-dimensional airfoil (NACA 0012) undergoing dynamic stall. The load cells are installed at each end of the airfoil and give the force response in two directions in the plane normal to the airfoil axis during oscillations. Experiments are carried out at a Reynolds number based on the airfoil chord equal to 7.7×10⁴, and at four reduced frequencies, k=0.005, 0.01, 0.02, and 0.04. Phase-averaged lift of the airfoil undergoing dynamic stall is presented. It is observed that hysteresis loops of the lift occur both when the airfoil is pitched to exceed its static stall limit and when it is still within its static stall limit, and they grow in size with increasing k at the same pitching mean angle of attack and pitching amplitude. Both the lift and the drag induced by the pitching motion are further analyzed using the methods of higher order correlation analysis and continuous wavelet transforms to undercover their nonlinear and nonstationary features, in addition to classical FFT-based spectral analysis. The results are quantitatively illustrated by an energy partition analysis. It is found that the unsteady lift and drag show opposite trends when the airfoil undergoes transition from the pre-stall regime to the full-stall regime. The degree of nonlinearity of the lift increases, and the lift show a nonstationary feature in the light-stall regime, while the nonlinearity of the drag decreases, and the drag shows nonstationary feature in both the light-stall and the full-stall regimes. Furthermore, the lift and the drag have significant nonlinear interactions as shown by the correlation analysis in the light-stall regime.     

Relations between steady flow and oscillatory shear measurements

Summary Results are given of a comparison between dynamic oscillatory and steady shear flow measurements with some polymer melts. Comparison of the steady shear flow viscosity,, with the absolute value of the dynamic viscosity, ¦¦, at equal values of the shear rate,q, and the circular frequency,, has shown the relation thatCox andHerz had found empirically to be substantially correct.Further, the coefficients of the normal stress differences obtained by streaming birefringence techniques have been compared with 2G () · ^{– 2} in the same range of shear rates as covered by the viscosity measurements (G is the real part of the dynamic shear modulus). Two polystyrenes with narrow molecular weight distribution showed the same shift factor along the orq axis for the normal stress coefficients with respect to 2G () · ^{– 2} and the steady shear flow viscosities with respect to the real part of the dynamic viscosity,. For two polyethylenes the results are not so conclusive owing to the smallness of the shift factor found. An empirical equation is proposed predicting the main normal stress difference from dynamic measurements only.

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Zusammenfassung Die Ergebnisse von Messungen unter erzwungenen Schwingungen und stationärer Scherströmung an einigen Polymerschmelzen werden miteinander verglichen. Der Vergleich der stationären Viskosität mit der absoluten dynamischen Viskosität ¦¦ bei gleichen Werten des Strömungsgradientenq und der Kreisfrequenz zeigt die Gültigkeit der empirischen Beziehung vonCox undHerz.Weiter wurden die Koeffizienten der Normalspannungsdifferenzen, welche durch Messung der Strömungsdoppelbrechung erhalten wurden, mit 2G() · ^–2 verglichen, und zwar wiederum bei gleichen Werten vonq und, wobeiG die Speicherkomponente des dynamischen Schubmoduls ist. Zwei Polystyrole mit enger Molekulargewichtsverteilung zeigen die gleiche Verschiebung entlang der-oderq-Achse für die Normalspannungskoeffizienten in bezug auf2G()· ^–2 und für die stationären Scherviskositäten in bezug auf den Realteil der dynamischen Viskosität. Für zwei Polyäthylene sind die Ergebnisse weniger signifikant, da die entsprechenden Verschiebungen zu klein waren. Eine empirische Beziehung zwischen den Hauptnormalspannungsdifferenzen und den dynamischen Meßwerten wird vorgeschlagen.

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Paper presented at the British Society of Rheology Conference, held at Shrivenham, from 9th–12th September, 1968.