Observation of the substructure of weakly deformed polycrystalline nickel

The paper describes the results of observing the substructure and measuring the subgrain size of polycrystalline nickel of purity 99·80% for a tensile deformation of 0·5–10%. It was found that a rapid decrease in the average grain size occurs already at small degrees of deformation. The deformation at which subgrains begin to form is identical with the critical deformation of recrystallization and in the case of nickel of the above purity it is 2% of the elongation. From 5% there are dislocations even inside the subgrains and in some places dense clusters are formed.     

Microstrain in dispersion-hardened steels

Using high-resolution neutron diffraction, microstrain was investigated in three series of samples of stainless austenitic dispersion-hardened steels, which are used as various structural reactor components. The effect of temperature and duration of heat treatment on the precipitation of dispersion-hardened phase particles, as well as on lattice parameter changes and microstrain, was studied. An increase in microstrain upon coherence failure was observed in all the steels.     

Features of plasma plume evolution and material removal efficiency during femtosecond laser ablation of nickel in high vacuum

We present an experimental characterization describing the characteristics features of the plasma plume dynamics and material removal efficiency during ultrashort, visible (527 nm, ≈300 fs) laser ablation of nickel in high vacuum. The spatio-temporal structure and expansion dynamics of the laser ablation plasma plume are investigated by using both time-gated fast imaging and optical emission spectroscopy. The spatio-temporal evolution of the ablation plume exhibits a layered structure which changes with the laser pulse fluence F. At low laser fluences (F<0.5 J/cm²) the plume consists of two main populations: fast Ni atoms and slower Ni nanoparticles, with average velocities of ≈10⁴ m/s for the atomic state and ≈10² m/s for the condensed state. At larger fluences (F>0.5 J/cm²), a third component of much faster atoms is observed to precede the main atomic plume component. These atoms can be ascribed to the recombination of faster ions with electrons in the early stages of the plume evolution. A particularly interesting feature of our analysis is that the study of the ablation efficiency as a function of the laser fluence indicates the existence of an optimal fluence range (a maximum) for nanoparticles generation, and an increase of atomization at larger fluences. PACS 52.50.-b; 52.38.Mf; 79.20.Ds; 81.07.-b     

Modeling of temperature and rate dependence of the flow stress and evolution of a deformation defect medium in dispersion-hardened materials

The influence of characteristics of the second phase, strain rate and temperature, and initial defect state of a material on the curves of deformation hardening and the kinetics of components of the defect sub-system is investigated using a mathematical model of the plastic deformation for dispersion-hardened materials with an incoherent hardening phase.     

Variations in defect substructure and fracture surface of commercially pure aluminum under creep in weak magnetic field

Commercially pure polycrystalline aluminum of grade A85, as a test material, is investigated. Using scanning and transmission electron microscopy the aluminum fine structure and fracture surface are analyzed. Fractures are studied in the regime of creep with and without a simultaneous effect of 0.3-T magnetic field. It is found that the application of a magnetic field in a linear stage of creep leads to substructure imperfection increasing. Furthermore, the magnetic field effect on aluminum in the process of creep causes the average scalar density of dislocations to increase and induces the process of dislocation loop formation to strengthen. Fractographic investigation of the fracture surface shows that in the fibrous fracture zone the average size of plastic fracture pits decreases more than twice under creep in the condition of external magnetic field compared with in the conventional experimental condition. In a shear zone, the magnetic field causes the average size of fracture pits to decrease. Experimental data obtained in the research allow us to conclude that the magnetic field effect on aluminum in the process of creep leads to the fracture toughness value of the material decreasing, which will affect the state of defect substructure of the volume and surface layer of the material. The influence of the magnetic field is analyzed on the basis of the magneto-plasticity effect.     

Influence of the temperature and strain rate on the evolution of the dislocation structure of a dispersion-hardened material with FCC matrix

A mathematical model of plastic strain in monocrystals of dispersion-hardened FCC materials with nanosize particles of the second phase is used to investigate the influence of the temperature and strain rate on the behavior of the material and evolution of its dislocation subsystem. It is established that the curves of the temperature dependence of work hardening and density of various dislocation subsystem components for materials with different (aluminum, copper, and nickel) matrices differ insignificantly.     

Effects of grain boundary diffusion of copper on nickel creep

We have investigated the effects of surface copper diffusion on the creep of large-grain nickel (average grain size about 20 m) and submicron crystalline nickel (grain size about 0.3 m). For both structural states of nickel we find an acceleration of creep over its value in vacuum, and an increase in plasticity during creep when copper has diffused deeply into the nickel from the surface. The temperature range over which these effects are observed in the submicron nickel is nearly 300° lower than that for the large-grain samples. This result is probably due to a significant increase in the grain-boundary and bulk diffusion coefficients of copper in submicron nickel when compared with large-grain nickel.Siberian Branch. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 12, pp. 83–86, December, 1994.     

High-temperature creep of nickel under conditions of grain-boundary diffusion of impurities from the surface

Comparative investigations of the effect of diffusion streams of copper atoms (a weakly segregating impurity) and silver atoms (a strongly segregating impurity) from the surface in the high-temperature plastic deformation of nickel have been carried out. It has been established that in the high-temperature plastic deformation of nickel, when there are diffusion streams of copper and silver from the surface, there is a reduction in the creep resistance of nickel due to an increase in the contribution of grain-boundary slip to the overall deformation. Two stages, characterized by different values of the rate sensitivity factor m, are observed on the curve of the stress against the rate of deformation over a certain temperature range for each impurity. In the region of deformation rates of sec⁻¹, m≊0.2, and for sec⁻¹, m becomes less than 0.05. Institute of Physics of the Strength and Study of Materials. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 7, pp. 119–125, July, 1997.     

Microstructural evolution of nickel under high-pressure torsion

The evolution peculiarities of grain and defect structures in nickel under high-pressure torsion were studied by transmission electron microscopy and X-ray diffraction analysis. Lattice reorientation mechanisms characteristic of different stages of plastic deformation were disclosed. The conditions and features of cooperative realization of various structure formation mechanisms under severe deformation were discussed.     

Laws of the deformation and failure of molybdenum in creep with grain-boundary activation by diffusional nickel fluxes

The diffusion of nickel from the surface of polycrystalline molybdenum influences the crack formation and plastic deformation in creep. Investigation shows that diffusional fluxes of nickel from the surface reduce the critical deformation at which the first cracks appear in molybdenum. The contribution of grain-boundary slip to the deformation of molybdenum in creep is considerably increased in the presence of nickel diffusion from the surface as a result of easier crack formation and grain-boundary activation.Institute of Strength Physics and Materials Science, Siberian Branch, Russian Academy of Sciences. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 7, pp. 16–21, July, 1992.     

Variation of apparent creep activation energy in plastic deformation of molybdenum in diffusion contact with nickel

The variation of the apparent creep activation energy as a function of the state of grain boundaries is investigated in the deformation of molybdenum in the presence of diffusion fluxes of nickel at the grain boundaries. It is shown that this energy varies in the same way as in the plastic deformation of classical superplastic materials.Physics Institute of Strength and Materials Science, Siberian Branch, Russian Academy of Sciences. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 5, pp. 110–113, May, 1993.     

Phase composition and defect substructure of nickel alloyed with boron and copper by electric explosion of conductors

Using methods of electron microscopy, we have discovered that combined electroexplosive alloying of nickel with boron and copper gives rise to a multilayer structure. An outer amorphous crystalline layer incorporating 2–3 nm nickel-and copper-boride, oxide, and boride-oxide crystallites is formed on the alloyed surface. The intermediate (subsurface) layer 1–2 μm thick is made up of NiB ₁₂ and Ni ₄ B ₃ crystallites 120–130 nm in size, with boron-and copper-oxide particles observed along the grain boundaries. The underlying thick layer exhibits a cellular Ni-Cu-B melt crystallization structure grading initially into a high-rate dendritic crystallization structure and then into a granular structure. The electroexplosive alloying process is found to bring into existence a high scalar dislocation-density substructure in nickel crystallites both in the alloyed zone and in the adjacent heat-affected zone. __________ Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 3, pp. 3–7, March 2007.     

Spin substructure of space-time

In a spin space, with noncommutative spinorial coordinatesC ^A which satisfyx ^AB =1/2{C ^A ,C ^*B }, we investigatex-dependent spin coordinate transformations which correspond to a local fermi-bose symmetry. A concept of a spin vector corresponding to these local transformations is established, and spin space is provided with a spinorial vierbein field which determines non-nil-potent line and volume elements which are direct generalizations of the conventional relativistic ones.