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1.
Three new glycosides, 6'-O-alpha-D-galactopyranosylsyringopicroside (1), secologanoside 7-methyl ester (2) and (+)-lariciresinol 4'-O-beta-D-glucopyranosyl-(1-->3)-beta-D-glucopyranoside (3), were isolated from the leaves of Syringa reticulata. Their structures were established on the basis of chemical and spectral data. Compound 1 is the first naturally occurring iridoid di-glycoside having melibiose. Comparison of the spectral data of 2 and that previously recognized as secologanoside 7-methyl ester led to the conclusion that the recognized structure should be revised to the sodium salt of secoxyloganin (2'). 相似文献
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Machida K Kaneko A Hosogai T Kakuda R Yaoita Y Kikuchi M 《Chemical & pharmaceutical bulletin》2002,50(4):493-497
Five new iridoid glycosides, (8Z)-ligstroside (1), (8Z)-nüzhenide (3), 6'-O-alpha-D-glucopyranosylsyringopicroside (4), 3'-O-beta-D-glucopyranosylsyringopicroside (5) and 4'-O-beta-D-glucopyranosylsyringopicroside (6) were isolated, together with a known one, (8E)-nüzhenide (2), from the leaves of Syringa reticulata. Their structures were established on the basis of chemical and spectral data. Compounds 1 and 3 are the first findings of a (8Z)-oleoside-type secoiridoid. Compound 4 is the first naturally occurring iridoid di-glycoside having an isomaltose. 相似文献
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Two lignans have been isolated from the bark ofSyringa vulgaris and identified: (+)-lariciresinol 4-β-D-glucopyranoside (I) and -olivil 4-β-D-glucopyranoside (II). This is the first time
that glycoside (9) has been described.
All-Union Scientific-Research Institute of Medicinal Plants Scientific-Production Association, Moscow. Translated from Khimiya
Prirodnykh Soedinenii, No. 6, pp. 768–771, November–December, 1991. 相似文献
4.
Two new neolignans, syripinnalignins A and B ( 1 and 2 , resp.), were isolated from the 95% EtOH extract of the stem of Syringa pinnatifolia Hemsl . var. alashanensis. The structures of 1 and 2 were elucidated by spectroscopic methods, including UV, IR, HR‐ESI‐MS, and extensive 1D‐ and 2D‐NMR techniques. 相似文献
5.
All-Union Scientific-Research Institute of Medicinal Plants, Scientific Production Combine, Moscow. Translated from Khimiya
Prirodnykh Soedinenii, No. 5, pp. 695–697, September–October, 1990. 相似文献
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Two lignans have been isolated from the bark ofSyringa vulgaris and identified: (+)-lariciresinol 4--D-glucopyranoside (I) and -olivil 4--D-glucopyranoside (II). This is the first time that glycoside (9) has been described.All-Union Scientific-Research Institute of Medicinal Plants Scientific-Production Association, Moscow. Translated from Khimiya Prirodnykh Soedinenii, No. 6, pp. 768–771, November–December, 1991. 相似文献
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Kurkin V. A. Evstratova R. I. Zapesochnaya G. G. Pimenova M. E. 《Chemistry of Natural Compounds》1992,28(5):511-512
Chemistry of Natural Compounds - 相似文献
12.
Studies on constituents with cytotoxic activity from the stem bark of Syringa velutina. 总被引:5,自引:0,他引:5
H J Park M S Lee K T Lee I C Sohn Y N Han K Miyamoto 《Chemical & pharmaceutical bulletin》1999,47(7):1029-1031
Cytotoxic compounds, oleuropein (1) and a phenylethanoid glycoside (2) were isolated from the stem bark of Syringa velutina KOM. along with coniferylaldehyde 4-O-glucoside, syringin, ligstroside, (+)-syringaresinol 4-O-glucoside, (+)-medioresinol 4"-O-glucoside and (-)-olivil 4"-O-glucoside. Phenylethanoid glycoside (2) was identified to be 3,4-dihydroxyphenylethyl alcohol 8-O-beta-D-glucopyranoside. This compound showed the most potent cytotoxic effect on several tumor cell lines (P-388, L-1210, SNU-5 and HL-60) among eight compounds isolated in the present study. We suggest that the 3,4-dihydroxyphenylethoxy moiety of this compound contributes to cytotoxicity. 相似文献
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Feng Zhao Ruifei Zhang Hexinge Zhang Shungang Jiao Alagnidun Alagnidun Suyile Chen 《Natural product research》2019,33(19):2809-2814
Two humulane-type sesquiterpenoids, namely (+)-alashanoid I (1a) and (–)-alashanoid I (1b), were isolated as a pair of enantiomers from the peeled stems of Syringa pinnatifolia. Their structures were elucidated by extensive spectroscopic data (1?D and 2?D NMR, UV, and IR), and the absolute configurations were resolved by X-ray diffraction and experimental and calculated ECD data analysis. 相似文献
15.
V. A. Kurkin N. A. Grinenko G. G. Zapesochnaya A. G. Dubichev E. D. Vorontsov 《Chemistry of Natural Compounds》1992,28(1):36-39
Using HPLC, the component composition of the bark ofSyringa vulgaris has been studied and a procedure has been developed for the quantitative determination of syringin in raw material from this plant. The seasonal dynamics of the accumulation of syringin in the bark of common lilac has been studied with the aid of a chromatospectrophotometric method and HPLC analysis.All-Union Scientific-Research Institute of Medicinal Plants Scientific-Production Combine, Moscow. Translated from Khimiya Prirodnykh Soedinenii, No. 1, pp. 45–49, January–February, 1992. 相似文献
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A new lignan, 4,4′-dihydroxy-3,3′-dimethoxy-6,9′-cycloligna-7,8′-dien-9′-al, was isolated from the stem of Syringa pinnatifolia Hems1. var. alashanensis MA. et S.Q. Zhou (S. pinnatifolia). This is the first report on the structure elucidation of a new compound based on spectroscopic methods including UV, IR, ESI-MS, 1D NMR and 2D NMR techniques. 相似文献
17.
Xue Song Feng Yang Qua Zhao Hua Wuc Lei Xua Dong Song Zhanga Hui Yuan Gaoa Li Jun Wu a School of Traditional Chinese Medicines Shenyang Pharmaceutical University Shenyang China b School of Pharmaceutical Sciences China Medical University Shenyang China c Pharmacy Department Mudanjiang Medical University Mudanjiang China 《中国化学快报》2009,20(6)
Chemical investigation of Syringa velutina Kom. led to the isolation of two new secoiridoid glucosides. Their structures were identified as 6'-0-(6, 7-dihyrofoliamenthoyl)-8-epi-kingisidic acid (syrveoside A, 1) and 6'-O-menthiafoloyl-8-epi-kingisidic acid (syrveoside B, 2) on the basis of chemical and physicochemical evidence. 相似文献
18.
Erzsébet Varga Csenge Barabás Anita Tóth Imre Boldizsár Béla Noszál 《Natural product research》2019,33(11):1664-1669
Metabolite profile, antioxidant and antinociceptive activities of Syringa vulgaris bark and leaf methanolic extracts were investigated. By means of HPLC-DAD-ESI-TOF and HPLC-DAD-ESI-MS/MS, a total of 33 phenolics were identified, including 15 secoiridoids, 6 phenylpropanoids, 3 flavonoids, 3 lignans and 6 low molecular weight phenols. Validated quantitative analysis show that syringin (2.52%) and rutin (1.13%) are the main phenolic compounds in bark and leaf, respectively. Notable radical scavenging and antinociceptive activities of the bark and leaf extracts were confirmed by in vitro DPPH● and ABTS●+ assays and by in vivo hot-plate method in mice, respectively. Our results could lay the scientific basic of future clinical perspectives of lilac bark and leaf. 相似文献
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Daniela Hanganu Mihaela Niculae Irina Ielciu Neli-Kinga Olah Melania Munteanu Ramona Burtescu Rzvan tefan Loredana Olar Emoke Pall Sanda Andrei Dan C. Vodnar Daniela Benedec Ilioara Oniga 《Molecules (Basel, Switzerland)》2021,26(11)
Syringa vulgaris L. (common lilac) is one of the most popular ornamental species, but also a promising not comprehensively studied source of bioactive compounds with important therapeutic potential. Our study was designed to characterize the chemical composition and to assess the antioxidant and cytotoxic properties of ethanolic extracts obtained from S. vulgaris L. flowers, leaves, bark, and fruit. The chemical profile of the ethanolic extracts was investigated using chromatographic (HPLC-DAD-ESI+, GC-MS) and spectral (UV-Vis, FT-IR) methods, while the protective effect against free radicals was evaluated in vitro by different chemical assays (DPPH, FRAP, CUPRAC). The cytotoxic activity was tested on two tumoral cell lines, HeLa, B16F10, using the MTT assay. Significant amounts of free or glycosylated chemical components belonging to various therapeutically important structural classes, such as phenyl-propanoids (syringin, acteoside, echinacoside), flavonoids (quercetin, kaempferol derivatives) and secoiridoids (secologanoside, oleuropein, 10-hydroxy oleuropein, demethyloleuropein, syringalactone A, nuzhenide, lingstroside) were obtained for the flowers, leaves and bark extracts, respectively. Furthermore, MTT tests pointed out a significant cytotoxic potential expressed in a non-dose-dependent manner toward the tumoral lines. The performed methods underlined that S. vulgaris extracts, in particular belonging to flowers and leaves, represent valuable sources of compounds with antioxidant and antitumoral potential. 相似文献