准傅里叶彩色全息图在显微术中的应用

光学显微镜与其他光学系统比较起来其景深特别短,且放大倍数越高,数值孔径越大,景深越短.计算表明(考虑到人眼的调节深度),放大倍数为100倍时,其景深为48μm,而放大500倍时,景深仅有28μm.因此,如果能提高显微镜的观察深度,无疑是有价值的.另一方面,在显微镜下观察的标本必须染色,这样,任何村本的自然色通过染色以后都不复存在.当切片染色以后,活的组织都将死亡.因此,如果可以再现一个自然色的标本.并用普通光学显微镜观察,则可获得较大的景深,从而扩大了光学显微镜的观察范围.利用全息的共轭再现实象,通过显微镜进行逐层调焦,是提高显微镜…     

超细Ni80Cr20合金丝的冷拉拔制备及表征

开展特定直径超细Ni80Cr20合金丝的冷拉拔制备研究,并通过扫描电子显微镜(SEM)、X射线衍射仪(XRD)和金属丝强力仪等对超细合金丝进行了表征。研究结果表明:烧头过程最佳电解液浓度为0.05mol/L,时间为3s;制备的镍铬合金丝直径为24.54μm,表面光滑,尺寸精准;拉拔后晶粒尺寸减小,退火后晶粒尺寸长大;拉拔态镍铬丝由于加工硬化,其伸长率由16%降低至1.88%;退火可改善镍铬丝性能,其断裂强度降低,伸长率增大,合金塑性增强,氮气退火丝的断裂强度大于真空退火丝的断裂强度,伸长率则相反。     

高峰值功率大模场全光纤脉冲放大器

报道了一种由纤芯直径分别为15μm和25μm的大模场光纤组成的全光纤脉冲放大器模块.当注入脉冲宽度为10 ns,重复频率为1 Hz.光谱宽度为0.3 nm,脉冲能量为80 nJ的激光脉冲时,经过两级放大输出的激光脉冲峰值功率为30 kW,单脉冲能量为300μJ.此外,实验研究了该放大器模块输出的时间特性.研究发现:由于受激布里渊散射(SBS)效应,限制了单纵模光纤激光在光纤中的高能量放大,采用宽带激光脉冲可以有效地抑制SBS效应,提高光纤放大器的SBS阈值.     

扩芯光纤原理及其在光器件耦合中的应用

介绍了两种可以增大单模光纤模场直径并出射准直平行光束的扩芯光纤(ECF)的原理和制作方法。分析了单模光纤熔接渐变折射率多模光纤法通过改变渐变折射率多模光纤的长度和自聚焦参量实现模场扩大缩小的原理,制作的扩芯光纤模场直径扩大到16．6μm,出射光束平行效果较好,轴向耦合容限比单模光纤扩大了近6倍。加热扩芯光纤则是通过控制加热温度和加热时间直接使单模光纤掺杂物质发生扩散,从而实现扩束和光束准直,模场直径达到15．4μm,横向、轴向耦合容限都比单模光纤有很大提高。因此扩芯光纤可以简化单模光纤的耦合对准过程,用来制作新型的单模光纤或掺铒光纤连接器,也可以用于其它光器件中与单模光纤的准直。     

双层孔大模场微结构光纤的模式特性分析

本文分析一种由两层低折射率孔组成的大模场光纤的模式特性,采用多极法和有限元方法数值计算并分析了内层孔与外层孔尺寸变化对光纤基模与高阶模的束缚损耗与弯曲损耗的影响,设计获得了一种具有较高的高阶模和基模损耗比同时允许一定程度弯曲的大模场光纤,结果表明:当内层孔直径为34μm,外层孔直径为24 μm时,其基模束缚损耗为0.00017 dB m,而高阶模束缚损耗为1.39 dB/m;光纤的基模模场面积为2450.9μm2,当弯曲半径为1.2m 时,弯曲损耗为0.106 dB/m.     

包层空气孔渐变的准光子晶体光纤的色散特性研究

设计了一种准光子晶体光纤,其包层由呈准周期分布的空气孔构成,其中靠近芯区的空气孔的直径是渐变的.采用带有良匹配层(APML)吸收边界的全矢量频域有限差分(FDFD)方法对其色散特性进行了数值分析,计算了孔间距取1.5μm～2.2μm,最小空气孔直径分别取0.4μm～0.6μm,从第一层到第三层直径线性递增量分别为0.1μm和0.2μm的条件下,这种光纤基模的色散曲线.结果表明:通过调节包层中三种不同尺寸的空气孔的大小以及孔间距这四个参数,可以得到不同平坦水平的色散曲线,甚至于超低超平坦的色散曲线.例如,当孔间距取1.7μm,空气孔直径分别取0.5μm、0.7μm、0.9μm,在1.4μm～1.7～m波段内,这种光纤的色散值可以控制在6.0±3.0 ps/km.nm范围内.     

单频脉冲光纤放大器中受激布里渊散射实验研究

从实验上研究了掺镱(Yb)双包层光纤放大器中单频脉冲信号放大时,受激布里渊散射(SBS)引起的脉冲畸变现象。实验中采用的单频双包层光纤放大器光纤长度14m,内包层直径130μm,纤芯模场直径6.5μm,在单频脉宽200 ns脉冲放大,且峰值功率3.3 W时观察到后向SBS脉冲,脉宽明显小于输入信号脉宽,分析了受激布里渊散射引起放大脉冲波形畸变的随机特性和功率特性,并采用自由光谱范围30 GHz的法布里-珀罗(F-P)扫描干涉仪验证了SBS频移。     

大模场Er3+/Yb3+共掺锥形微结构光纤1.5μm激光特性

采用全矢量有限元法设计了一种大模场双包层微结构光纤及锥形波导结构.采用复丝拉制方法制备了成分为45Bi2 O3-29GeO2-15Ga2 O3-10Na2 O-1CeO2的大模场双包层微结构光纤,纤芯直径为70μm,内包层的占空比为0.25,模场面积约为3014.8μm2.采用熔融拉锥技术制备了纤芯直径为17.5μm、...     

Tl-2212本征约瑟夫森结型负阻器件及负阻放大器

我们利用Tl—2212超导薄膜制作出了的本征约瑟夫森结型负阻器件．对于4μm长3μm宽的微桥型负阻器件，峰值电压为0．09V，峰值电流为1．44mA．谷值电压为0．75V，谷值电流为1．05mA，线性区间内负阻阻值约为-1400Ω利用这种器件．制作了简单的负阻并联式电流放大器．实验证明它确实对信号具有电流放大作用，放大倍数可以通过改变负载电阻的大小来改变．     

有限包层半径光纤Bragg光栅的理论研究

采用光纤波导三层模型,对有限包层半径光纤Bragg光栅导模有效折射率的改变进行了理论分析,结果表明:当包层直径小于16μm时,单模光纤Bragg光栅(纤芯直径为8.3μm)的导模有效折射率才开始发生明显变化.在包层外添加外包层,通过改变外包层的折射率可以实现对光栅Bragg反射波长的调谐,同时对不同芯子直径的光栅Bragg波长移动进行了数值计算.在保证光纤归一化频率不变的前提下,芯径越小Bragg波长调谐范围越大,当包层厚度为1μm时,芯径为a＝2.2μm的光栅Bragg波长调谐范围约为3.9μm.     

冷拉拔超细Ni80Cr20合金丝卷曲因素分析

Ni80Cr20超细丝经冷加工后呈规则的三维螺旋卷曲状态。实验研究了拉拔角度、变形量、拉拔速度和模具定径区长度对超细丝材曲率的影响，制定了NiCr合金丝单模冷拉拔工艺。结果表明:随拉拔角度的增加，丝材曲率逐渐增加；变形量增加，拉拔角度为17时，丝材曲率没有明显规律，基本在0.56 mm-1左右，但拉拔角度为0时，丝材曲率逐渐增加；拉拔速度小于10 mmin-1时，曲率逐渐增加，大于10 mmin-1时，曲率增加趋势变缓，大于30 mmin-1曲率又有所下降；定径区长度越长丝材曲率越小。分析认为，NiCr丝材表面产生的附加切变形及切变层的流动速度的不一致性是丝材产生卷曲的原因，且曲率越大残余应力越大。为减小不均匀变形，冷拉拔工艺采用0拉拔、拉拔速度10 mmin-1、模具定径区长度为模具定径区直径的60%。     

Measurements of bulk-to-surface segregation of impurities in electrodeposited NiCr alloys by auger electron spectroscopy

Auger Electron Spectroscopy (AES) measurements of the non-equilibrium segregation of K to the surface of an electrodeposited NiCr alloy of 20%Ni-80%Cr composition are reported. It is shown that a surface enrichment of K takes place on the surface to a maximum of 8% coverage in the temperature range 400–550°C. The process is initially diffusion-connrolled, with an activation energy of 17 ± 3 kJ/mol. An electrodeposited alloy of approximately 80%Ni-20%Cr composition showed a considerable C-enrichment at the surface in the temperature range 300 to 600°C. A cast alloy of the same composition showed a similar C-enrichment in the temperature range 300 to 455°C. The electrodeposited alloy of 20%Ni-80%Cr showed no such C-enrichment, due to the segregation of both K and Cr to the surface in the range 300 to 600°C and the formation of chromium carbide precipitates.     

SiC在高温高压下溶于金属触媒中形成金刚石的原子过程

从原子间相互作用及运动出发，阐明ＳｉＣ在高温高压下溶于金属触媒中形成金刚石的原子过程，并在此基础上进而阐明Ｎｉ７０Ｍｎ２５Ｃｏ５是促使ＳｉＣ形成金刚石的高效率触媒合金。日本文部省的资助     

纳米团聚生长的多重分形谱

采用小角x射线散射（SAXS）方法，对两类具有代表性的纳米团聚的生长分形进行了表征.一 类为用化学方法 (水合肼溶液还原法) 制备的纳米金属Ni粉；另一类通过物理方法(纳米晶 化处理)，由非晶基体相中生长纳米晶相、形成非晶/纳米晶双相结构的Finemet (Fe_{73 .5} Cu₁Nb₃Si_13.5B₉) 合金.上述两 类材料的纳米团聚在生长过程中都存在 明显元素扩散迁移，形成在1—100 nm范围内的元素分布非均匀区域.这些元素分布的非均匀 区域具有多重质量生长分形特征，其尺度大小和分布方式对最终的材料的物理性能至关重要 .SAXS方法是表征这类具有分形生长特征的纳米团聚微观结构信息的强有力手段.从方法论的 角度详述了从SAXS测量到获得多重分形谱的处理过程，这一实验研究分析手段对于定量考察 纳米微结构形貌的生长机理和性能的其他研究课题有一定的帮助作用. 关键词： 纳米材料 分形生长 小角x射线散射 磁性材料     

Synergetic effects of impurities and alloying element Cr on oxidation and dissolution corrosion of Ni (111) surfaces: A DFT study

Using density-functional calculations, we studied the interactions between interstitial impurities (H, O, N, S, and P) and Ni (111) surfaces doped, or not, with Cr, and studied the effect of Cr doping on the dissolution corrosion resistance of Ni(111) surfaces. The aim of this work was to study, at the atomic scale, the effects of Cr on the segregation behaviors of impurities and the synergetic effects between co-doped atoms on the resistance to dissolution corrosion of Ni (111) surfaces. The results indicate that impurities S, P, O, and H prefer to be trapped at near-surface sites, that Cr was uniformly distributed in the Ni crystal and can affect the segregation behavior of impurities S and P to move toward the surface, and it affects impurities N and O such that they shift from the surface to the subsurface. The formation of near-surface Cr nitrides (speculated to be Cr₂N based on the results obtained for particular co-doped surfaces) was also noted. Introducing Cr enhances the structural stability of the Ni (111) surface and protects it from being corroded when impurities are present. The elementary processes studied afforded microscopic insights into the formation of a Cr-depleted zone, a phenomenon that leads to local corrosion of the Ni alloy surface. The results of our theoretical calculations explain some of the experimental results previously observed at the atomic scale.     

Study of the microstructure influence on the transport properties of Bi86.5Sb13.5 polycrystalline alloy

This study is focused on the investigation of the transport properties of Bi_86.5Sb_13.5 polycrystalline alloys. Bulk materials were prepared by cold pressing ultrafine powders of alloy and by annealing the resulting pellets. Special care was taken to avoid contamination of the powders. Starting with powders of average grain size of 0.06 μm bulk semi-conducting sample with mean grain size respectively of 0.1, 0.8, 2.5 and 200 μm were obtained. The influence of the grain size on both electrical resistivity, thermal conductivity, thermoelectric power, thermoelectric figure of merit is presented within the range 80-330 K. The thermoelectric properties are discussed and compared with those of single crystals presented in previous studies.     

One way of surface alloying treatment on iron surface based on surface mechanical attrition treatment and heat treatment

A method of surface alloying treatment has been developed: Ni powders were welded into the surface of iron plates by Surface Mechanical Attrition Treatment (SMAT), followed by annealing at certain temperature for 30 min. A Ni-Fe alloy layer with thickness about 100 μm in the sample surface was fabricated on pure iron plate. Scanning electron microscope (SEM), glow discharge spectrum (GDS), and X-ray diffraction (XRD) methods were used to analyze the microstructure, the composition and the phases of the alloy layer. Studies on the interface microstructure indicated that there was significant atomic diffusion and formation of multilayer of intermetallic compound and solid solution in SMAT process. Subsequent annealing accelerates the alloying process. The corrosion test shows the sample by SMAT treated with Ni powders exhibit the best corrosion resistance.     

Electrochemical corrosion and oxidation resistances of Zr_(60)Ni_(21)Al_(19) bulk amorphous alloys

Electrochemical corrosion and oxidation resistances of Zr 60 Ni 21 Al 19 amorphous alloy were studied. The ternary amorphous alloy exhibits greater positive potential than its crystalline counterpart and 0Cr19Ni9Ti stainless steel. Its weight loss result measured in 2 mol/L HCl solution is in agreement with the potentiodynamic curve. But there is no obvious difference in the oxidation resistances between Zr 60 Ni 21 Al 19 amorphous and its crystalline alloys. They both exhibit high oxidation resistance.     

铜镍合金丝电爆炸放电特性与时空演化行为

脉冲电流驱动金属丝电爆炸可产生具有较高能量密度的等离子体,并伴随脉冲电磁辐射、强冲击波等效应,广泛应用于Z箍缩、电热化学武器、油气助采等领域;与纯金属相比,合金具备电阻率高、成分可调、相变复杂等特点,在电爆炸效应参数的调控方面具有很大潜力。开展了大气空气介质中铜、镍、铜镍（康铜）丝在微秒时间尺度电脉冲作用下电爆炸实验研究,通过放电参数与自辐射图像诊断,获取电爆炸过程放电参数与时空演变的特性规律,得到脉冲电流作用下合金电爆炸在相变与等离子体方面的特征。实验发现,在电爆炸早期,铜镍合金的高电阻率能够提高能量沉积效率:铜52%、镍74%、铜镍合金78%;而相爆开始后,合金丝负载则更接近纯镍丝负载性能。等离子体通道早期膨胀速率在5 mm/μs量级,随后迅速衰减;合金丝等离子体膨胀时间更久,击穿后平均电阻率上升缓慢,且等离子体辐射与金属爆炸产物在空间尺度上存在关联性。特别地,铜镍合金气溶胶分层同时具有横向和纵向特征（特征尺度10?1 mm）,但整体较铜气溶胶更为均匀。