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1.
分光光度法测定荞麦中芦丁含量   总被引:10,自引:1,他引:10  
建立一种简单、准确测定荞麦中芦丁含量的分光光度法,讨论最佳试验条件及试剂用量,反应产物在500nm有相对稳定吸收峰,该法灵敏、可靠(ε=7.5×10 ̄4L/mol·cm)。回收率96.40%─105.50%,相对标准偏差小于1.42%。  相似文献   

2.
分光光度法测定银杏中有机锗   总被引:4,自引:0,他引:4  
本文用分光光度法测定银杏中的有机锗含量。结果表明,灰化法操作简单、准确,方法回收率为99.24%-100.26%,结果满意。  相似文献   

3.
阿莫西林-铜络合物光度法测定阿莫西林   总被引:10,自引:0,他引:10  
赵丽瑞 《光谱实验室》1999,16(2):189-190
本文提出了一种简便,快速,准确测定阿莫西林含量的方法,在Na2CO3介质中,阿莫西林与铜离子形成络合物,于334nm处产生最大吸收,测定阿莫西林的线性范围为2-50g.mL^-1本方法用于阿莫西林原料样品的测定结果满意。  相似文献   

4.
DSPCF分光光度法测定水中微量铜   总被引:7,自引:1,他引:6  
在醋酸-醋酸钠介质中,铜与DSPCF形成稳定的紫红色配合的,其最大吸收波长为580nm,表观摩尔吸光系数为4.8×10^4L·mol^-1·cm^-1,显色反应瞬间完成,有色配合物稳定24h以上,铜量在0-0.8mg/L范围内符合比耳定律,用于水样中微量铜的测定,结果满意。  相似文献   

5.
湿法消化荧光法测定蔬菜中的微量锗   总被引:4,自引:0,他引:4  
本文研究了蔬菜中微量锗的荧光测定方法,用混酸消化样品,不经萃取分离可用标准加入法测定计算样品的含量。  相似文献   

6.
侯宝花 《光谱实验室》2003,20(1):108-109
本文详细讨论了铸铁试样中硅的测定结果与粒度的关系。  相似文献   

7.
在环己烷介质中,溴氰菊酯在278nm处有特征吸收峰,根据此建立了一种紫外分光光度法测定溴氰菊脂的新方法,方法用于溴氰菊酯粉剂中溴氰菊酯含量的测定,结果满意。  相似文献   

8.
国内汞测定评述   总被引:3,自引:0,他引:3  
本文评述了应用化学法、原子荧光法、原子吸收法、色谱法、电化学法、间接法、以及其他方法对Hg的分析。  相似文献   

9.
三波长分光光度法测定色氨酸,酪氨酸和苯丙氨酸的研究   总被引:2,自引:0,他引:2  
本文用三波长分光光度法测定色氨酸,酪氨酸和苯丙氨酸,利用计算机选择最佳波长组合,可实现三种组分的同时测定,合成样品的分析结果表明,方法的准确和精密度都令人满意。  相似文献   

10.
黄芩中锗的分光光度研究   总被引:4,自引:0,他引:4  
对黄芩中的锗进行了分光光度法研究,结果表明,黄芩中含有丰富的有机锗。本方法简单可靠,可获得满意的分析结果。  相似文献   

11.
Results of radionuclide activity concentration measurements in deposition and ground-level air conducted at the station of the Institute of Physics situated 3.5 km from the Ignalina Nuclear Power Plant (Ignalina NPP) in 2005 are analyzed. Atmospheric depositional fluxes of 7Be, 60Co and 137Cs are estimated. Radionuclide particle deposition rates are calculated. The Hybrid Single-Particle Lagrangian Integrated Trajectory (HYSPLIT) model of the global dispersion and deposition is used to explain variations in the 137Cs activity concentration in the ground-level air in the Ignalina NPP region in 2005. An increase in the 137Cs activity concentration of up to 17.4 μBq m−3 on 30 October-5 November is studied. Modelling results show that the Chernobyl NPP Unit 4 Sarcophagus and the radiocaesium resuspension from the Chernobyl NPP accident polluted regions are sources of 137Cs to the environment of the Ignalina NPP. Results on solubility in water of aerosols — carriers of 137Cs — are discussed.  相似文献   

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13.
The solutions of a renormalized BCS equation are studied in three space dimensions in s, p and d waves for finite-range separable potentials in the weak to medium coupling region. In the weak-coupling limit, the present BCS model yields a small coherence length and a large critical temperature, , appropriate for some high- materials. The BCS gap, , and specific heat as a function of zero-temperature condensation energy are found to exhibit potential-independent universal scalings. The entropy, specific heat, spin susceptibility and penetration depth as a function of temperature exhibit universal scaling below in p and d waves. Received: 18 July 1997 / Revised: 8 September 1997 / Accepted: 29 September 1997  相似文献   

14.
The thermal instability of a layer of Rivlin-Ericksen elastico-viscous fluid in porous medium acted on by a uniform magnetic field is considered. For stationary convection, Rivlin-Ericksen elastico-viscous fluid behaves like a Newtonian fluid. The magnetic field is found to have stabilizing effect whereas medium permeability has destabilizing effect. The magnetic field introduces oscillatory modes in the system, A sufficient condition for the non-existence of overstability is also obtained.  相似文献   

15.
It is shown that bulk semiconductors exhibit strongly asymmetric Fano-type resonance profiles in magnetoabsorption processes involving the formation of hot electron-hole pairs (EHPs) and accompanied by the scattering of the EHPs by defects. This result is valid for transitions to electronic states with large Landau quantum numbers, when the Coulomb interaction plays a small role. The physical reason for such a sharp change in the magnetoabsorption coefficient as compared with the expected result for the ordinary density of states in a quantizing magnetic field is that the electronic excitations are quasi-one-dimensional. The form of the resonance absorption is in good qualitative agreement with the experimental data. Pis’ma Zh. éksp. Teor. Fiz. 63, No. 8, 619–622 (25 April 1996)  相似文献   

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17.
The concepts of uncertainty in prediction and inference are introduced and illustrated using the diffraction of light as an example. The close relationship between the concepts of uncertainty in inference and resolving power is noted. A general quantitative measure of uncertainty in inference can be obtained by means of the so-called statistical distance between probability distributions. When applied to quantum mechanics, this distance leads to a measure of the distinguishability of quantum states, which essentially is the absolute value of the matrix element between the states. The importance of this result to the quantum mechanical uncertainty principle is noted. The second part of the paper provides a derivation of the statistical distance on the basis of the so-called method of support.  相似文献   

18.
We present the action and transformation laws of supergravity in 11 dimensions which is expected to be closely related to the O(8) theory in 4 dimensions after dimensional reduction.  相似文献   

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