不同加载状态下TA2钛合金绝热剪切破坏响应特性

一般认为绝热剪切现象在宏观上表现为材料动态本构失稳,即热软化大于应变硬化.本文采用帽型受迫剪切试样研究TA2钛合金的动态力学特性和本构失稳过程.首先对剪切区加载应力状态进行理论和数值分析,通过合理设计帽型试样,剪切区变形可近似按剪切状态处理;结合二维数字图像相关法(two-dimensional digital image correlation,DIC-2D)直接测试试样剪切区应变演化,给出帽型受迫剪切实验的等效应力-应变响应曲线.进一步,利用Hopkinson压杆对TA2钛合金开展动态压缩及帽型剪切对比试验研究,比较压缩、剪切试验得到的等效应力-应变曲线,采用"冻结"试样方法分析试样中绝热剪切局域化演化过程,探讨不同加载状态下TA2钛合金的绝热剪切破坏现象及其动态力学响应特性.实验结果表明,在塑性变形初始阶段,动态压缩及剪切加载下的等效应力-应变曲线符合较好,但随塑性损伤发展及绝热剪切带形成,两者出现分离,表明损伤及绝热剪切演化过程与应力状态相关.剪切试样实验得到的本构"软化"特性能够反映绝热剪切带起始、破坏演化过程的力学响应特性,而在动态压缩实验中,即使试样中已出现双锥形的绝热剪切带及局部裂纹分布,其表观等效应力-应变曲线并不出现软化特征,动态压缩实验无法得到关于绝热剪切起始、发展以及破坏的本构软化响应特性.     

Ta2钛合金绝热剪切失稳起始温度研究

利用分离式霍普金森压杆加载TA2钛合金扁平帽型试样,结合高速红外测温与金相观察,分析动态加载下帽型试样受迫剪切力学响应以及绝热剪切带温度演化,确定绝热剪切带起始温度,并讨论绝热剪切失稳起始条件。结果显示,绝热剪切带起始温度约为470K,明显低于再结晶温度,以温度470K作为起始条件,对应剪切应力时程曲线起始时刻,并非剪切应力最大值,而是应力软化至504MPa,即发生应力“塌陷”处,应力下降8.86%,塑性应变继续发展     

TC4在动态载荷下的剪切行为研究

使用分离式霍布金森压杆(SHPB)对2种TC4(Ti-6Al-4V)试样(单边剪切试样与双边剪切试样)在应变率104 s-1下进行动态剪切加载，利用SIM D8高速照相系统捕捉了绝热剪切带扩展的整个历程，得到了TC4在拍照时刻的应力应变曲线；使用金相显微镜和SEM扫描电镜对TC4绝热剪切带的微观形貌进行观察，发现绝热剪切带宽度为5~12 μm，断口从韧窝断裂演变为解理断裂，可观测到韧窝状与河流花样断口形貌，但是并未看到相变的发生；对2种试样就产生绝热剪切带的形式与敏感性进行了分析，实验表明双边试样更易产生绝热剪切带；通过高速照相系统的标定换算，得到TC4绝热剪切带产生的临界剪切应变在78%~88%之间。在SHPB动态加载条件下，TC4绝热剪切带的扩展速度在460~1 250 m/s之间，且应变率越高，剪切带扩展越快，扩展平均速度与名义应变率近似呈线性关系；另外，在同一加载速率下，剪切带并不是匀速扩展，其扩展速度随载荷的增加而不断增加。     

电弧增材制造不锈钢动态加载绝热剪切带内组织研究

绝热剪切失效是增材制造金属材料在高应变率载荷下的重要失效方式。使用电火花从冷金属过渡电弧增材技术制备的316L不锈钢单壁上沿着制造方向和扫描方向割出动态加载圆柱试样(尺寸为?4 mm×4 mm)。采用分离式霍普金森杆对增材制造316L试样在应变率4 000到6 000 s^-1下加载至绝热剪切状态,研究了其动态剪切变形行为特别是剪切带内微观组织特征结构。不同应变率动态加载下,电弧增材制造316L不锈钢的动态应力首先由于应变硬化而增大,随后绝热剪切热软化与应变硬化的平衡导致了动态变形最后阶段的应力平台效应。绝热剪切带中亚晶经历了动态再结晶过程,具有与基体完全不同的等轴晶形貌,晶粒尺寸大约在200～300 nm。动态剪切复杂热力过程导致剪切带内的亚晶形成了双重织构,既有与基体一致的沿着压缩方向的<110>丝织构,也有与宏观剪切方向相关的晶体学织构,即(111)沿着宏观剪切面,<112>沿着宏观剪切方向。不同剪切带的等轴亚晶都有大量残余Σ3 60°晶界,同时存在与基体相同的孪生织构,可以证明孪生再结晶是绝热剪切带内亚晶主要的动态再结晶机制。宏观绝热...     

快速加载下TNT材料中绝热剪切带的细观研究

本文对快加载后的国产ＴＮＴ材料，采用光学显微镜和扫描电镜观察，研究了其显微组织，结果表明：在快速加载条件下材料中有绝热剪切带生成。剪切带在细观上的表现形式为：（１）以应变高度集中，晶粒剧烈扭曲为特征的细观组织形貌；（２）在局部区域，晶粒被急剧拉长，形成粗亮而边界清晰的剪切带。在快速加载条件下ＴＮＴ材料中绝热剪切带的产生同时取决于应变和应变切带。在快速的加载条件ＴＮＴ材料中绝热剪切带的产生同时决于应     

921A 钢纯剪切帽状试件绝热剪切变形的数值模拟

结合相关实验,通过一系列基于921A 钢纯剪切帽状试件的SHPB数值模拟,研究试件的绝热剪 切行为,分析试件内绝热剪切带(ASB)的产生、发展以及相应的试件温度场分布。研究发现:ASB是通过剪 切区两端高温高应变的不稳定区域的扩展而形成;ASB的扩展速率与加载速率相关;在本文加载速率范围 内,ASB带宽无明显变化,均为约70m,基本与所设计的试件剪切区宽度一致;且对应所有加载速率,ASB 均为形变带。     

再结晶组织对TA2纯钛绝热剪切行为的影响

使用二辊轧机对TA2工业纯钛进行多道次大应变冷轧处理,制备了冷轧总变形量为70%的TA2纯钛板。通过对冷轧TA2纯钛板进行500℃加热、不同保温时间的退火处理,获得了具有不同再结晶组织的钛板。基于帽形试样和限位环变形控制技术,在分离式霍普金森压杆装置上对不同再结晶组织的试样进行动态冲击冻结实验,结合光学显微镜和扫描电子显微镜表征试样冲击前后微观组织的变化,研究了再结晶组织对TA2纯钛绝热剪切行为的影响。结果表明,随着退火保温时间的延长,试样再结晶晶粒占比逐渐增大,晶粒分布由分散向局部聚集转变;在相同应变和应变率下,在所有试样中都观察到了绝热剪切带,再结晶晶粒占比高的试样更易诱发绝热剪切带中裂纹形核扩展。对比变形前后试样再结晶组织和几何必需位错变化,结合剪切区整体温升分析发现,再结晶晶粒作为材料软化点能够诱发剪切带的形成,而剪切带发展后期产生的绝热温升会促进剪切带内材料发生二次再结晶,提高剪切带内材料的韧性,延缓剪切裂纹的形成。     

纯锆在压缩加载下微观变形断裂机制研究

利用材料试验机和SHPB装置研究了常态下纯锆的准静态和动态压缩力学性能。塑性变形阶段的流动应力及硬化率随应变率提高而增大,应变10％～20％段的应力-应变曲线表现出凹向上趋势。金相观测表明孪晶是纯锆的重要变形机制,孪晶密度随应变及应变率的增长而增大。大应变时,在动态压缩试样表面观测到与压缩轴呈45&#176;的宏观裂纹。试样纵向剖开后,金相观测到发展的绝热剪切带。     

表面粗糙度对TC4钛合金柱壳剪切带形成的影响

剪切带是材料在高应变率加载条件下特有的变形和损伤形式之一,关于影响金属材料中剪切带形成的敏感性因素及其机理的研究,一直是科学研究和工程设计中关注的重点问题. 在柱壳高速坍塌过程中,剪切带优先在内表面形核, 其形核及扩展行为受内表面介观状态的影响显著.本文采用爆轰加载厚壁圆筒坍塌实验技术,结合材料表面处理技术、微结构表征技术和剪切带理论模型分析,研究了内表面粗糙度变化对TC4钛合金柱壳剪切带形成影响的细观动力学规律.结果表明, 在爆炸加载形成的高应变率条件下,表面粗糙度对TC4钛合金柱壳中剪切带形成具有明显影响. 在相同的变形条件下,随着试样内表面粗糙度的增大, 剪切带数量、长度和形核速率均增大;表面粗糙度越大, 部分剪切带扩展速率越快, 剪切带长度差异越大,剪切带的屏蔽效应增强. 分析表明,实验获得的剪切带间距与W-O模型和M模型预测结果基本吻合,具体数值受试样内表面粗糙度影响, 随着表面粗糙度的增大,实验结果逐渐小于预测数值.      

分子动力学模拟金属玻璃板拉伸时剪切带的形成和演化过程

金属玻璃在低温高应力条件下容易生成剪切带而导致结构的破坏,大大限制了它的推广应用。本文采用分子动力学模拟研究了三种Cu64Zr36（不带缺口、一侧带缺口、两侧带缺口）金属玻璃板试样在拉伸过程中剪切带的形成和演化过程及其力学性能。结果表明：不带缺口金属玻璃板试样在低温高应力的拉伸过程中会自发出现局部剪切转变区,发生剪切局部化,继续拉伸会在与加载轴大约成45°方向上形成剪切带。剪切带的形成与剪切转变区的分布和局部化有关,带缺口比不带缺口的试样会更早出现应变局部化,即在较低的拉伸应变下便形成剪切带,其拉伸强度也相应较低。相同条件下,一侧带缺口与两侧带缺口的试样在拉伸强度上几乎相同,但两侧带缺口试样的应变局部化程度稍低,主要是两侧缺口处均出现了剪切转变区,导致其分布和局部化不够集中,这也是形成主剪切带和次剪切带的主要原因。以上结果为进一步从原子尺度理解金属玻璃剪切带的形成和演化特征提供了重要的信息。     

试样形状对轴承钢绝热剪切带微观组织的影响

绝热剪切带(ASB)的微观组织受试样几何形状的影响。对圆柱、帽形和剪切压缩型三种不同形状的试样进行分离式霍普金森压杆高速冲击试验,研究试样形状对轴承钢绝热剪切带的形成和微观组织的影响。结果表明,在应变率为1 800～3 100 s^-1的范围内,材料对应变率的敏感性很低。圆柱试样呈现明显的应变硬化,而帽形试样和剪切压缩型试样(SCS)在不同应变率下分别出现应变硬化和无应变硬化的特征,但流变应力并未因应变硬化而提高。试样形状对ASB的微观形貌和组织有很大影响。圆柱试样上产生了窄且细长的ASB,只发生了应变诱发的晶粒细化,属于形变ASB;帽形试样和SCS则形成大片状的ASB,由等轴晶组成,且发生了体心立方体(BCC)马氏体转变为面心立方体(FCC)奥氏体的相变,属于相变ASB。尤其是SCS中ASB的等轴晶,有非常清晰的晶界,是典型的动态再结晶晶粒。温升计算结果显示,圆柱试样ASB的温升远低于奥氏体相变温度,而帽形试样和SCS的温升高于马氏体的熔点,导致局部熔融。     

A NOVEL APPROACH TO TESTING THE DYNAMIC SHEAR RESPONSE OF Ti-6Al-4V

Modifications were made on the traditional split Hopkinson pressure bar (SHPB) system to conduct dynamic shear tests. The shear response of Ti-6Al-4V was acquired at a shear strain rate of 10 4 s 1 by using this modified apparatus. The geometry as well as the clamping mode of the double-notch specimen was optimized by commercial FEM software ABAQUS, and the feasibility of the experiment set-up was validated. A shear stress calibration coefficient of τ = 1.03 and a shear strain calibration coefficient of Γ = 0.50 were obtained.We have employed high-speed photography to record the deformation process, especially the initiation and propagation of adiabatic shear band (ASB), during the dynamic shear test. The frames show that the time duration from ASB initiation to its completion is less than 2 μs, from which we can estimate that the propagation speed of ASB within Ti-6Al-4V is more than 1250 m/s under such loading conditions. The temperature rise within ASB is also estimated to be T 2 ≈ 1460℃ based on energy balance. Such high temperature has led to softening of the material within the ASBs, and has intensified the shear localization and finally resulted in fracture of the material.     

表面加工塑性层对金属柱壳剪切带自组织单旋起始的影响

在外爆加载金属柱壳高速坍塌过程中, 发生塑性变形失稳形成的剪切带具有高度的自组织特征, 甚至出现剪切带排列的单旋现象—剪切带在顺时针和逆时针两个方向呈现一个方向占优的现象. 柱壳在坍塌时, 最大剪切应力位于柱壳内表面, 剪切带的形核及扩展行为受内表面材料介观状态的影响显著. 本文通过选材和控制柱壳加工工艺, 获得了内表面具有不同厚度塑性层的20钢柱壳, 采用厚壁圆筒实验技术, 研究了表面加工塑性层对金属柱壳绝热剪切带自组织单旋现象起始的影响规律及其物理机制. 研究结果表明, 金属柱壳内表面加工塑性层显著改变了试样剪切带的起始条件, 沿顺时针或逆时针方向排列的剪切带形核数量在总剪切带数量中所占比例取决于表面加工塑性层的厚度和晶粒取向, 具有单一晶粒拉伸方向的较厚塑性层样品更容易形成单向螺旋剪切带结构. 在相同变形条件下, 随着塑性层厚度增加, 剪切带平均形核速率和扩展速率增大, 剪切带平均间距减小. 结果可为理解金属柱壳在高速塌陷过程中绝热剪切带占优取向现象提供有价值的参考.      

In Situ Observation of Adiabatic Shear Band Formation in Aluminum Alloys

We used high-speed X-ray phase contrast imaging and infrared thermal imaging techniques to study the formation processes of adiabatic shear bands in aluminum 7075-T6 and 6061-T6 alloys. A modified compression Kolsky bar setup was used to apply the dynamic loading. A flat hat-shaped specimen design was adopted for generating the shear bands at the designated locations. Experimental results show that 7075-T6 exhibits less ductility and a narrower shear band than 6061-T6. Maximum temperatures of 720 K and 770 K were locally determined within the shear band zones for 7075-T6 and 6061-T6 respectively. This local high temperature zone and the resulting thermal instability were found to relate to the shear band formation in these aluminum alloys.

     

An experimental and numerical study of the localization behavior of tantalum and stainless steel

In general, the shear localization process involves initiation and growth. Initiation is expected to be a stochastic process in material space where anisotropy in the elastic–plastic behavior of single crystals and inter-crystalline interactions serve to form natural perturbations to the material’s local stability. A hat-shaped sample geometry was used to study shear localization growth. It is an axi-symmetric sample with an upper “hat” portion and a lower “brim” portion with the shear zone located between the hat and brim. The shear zone length is 870–890 μm with deformation imposed through a split-Hopkinson pressure bar system at maximum top-to-bottom velocity in the range of 8–25 m/s. We present experimental results of the deformation response of tantalum and 316L stainless steel samples. The tantalum samples did not form shear bands but the stainless steel sample formed a late stage shear band. We have also modeled these experiments using both conductive and adiabatic continuum models. An anisotropic elasto-viscoplastic constitutive model with damage evolution was used within the finite element code EPIC. A Mie-Gruneisen equation of state and the rate and temperature sensitive MTS flow stress model together with a Gurson flow surface were employed. The models performed well in predicting the experimental data. The numerical results for tantalum suggested a maximum equivalent strain rate on the order of 7 × 10⁴ s⁻¹ in the gage section for an imposed top surface displacement rate of 17.5 m/s. The models also suggested that for an initial temperature of 298 K a temperature in the neighborhood of 900 K was reached within the shear section. The numerical results for stainless steel suggest that melting temperature was reached throughout the shear band shortly after peak load. Due to sample geometry, the stress state in the shear zone was not pure shear; a significant normal stress relative to the shear zone basis line was developed.     

On stress collapse in adiabatic shear bands

The dynamics of adiabatic shear band formation is considered making use of a simplified thermo/visco/plastic flow law. A new numerical solution is used to follow the growth of a perturbation from initiation, through early growth and severe localization, to a slowly varying terminal configuration. Asymptotic analyses predict the early and late stage patterns, but the timing and structure of the abrupt transition to severe localization can only be studied numerically, to date. A characteristic feature of the process is that temperature and plastic strain rate begin to localize immediately, but only slowly, whereas the stress first evolves almost as if there were no perturbation, but then collapses rapidly when severe localization occurs.     

高锰钢帽型样品在高速冲击下的剪切行为

绝热剪切带是材料在高速变形时一种典型的破坏形式,为了更好地理解高速冲击过程中绝热剪切带的形成和扩展,基于Johnson-Cook本构模型,利用ANSYS/LS-DYNA软件对高锰钢帽型样品高速冲击过程的剪切行为进行了二维数值模拟。结果表明:横穿剪切带方向,应力应变分布都是剪切带中心最高,然后向两边逐渐降低,类似于高斯分布; 平行于剪切带方向,应力应变分布则是呈两端高中间低的特点。然后利用模拟的应力应变场分布确定了剪切带和裂纹形成及扩展方向,即从剪切区两端形成并向中间扩展;最后通过编辑软件的k文件直接得到了剪切带内部及周围形变影响区和基体的温度分布,其和应力应变场分布规律一致,结果与实验结果基本吻合。