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1.
Modified derivatives of angular and linear pyranocoumarins containing a condensed cyclohexane moiety were prepared by fusing
a 2,2-dimethyltetrahydropyran ring to the coumarin system and annelating a pyrone ring to derivatives of 2,2-dimethylchromane.
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Translated from Khimiya Prirodnykh Soedinenii, No. 4, pp. 313–318, July–August, 2005. 相似文献
2.
A. D. Grebenyuk V. I. Vinogradova A. K. Tashmukhamedova 《Chemistry of Natural Compounds》2006,42(5):585-587
New derivatives of dibenzo-24-crown-8-dicarboxylic acid diamide with salsoline, salsolidine, and anabasine moieties were prepared
by condensation of the alkaloids with 4′,4″(5″)-dibenzo-24-crown-8-dicarboxylic acid dichloride.
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Translated from Khimiya Prirodnykh Soedinenii, No. 5, pp. 471–473, September–October, 2006. 相似文献
3.
E. M. Suleimenov O. V. Morozova V. A. Raldugin Yu. V. Gatilov T. V. Rybalova M. M. Shakirov R. Seidakhmetov R. M. Aksartov S. M. Adekenov 《Chemistry of Natural Compounds》2005,41(5):556-560
Four sesquiterpene lactones with the germacrane structure were isolated from the aerial part of Stizolophus balsamita. X-ray structure analyses showed that two of them were previously known balsamin derivatives. A third was a crystalline isomorphous
mixture of the known lactone stizolin and 11,13-dihydrostizolin in a 53:47 ratio. The biological activities of the balsamin
derivatives were investigated.
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Translated from Khimiya Prirodnykh Soedinenii, No. 5, pp. 454–457, September–October, 2005. 相似文献
4.
L. R. Mikhailova M. V. Khudobko L. A. BaltinaJr. L. V. Spirikhin R. M. Kondratenko L. A. Baltina 《Chemistry of Natural Compounds》2009,45(3):393-397
Ring A was transformed and new A-homo-4-aza- and 3-cyano-3,4-seco-olean-4-ene derivatives of 3β-hydroxy18βH-olean-9,12-dien-30-oic acid were synthesized.
Translated from Khimiya Prirodnykh Soedinenii, No. 3, pp. 335–338, May–June, 2009. 相似文献
5.
A simple, sensitive and low-cost method was developed for the determination of aspartate (Asp) and glutamate (Glu) in rabbit
retina. Polymer monolith microextraction (PMME) using a poly(acrylamide–vinylpyridine–N,N′-methylene bisacrylamide) (AA–VP–Bis) monolithic column was combined with derivatization of Asp and Glu using 8-phenyl-(4-oxy-acetic
acid N-hydroxysuccinimide ester)-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene (TMPAB-OSu), and this was used to analyze the derivatives of Asp and Glu by high-performance liquid chromatography
(HPLC) with fluorescence detection. The conditions for the derivatization and the subsequent extraction of Asp and Glu derivatives
were optimized. The enrichment factors for the derivatives of Asp and Glu were found to be 14.1 and 14.7, respectively, by
PMME. The limits of detection of Asp and Glu were 0.14 and 0.53 nmol/L, respectively. The precision and recovery were evaluated
with spiked retina. The inter- and intraday relative standard deviations were less than 10%. The proposed method was successfully
applied to the determination of Asp and Glu levels in rabbit retina samples with different stages of intraocular hypertension. 相似文献
6.
T. I. Akimova V. A. Kaminsky I. V. Svistunova 《Chemistry of Heterocyclic Compounds》2005,41(11):1374-1380
Xanthene derivatives and ortho-substituted phenols were obtained during the dehydrogenation of 1,5-diketones and their ketol
forms at a Pt/C catalyst at 280–320°C.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1637–1643, November, 2005. 相似文献
7.
Ecdysterone, cyasterone, ajugalactone, ajugasterone B, 22-acetylcyasterone, and turkesterone were isolated from leaves of
Ajuga turkestanica (Labiatae). Their structures were established using spectral and chemical data. The 2,3,22-triacetate, 2,3,22-tri-O-p-iodobenzoylthiocarbamate, and 2-O-p-iodobenzoylthiocarbamate derivatives of cyasterone were synthesized.
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Translated from Khimiya Prirodnykh Soedinenii, No. 5, pp. 449–451, September–October, 2006. 相似文献
8.
G. Yu. Ishmuratov M. P. Yakovleva V. A. Ganieva R. Ya. Kharisov R. R. Gazetdinov A. M. Abulkaramova G. A. Tolstikov 《Chemistry of Natural Compounds》2006,42(1):92-95
Three new approaches to the synthesis of 1-bromo-3S-methylundecane, a key synthon in the synthesis of (S,S,S)-diprionylacetate, a sex pheromone of pine sawflies of the genera Diprion and Neodiprion, were proposed based on chemo-and stereoselective transformations of L-(-)-menthol derivatives.
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Translated from Khimiya Prirodnykh Soedinenii, No. 1, pp. 73–76, January–February, 2006. 相似文献
9.
A series of derivatives of the natural sesquiterpene lactones alantolactone (1) and isoalantolactone (2) was prepared. The α-methylene-γ-lactone moiety was retained in the structures of these for further modifications using reactions
that affected exclusively the nonconjugated double bonds of the decalin ring.
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Translated from Khimiya Prirodnykh Soedinenii, No. 4, pp. 325–330, July–August, 2006. 相似文献
10.
N. N. Chopabaeva 《Chemistry of Natural Compounds》2007,43(5):598-602
Polyfunctional ion-exchangers were synthesized by heterophase amination of α-oxide derivatives of hydrolyzed lignin with aliphatic di-and polyamines. Optimal conditions for their preparation were determined.
Certain physicochemical properties were studied.
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Translated from Khimiya Prirodnykh Soedinenii, No. 5, pp. 492–495, September–October, 2007. 相似文献
11.
New biologically active quaternary salts of the alkaloids ajmaline, quinine, hyoscyamine, codeine, and strychnine were synthesized.
So-called separable conformers were observed among the ajmaline derivatives.
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Translated from Khimiya Prirodnykh Soedinenii, No. 4, pp. 381–383, July–August, 2006. 相似文献
12.
Recyclization of the chromone ring in several natural isoflavonoids and their analogs by reaction with hydroxylamine was studied.
It has been found that the most suitable base for carrying out the reaction is N-methylmorpholine. Several derivatives of
4-aryl-5-(2-hydroxyphenyl)isoxazole were synthesized.
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Translated from Khimiya Prirodnykh Soedinenii, No. 4, pp. 332–336, July–August, 2007. 相似文献
13.
Methyl iodide activated stereospecific α-mannosylations utilising 2-pyridyl-1-thiomannopyranoside derivatives (2,3,4) as donors
and suitably protected myo-inositol derivatives (1,25,27,29) as acceptors to prepare 2-0-α-D-mannopyranosyl-6-[O-α-D-mannopyranosyl-(1–6)-O-α-D-mannopyranosyl-(l-6)-O-α-D-mannopyranosyl]-D-myo-inositol derivative (31) is described.
IICT Commun. No. 3355 相似文献
14.
K. A. Frolov V. V. Dotsenko S. G. Krivokolysko V. P. Litvinov 《Russian Chemical Bulletin》2005,54(9):2226-2228
Reactions of (Z)-5-benzylidene-2-thiohydantoin with formaldehyde and primary aromatic amines afforded novel derivatives of imidazo[2,1-b][1,3,5]thiadiazine in 50–69% yields.
Dedicated to Academician N. S. Zefirov on the occasion of his 70th birthday.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 9, pp. 2158–2160, September, 2005. 相似文献
15.
Theoretical information indices of cis- and trans-4-cyclohexene-1,2-dicarboxylic acids and their methyl and dimethyl substituted derivatives are calculated. Correlations between
the indices and physicochemical properties of these compounds are analyzed.
Original Russian Text Copyright ? 2009 by M. S. Salakhov, B. T. Bagmanov, and O. T. Grechkina
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Translated from Zhurnal Strukturnoi Khimii, Vol. 50, No. 1, pp. 183–187, January–February, 2009. 相似文献
16.
Victor V. Dotsenko Sergey G. Krivokolysko Victor P. Litvinov 《Monatshefte für Chemie / Chemical Monthly》2008,139(6):657-661
Morpholinium 3-cyano-4-methyl-6-oxo-1,6-dihydropyridine-2-thiolate upon treatment with primary amines and a formaldehyde excess
under mild conditions produces bis(pyrido[2,1-b][1,3,5]thiadiazin-7-yl)methane derivatives in good yields (67–87%).
Correspondence: Victor V. Dotsenko, State Enterprise “Luganskstandartmetrology”, 91021 Lugansk, Ukraine. 相似文献
17.
L. Bukowski Z. Zwolska E. Augustynowicz-Kopec 《Chemistry of Heterocyclic Compounds》2006,42(10):1358-1365
The reactions of 2-acetylimidazo[4,5-b]pyridine hydrazone with some alkyl-and arylisothiocyanates and some orthoesters were
carried out. Various new derivatives of the titled compound such as thiosemicarbazones, ethoxymethylenehydrazones, and derivatives
of the new pyrido-[3′,2′:4,5]imidazo[1,2-d][1,2,4]triazine ring system were obtained. Biological data for selected compounds
are presented.
Published in Khimiya Geterotsiklicheskikh Soedinenii, No. 10, pp. 1571–1579, October, 2006. 相似文献
18.
L. M. Likhosherstov O. S. Novikova A. O. Zheltova V. N. Shibaev 《Russian Chemical Bulletin》2000,49(8):1454-1459
A convenient preparative procedure was developed for the synthesis ofN-glycyl-β-glycopyranosylamines, derivatives of monosaccharides (d-galactose,d-mannose,l-fucose, andN-acetyl-d-glucosamine) and disaccharides (lactose, melibiose, cellobiose, and maltose). These compounds were demonstrated to be useful
for the preparation of glycoconjugates of biologically active compounds containing the carboxy group (nicotinic, orotic, kynurenic,
and indoleacetic acids). Synthetic pathways were developed for conversions ofN-glycyl-β-glycopyranosylamines into derivatives containing the carboxy group with the use of malonic andl-tartaric acid derivatives.
Published inIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 8, pp. 1461–1466, August, 2000. 相似文献
19.
Viktoria S. Moskvina Olexander V. Turov Volodymyr P. Khilya Myroslav M. Garazd Ulrich M. Groth 《Monatshefte für Chemie / Chemical Monthly》2008,139(11):1391-1396
New functionalized derivatives of 8,8,10-trimethyl-4-phenyl-7,8-dihydro-2H,6H-pyrano[3,2-g]-chromene-2,6-dione – analogues of the natural compound graveolone – possessing hydrazine, hydroxylamine, and thiosemicarbazide
residues were synthesized and their reactions with acetic anhydride were studied. The structure of the obtained compounds
was confirmed by NMR spectroscopy.
Correspondence: Viktoria Moskvina, Chemistry Department, Kyiv National Taras Shevchenko University, 60, ul. Vladimirskaya,
01033 Kyiv, Ukraine. 相似文献
20.
I. Manojlović G. Bogdanović-Dusanović W. Gritsanapan N. Manojlović 《Chemical Papers》2006,60(6):466-468
Five hydroxyanthraquinone derivatives physcion, emodin, fallacinal, teloschistin, and 1,3-dimethoxy-8-hydroxy-6-methyl-9,10-anthraquinone
were isolated from the lichen Caloplaca cerina growing in Serbia. Three anthraquinone derivatives, namely physcion, emodin, and rhein were isolated and identified from
the Thai medicinal plant Cassia tora.
Presented at the 33rd International Conference of the Slovak Society of Chemical Engineering, Tatranské Matliare, 22–26 May
2006. 相似文献