Visualization of flow boiling of liquid nitrogen in a vertical mini-tube

The flow boiling patterns of liquid nitrogen in a vertical mini-tube with an inner diameter of 1.931 mm are visualized with a high-speed digital camera. The superficial gas and liquid velocities are in the ranges of 0.01–26.5 m/s and 0.01–1.2 m/s, respectively. Four typical flow patterns, namely, bubbly, slug, churn and annular flow are observed. Some interesting scenes about the entrainment and liquid droplet deposition in the churn and annular flow, and the flow reversal with the indication of negative pressure drop, are also presented. Based on the visualization, the two-phase flow regime maps are obtained. Compared with the flow regime maps for gas–water flow in tubes with similar hydraulic diameters, the region of slug flow in the present study reduces significantly. Correspondingly, the transition boundary from the bubbly flow to slug flow shifts to higher superficial gas velocity, and that of churn to annular flow moves to lower superficial gas velocity. Moreover, time-averaged void fraction is calculated by quantitative image-digitizing technique and compared with various prediction models. Finally, three kinds of oscillations with long-period and large-amplitude are found, possible explanation for the oscillations is given by comparing the instantaneous flow images with the data of pressure, mass flux and temperature recorded synchronously.     

Experimental study on axial development of liquid film in vertical upward annular two-phase flow

Accurate measurements of the interfacial wave structure of upward annular two-phase flow in a vertical pipe were performed using a laser focus displacement meter (LFD). The purpose of this study was to clarify the effectiveness of the LFD for obtaining detailed information on the interfacial displacement of a liquid film in annular two-phase flow and to investigate the effect of axial distance from the air–water inlet on the phenomena. Adiabatic upward annular air–water flow experiments were conducted using a 3 m long, 11 mm ID pipe. Measurements of interfacial waves were conducted at 21 axial locations, spaced 110 mm apart in the pipe. The axial distances from the inlet (z) normalized by the pipe diameter (D) varied over z/D = 50–250. Data were collected for predetermined gas and liquid flow conditions and for Reynolds numbers ranging from Re_G = 31,800 to 98,300 for the gas phase and Re_L = 1050 to 9430 for the liquid phase. Using the LFD, we obtained such local properties as the minimum thickness, maximum thickness, and passing frequency of the waves. The maximum film thickness and passing frequency of disturbance waves decreased gradually, with some oscillations, as flow developed. The flow development, i.e., decreasing film thickness and passing frequency, persisted until the end of the pipe, which means that the flow might never reach the fully developed state. The minimum film thickness decreased with flow development and with increasing gas flow rate. These results are discussed, taking into account the buffer layer calculated from Karman’s three-layer model. A correlation is proposed between the minimum film thickness obtained in relation to the interfacial shear stress and the Reynolds number of the liquid.     

Studies on two-phase co-current air/non-Newtonian shear-thinning fluid flows in inclined smooth pipes

In this work, co-current flow characteristics of air/non-Newtonian liquid systems in inclined smooth pipes are studied experimentally and theoretically using transparent tubes of 20, 40 and 60 mm in diameter. Each tube includes two 10 m long pipe branches connected by a U-bend that is capable of being inclined to any angle, from a completely horizontal to a fully vertical position. The flow rate of each phase is varied over a wide range. The studied flow phenomena are bubbly flow, stratified flow, plug flow, slug flow, churn flow and annular flow. These are observed and recorded by a high-speed camera over a wide range of operating conditions. The effects of the liquid phase properties, the inclination angle and the pipe diameter on two-phase flow characteristics are systematically studied. The Heywood–Charles model for horizontal flow was modified to accommodate stratified flow in inclined pipes, taking into account the average void fraction and pressure drop of the mixture flow of a gas/non-Newtonian liquid. The pressure drop gradient model of Taitel and Barnea for a gas/Newtonian liquid slug flow was extended to include liquids possessing shear-thinning flow behaviour in inclined pipes. The comparison of the predicted values with the experimental data shows that the models presented here provide a reasonable estimate of the average void fraction and the corresponding pressure drop for the mixture flow of a gas/non-Newtonian liquid.     

The effect of surfactants on air–water annular and churn flow in vertical pipes. Part 1: Morphology of the air–water interface

In this work, the influence of surfactants on air–water flow was studied by performing experiments in a 12 metre long, 50 mm inner diameter, vertical pipe at ambient conditions. High-speed visualisation of the flow shows that the morphology of the air–water interface determines the formation of foam. The foam subsequently alters the flow morphology significantly. In annular flow, the foam suppresses the roll waves, and a foamy crest is formed on the ripple waves. In the churn flow regime, the flooding waves and the downwards motion of the liquid film are suppressed by the foam. The foam is transported in foam waves moving upwards superposed on an almost stagnant foam substrate at the pipe wall. Foam thus effectively reduces the superficial gas velocity at which the transition from annular to churn flow occurs. These experiments make more clear how surfactants can postpone liquid loading in vertical pipes, such as in gas wells.     

The effect of the diameter on air-water annular and churn flow in vertical pipes with and without surfactants

In this work, we present results of flow visualisation, pressure gradient measurements, and liquid holdup measurements for air-water flow without and with surfactants in vertical pipes with diameters of 34 mm, 50 mm, and 80 mm. The surfactants cause the formation of foam. This foam has a larger volume and a smaller density than the liquid. The larger volume results in a larger pressure gradient at large gas flow rates. At small gas flow rates, the lower density of the foam causes the transition between the regular annular flow regime and the irregular churn flow regime to shift to lower gas flow rates. As a result foam reduces the pressure gradient and the liquid holdup at small gas flow rates. Surfactants reduce the pressure gradient more effectively for thinner liquid films at the wall; therefore, they are more effective for small pipe diameters and small liquid flow rates.     

Flow patterns of n-hexadecane–CO2 liquid–liquid two-phase flow in vertical pipes under high pressure

To promote a better understanding of liquid–liquid two-phase flow behavior, particularly under high pressure, flow patterns of n-hexadecane–CO₂ liquid–liquid two-phase upward flow in vertical stainless steel pipes were experimentally investigated. Observations were made in two 0.0015 m I.D. pipes of different lengths (0.068 m and 0.5 m) under high pressure varying from 10.3 to 29.6 MPa using a high pressure visualization system. The total flow rate was fixed at 2.0 × 10⁻⁶ m³/min, while the flow rate ratio (φ) varied from 0.05 to 19. Bubbly flow, plug flow, slug flow, annular flow, and near-one-phase flow regions were found in both pipes, while stratified flow was observed only in the 0.068 m pipe. Flow pattern maps were constructed in the flow rate ratio versus pressure graph, which demonstrates significant impacts of flow rate ratio, pipe length, and pressure on flow patterns. These impacts are discussed in detail. To the authors’ best knowledge, this work is the first attempt to observe complex liquid–liquid two-phase flow behavior with flow pattern transitions under high pressure, and contributes to a better understanding of liquid–liquid two-phase flow behavior.     

The formation of hydrodynamic slugs by the interaction of waves in gas–liquid two-phase pipe flow

This paper examines the effects of wave interaction on the formation of hydrodynamic slugs in two-phase pipe flow at relatively low gas and liquid superficial velocities. The experiments were conducted using a horizontal 31 m long, D = 10 cm internal diameter transparent pipe at atmospheric pressure. High resolution photography allowed the location of the gas–liquid interface to be measured with a high degree of accuracy at 5 Hz. Image analysis allowed individual waves to be tracked over a 14D section of the pipe. Regular waves having similar properties such as speed, amplitude and length were seen far from the region of slug formation. However, near the transition region, where hydrodynamic slugs were formed, significant differences between wave properties were observed which resulted in wave interaction leading to a type of sub-harmonic resonance and slug formation. The formation of hydrodynamic slugs due to wave interaction differs from predictions for slug formation using long wavelength stability theory. The properties of the waves were quantified which gave detailed information on the resonance mechanism found near the transition to slugging.     

The characteristics of gas/liquid flow in large risers at high pressures

Although most of the work reported on two-phase flows are limited to small pipe diameters, two-phase flow in large risers are increasingly being encountered in the petroleum and nuclear industries. In the present work, a wire mesh sensor was employed to obtain void fraction and bubble size distribution data and visualizations of steam/water flow in a large vertical pipe (194 mm in diameter) at 46 bar. For comparison purposes, measurements were made at similar phase velocities and physical properties to a dataset for nitrogen/naphtha flow in a similar-sized riser. There exist significant differences between both sets of data. Churn-turbulent flow is observed in the present work instead of slug flow, and this differs from the intermittent and semi-annular flow patterns reported for nitrogen/naphtha data. The mean void fraction of the nitrogen/naphtha data is higher than that of the present steam/water data due to the differences in purity in the liquid phases. Furthermore, core peak distributions are observed for the present work in contrast to the flatter profiles deduced for the nitrogen/naphtha using a power law relationship.     

Do huge waves exist in horizontal gas-liquid pipe flow?

Huge waves are periodic interfacial structures which are observed in vertical co-current gas-liquid two-phase flow under churn and the transition between churn and annular flows. Published data examining vertical gas-liquid flow indicate that a huge wave has either a continuous gas core surrounded by a large-scale interfacial wave or a core with a highly-agitated mixture of gas and liquid.Employing a Wire-Mesh Sensor (WMS), the spatio/temporal investigation of high flow rate horizontal air-water flow divulged some recurrent liquid structures (one may call pseudo-slugs) analogous to huge waves of (vertical) churn flow. In both cases, the blow-through (penetration of gas into the liquid structure) was the most manifest feature.Different qualitative and quantitative methods were employed to compare the behavior of pseudo-slug to churn flow. The quantitative measures included Probability Density Function analysis (PDF), distribution coefficient in drift flux model, structural velocity, core average velocity, interfacial friction factor, and slippage number. Both flow regimes demonstrated similar behavior.     

Laminar bubbly flow in an open capillary channel in microgravity

The study of a bubbly laminar two-phase flow in an open capillary channel under microgravity conditions was conducted aboard the sounding rocket, Texus-45. The channel consists of two parallel plates of width b = 25 mm and distance a = 10 mm. The flow along the length l = 80 mm is confined by a free surface on one side and a plate on the opposite side. The bubbles are injected at the nozzle of the capillary channel via six capillary tubes of 100 μm in inner diameter. Different liquid and gas flow rates were tested leading to different liquid free surface shape and bubble size.     

Effect of diameter on two-phase pressure drop in narrow tubes

The effect of tube diameter on two-phase frictional pressure drop was investigated in circular tubes with inner diameters of 0.6, 1.2, 1.7, 2.6 and 3.4 mm using air and water. The gas and liquid superficial velocity ranges were 0.01-50 m/s and 0.01-3 m/s, respectively. The gas and liquid flow rates were measured and the two-phase flow pattern images were recorded using high-speed CMOS camera. Unique flow patterns were observed for smaller tube diameters. Pressure drop was measured and compared with various existing models such as homogeneous model and Lockhart-Martinelli model. It appears that the dominant effect of surface tension shrinking the flow stratification in the annular regime is important. It was found that existing models are inadequate in predicting the pressure drop for all the flow regimes visualized. Based on the analysis of present experimental frictional pressure drop data a correlation is proposed for predicting Chisholm parameter “C” in slug annular flow pattern. For all other flow regimes Chisholm’s original correlation appears to be adequate except the bubbly flow regime where homogeneous model works well. The modification results in overall mean deviation of pressure drop within 25% for all tube diameters considered. This approach of flow regime based modification of liquid gas interaction parameter appears to be the key to pressure drop prediction in narrow tubes.     

Experimental investigation on the slip between oil and water in horizontal pipes

This work is devoted to study of the slip phenomenon between phases in water–oil two-phase flow in horizontal pipes. The emphasis is placed on the effects of input fluids flow rates, pipe diameter and viscosities of oil phase on the slip. Experiments were conducted to measure the holdup in two horizontal pipes with 0.05 m diameter and 0.025 m diameter, respectively, using two different viscosities of white oil and tap water as liquid phases. Results showed that the ratios of in situ oil to water velocity at the pipe of small diameter are higher than those at the pipe of big diameter when having same input flow rates. At low input water flow rate, there is a large deviation on the holdup between two flow systems with different oil viscosities and the deviation becomes gradually smaller with further increased input water flow rate.     

Experimental study on oil–water flow in horizontal and slightly inclined pipes

Oil–water two-phase flow experiments were conducted in a 15 m long, 8.28 cm diameter, inclinable steel pipe using mineral oil (density of 830 kg/m³ and viscosity of 7.5 mPa s) and brine (density of 1060 kg/m³ and viscosity of 0.8 mPa s). Steady-state data on flow patterns, two-phase pressure gradient and holdup were obtained over the entire range of flow rates for pipe inclinations of −5°, −2°, −1.5°, 0°, 1°, 2° and 5°. The characterization of flow patterns and identification of their boundaries was achieved via observation of recorded movies and by analysis of the relative deviation from the homogeneous behavior. A stratified wavy flow pattern with no mixing at the interface was identified in downward and upward flow. Two gamma-ray densitometers allowed for accurate measurement of the absolute in situ volumetric fraction (holdup) of each phase for all flow patterns. Extensive results of holdup and two-phase pressure gradient as a function of the superficial velocities, flow pattern and inclinations are reported. The new experimental data are compared with results of a flow pattern dependent prediction model, which uses the area-averaged steady-state two-fluid model for stratified flow and the homogeneous model for dispersed flow. Prediction accuracies for oil/water holdups and pressure gradients are presented as function of pipe inclination for all flow patterns observed. There is scope for improvement for in particular dual-continuous flow patterns.     

Nitrogen/non-Newtonian fluid two-phase upward flow in non-circular microchannels

This paper presents experimental investigations on nitrogen/non-Newtonian fluid two-phase flow in vertical noncircular microchannels, which have square or triangular cross-section with the hydraulic diameters being D_h = 2.5, 2.886 and 0.866 mm, respectively, by visualization method. Three non-Newtonian aqueous solutions with typical rheological properties, i.e., 0.4% carboxymethyl cellulose (CMC), 0.2% polyacrylamide (PAM) and 0.2% xanthan gum (XG) are chosen as the working fluids. The common flow patterns are identified as slug flow, churn flow and annular flow. The dispersed bubble flow is only found in the case with nitrogen/CMC solution two-phase flow in the largest channel. A new flow pattern of nitrogen/PAM solution two-phase flow, named chained bubble/slug flow, is observed in all the test channels. The flow regime maps are also developed and the results show that the rheological properties of the non-Newtonian fluid have remarkable influence on the flow pattern transitions. The geometrical factors of the microchannel such as the cross-section shape and hydraulic diameter of the channel can also affect the flow regime map. Finally, the results obtained in this work are compared with the available flow pattern transitions.     

Experimental study on a two-phase critical flow with a non-condensable gas at high pressure conditions

An experimental study was performed on a two-phase critical flow with a non-condensable gas at high pressure conditions. Experimental data for the critical flow rates were generated by using sharp-edged stainless steel pipes with an inner diameter of 10.9 mm, a thickness of 3.2 mm, and a length of 1000 mm. The test conditions were varied by using the stagnation pressures of 4.0, 7.0, and 10.0 MPa, water subcoolings of 0.0, 20.0, and 50.0 °C, and nitrogen gas flow rates of 0.0–0.22 kg/s. The experimental results show that the critical mass flux decreases rapidly with an increase of the volumetric non-condensable gas fraction. Also the critical mass flux increases with an increase of the stagnation pressure and a decrease of the stagnation temperature. An empirical correlation of the non-dimensional critical mass flux, which is expressed as an exponential function of the non-condensable gas fraction of the volumetric flow, is obtained from the experimental data.     

An appraisal of liquid–liquid slug flow in different pipe orientations

Gas–liquid slug flow occurs over a wide range of phase flow rates and in a variety of practical applications during gas–liquid two-phase flows. The range of slug flow increases further in narrow pipes (<0.0254 m), undulated pipelines, riser tube, etc. On the other hand, the past literature shows that slug flow is rarely observed for liquid–liquid cases. In the present study, an interest was felt to investigate whether liquid–liquid slug flow occurs in situations known for excessive slugging in gas–liquid cases. For this, experiments have been performed in narrow (0.012 m ID) vertical and horizontal pipes and an undulated pipeline of 0.0254 m internal diameter where the V-shaped undulation comprises of an uphill and a downhill section between two horizontal pipes. The studies have been performed for both peak and valley orientation of the undulation. Kerosene and water have been selected as the test fluids and the optical probe technique has been used to supplement visual observations especially at higher flow rates. The studies have revealed the existence of the slug flow pattern over a wide range of phase flow rates in all the three geometries. Interestingly, it has been noted that the introduction of an undulation induces flow patterns which bear a closer resemblance to gas–liquid flows as compared to liquid–liquid flows through a horizontal pipe of 0.0254 m diameter.     

Multiphase drag reduction: Effect of eliminating slugs

Two-phase pressure drop measurements were taken for air/water mixtures in a 0.052-m diameter horizontal pipe with special focus on the superficial liquid velocity range of 0.03–1.2 m/s at superficial gas velocities of 3.8, 5.2, and 6.6 m/s. It was found that the addition of 400 ppm of sodium dodecyl sulfate (SDS) to the water reduced the pressure drop by 25–40% when compared to equal flow rates without SDS. The pressure drop reduction occurred where the SDS eliminated the occurrence of the intermittent flow present with water. It was also found that the same concentration of SDS had virtually no effect on single phase liquid pressure drop. The pressure drop reduction appears to be due solely to the suppression of intermittent flow patterns.     

Structures in gas–liquid churn flow in a large diameter vertical pipe

Gas–Liquid two phase co-current flow in a vertical riser with an internal diameter of 127 mm was investigated in the churn flow pattern. This paper presents detailed experimental data obtained using a Wire Mesh Sensor. It shows that the most obvious features of the flow are huge waves travelling on the liquid film. Wisps, large tendrils of liquid and the product of incomplete atomisation, which had previously detected in smaller diameter pipes, have also been found in the larger diameter pipe employed here. The output of the Wire Mesh Sensor has been used to determine the overall void fraction. When examined within a drift flux framework, it shows a distribution coefficient of ∼1, in contrast to data for lower gas flow rates. Film thickness time series extracted from the Wire Mesh Sensor output have been examined and the trends of mean film thickness, that of the base film and the wave peaks are presented and discussed. The occurrence of wisps and their frequencies have been quantified.     

Macro-to-microchannel transition in two-phase flow: Part 1 - Two-phase flow patterns and film thickness measurements

The classification of macroscale, mesoscale and microscale channels with respect to two-phase processes is still an open question. The main objective of this study focuses on investigating the macro-to-microscale transition during flow boiling in small scale channels of three different sizes with three different refrigerants over a range of saturation conditions to investigate the effects of channel confinement on two-phase flow patterns and liquid film stratification in a single circular horizontal channel (Part 2 covers the flow boiling heat transfer and critical heat flux). This paper presents the experimental two-phase flow pattern transition data together with a top/bottom liquid film thickness comparison for refrigerants R134a, R236fa and R245fa during flow boiling in small channels of 1.03, 2.20 and 3.04 mm diameter. Based on this work, an improved flow pattern map has been proposed by determining the flow patterns transitions existing under different conditions including the transition to macroscale slug/plug flow at a confinement number of Co ≈ 0.3-0.4. From the top/bottom liquid film thickness comparison results, it was observed that the gravity forces are fully suppressed and overcome by the surface tension and shear forces when the confinement number approaches 1, Co ≈ 1. Thus, as a new approximate rule, the lower threshold of macroscale flow is Co = 0.3-0.4 while the upper threshold of symmetric microscale flow is Co ≈ 1 with a transition (or mesoscale) region in-between.     

Heat transfer to air–water annular flow in a horizontal pipe

Two-phase air–water flow and heat transfer in a 25 mm internal diameter horizontal pipe were investigated experimentally. The water superficial velocity varied from 24.2 m/s to 41.5 m/s and the air superficial velocity varied from 0.02 m/s to 0.09 m/s. The aim of the study was to determine the heat transfer coefficient and its connection to flow pattern and liquid film thickness. The flow patterns were visualized using a high speed video camera, and the film thickness was measured by the conductive tomography technique. The heat transfer coefficient was calculated from the temperature measurements using the infrared thermography method. It was found that the heat transfer coefficient at the bottom of the pipe is up to three times higher than that at the top, and becomes more uniform around the pipe for higher air flow-rates. Correlations on local and average Nusselt number were obtained and compared to results reported in the literature. The behavior of local heat transfer coefficient was analyzed and the role of film thickness and flow pattern was clarified.