Disintegration of flows of superheated liquid films and jets

This paper represents results on investigating the dynamics of boiling and disintegration of superheated liquid films and jets. The first part deals with experimental study of boiling liquid outflow through short cylindrical and slit channels. Evolution of disintegration of a hot water jet flow is observed both at low and moderate superheating and at high and limit superheating, and also for vaporization mechanisms corresponding to these superheatings. Peculiarities of disintegration of jets through slit and cylindrical channels are noticed. Results on measuring the reactive thrust of the jet through a slit channel under different geometrical conditions behind the channel outlet are represented. The 1/f fluctuations in transient regimes of superheated liquid boiling and in transient regimes of behavior of the jet shape are found. The second part of this article represents results on experimental investigation of nonsteady heat transfer and dynamics of the development of crisis phenomena at boiling of a falling subcooled liquid film in the conditions of stepwise heat release. The experimental data were obtained using synchronized high-speed infrared thermography and video. It is shown that with growth and condensation of vapor bubbles, on the liquid film interface appear large-amplitude waves that lead to considerably increasing local intensity of heat transfer. New data on the boiling incipience temperature in a subcooled liquid film, depending on the heat flux density, are obtained. It is found that the development of boiling crisis is a result of appearance of local dry patches and their subsequent growth by the mechanism of longitudinal thermal conductivity in the heat transfer wall as the equilibrium heat flux density is exceeded.     

Phase field modeling of liquid jets in low gravity

An axisymmetric phase field model is developed and used to model surface tension forces on liquid jets in microgravity. The previous work in this area is reviewed and a baseline drop tower experiment selected for model comparison. The model is solved numerically with a compact fourth order stencil on an equally spaced axisymmetric grid. After grid convergence studies, a grid is selected and all drop tower tests modeled. Agreement was assessed by comparing predicted and measured free surface rise. Trend wise agreement is good but agreement in magnitude is only fair. Suspected sources of disagreement are the simple turbulence model and the existence of slosh baffles in the experiment that were not included in the model. Parametric investigation was conducted to study the influence of key parameters on the geysers formed by jets in microgravity. Investigation of the contact angle showed the expected trend of increasing contact angle increasing geyser height. Investigation of the tank radius showed some interesting effects and demonstrated the zone of free surface deformation is quite large. Variation of the surface tension with a laminar jet showed clearly the evolution of free surface shape with Weber number. A breakthrough Weber number of 1 was predicted by the variation of the surface tension model which is close to the experimentally measured Weber number of 1.5 found in prior experimental work.     

Instabilities and decay rates of charged viscous liquid jets

The eigenmodes and characteristic frequencies of surface deformations of real fluids in the geometry of a cylindrical jet, which is homogeneously charged, are calculated using the linearized Navier-Stokes equation with free surface boundary conditions. A stability phase diagram in the wavenumber-fissility plane is given. Two types of instabilities are described, surface tension and Coulomb force induced. The known modes for ideal potential flow are extended to arbitrary viscosity. In addition new types of modes are described (eigenfunctions and decay rates) which represent rotational flow and have no correspondence to Rayleigh's jet instability.     

A new particle method for simulating breakup of liquid jets

A corrected smoothed particle hydrodynamics (CSPH) method for simulating two-phase flows including surface tension is presented. The effects of the instability in the compressional regime and particle deficiency are suppressed by adopting a new smoothing kernel and its gradient corrections. The insensitivity to the compressional instability of the adopted method is confirmed by numerical tests. The method is validated and calibrated through a series of standard numerical tests and showed quantitative agreements. The method is extended to two-dimensional jet breakup problems and provided good comparison to the theoretical and experimental results. In particular, the numerical model exhibits the transition from the jetting to dripping when the Weber number is close to its theoretical critical value.     

Novel wet SEM imaging of organically modified montmorillonite clay dispersions

Rheology and a novel application of wet scanning electron microscopy (WSEM) are performed on organically modified montmorillonite clay dispersions differing in free surfactant content. The dispersion without free surfactant exhibits a higher yield stress and strongly hysteretic rheology. WSEM imaging shows the influence of free surfactant on the quiescent distribution of nano- and microscale organoclay domains. Spatially resolved elemental analysis using energy dispersive X-ray spectroscopy defines regions consisting primarily of clay silicate versus those that are dominantly solvent. The contrasting images suggest that free surfactant screens attractive van der Waals forces between domains, leading to a more homogeneously distributed but structurally weaker mesoscopic network. WSEM is shown to be a valuable complementary technique in characterizing the network morphology of organoclay dispersions. More broadly, WSEM demonstrates great potential for the direct imaging of the microstructure of other classes of suspensions and particulate gels. PACS  61.16.Bg; 82.70.Uv; 82.70.Dd; 83.60.Pq; 83.80.Hj     

Electron channelling contrast imaging of dislocations in a conventional SEM

Abstract

Dislocations in shock loaded tantalum single crystals were imaged using both transmission electron microscope (TEM) and electron channelling contrast image (ECCI) in a scanning electron microscope with a conventional backscattered electron detector. The results were compared with backscattered electron intensity profiles across dislocations calculated via the dynamic theory of electron diffraction. A one-to-one correspondence between ECCI and TEM is established. High voltage and low index reflections should be used to obtain the highest dislocation contrast and greatest imaging depth.     

Nonlinear instability of charged liquid jets: Effect of interfacial charge relaxation

A linear and nonlinear study has been made of cylindrical interface, carrying a uniform surface charge in the presence of a finite rate of charge relaxation, is investigated by using multiple scales method. The linear stability flow is analyzed by deriving a dispersion relation for the growth waves, and solving it analytically and numerically to find marginal stability curves. We investigate the electric charge relaxation effects on the stability of the flow by considering various limiting cases. We also examine the effects of finite charge relaxation times in axisymmetric and nonaxisymmetric modes. In the nonlinear approach, it is shown that the evolution of the amplitude is governed by a Ginzburg–Landau equation. There is also obtained a nonlinear modified Schrödinger equation describing the evolution of wave packets for small charge relaxation time. Further, the classic Schrödinger equation is obtained when the influence of relaxation time charge is neglected. On the other hand, the complex amplitude of quasi-monochromatic standing waves near the cutoff wavenumber is governed by a similarly type of nonlinear Schrödinger equation in which the roles of time and space are interchanged. This equation makes it possible to estimate the nonlinear effect on the cutoff wavenumber. The nonlinear theory, when used to investigate the stability of charged liquid jet, appears accurately to predict a new unstable regions. The effects of the surface charge and charge relaxation on the stability are identified. The various stability criteria are discussed both analytically and numerically and the stability diagrams are obtained.     

Breakup of elliptical liquid jets in gaseous crossflows at low Weber numbers

Journal of Visualization - Breakup of circular and elliptical liquid jets in subsonic gaseous crossflows is experimentally studied using shadowgraph technique. The experiments are performed at...     

Equilibrium shape and hysteresis behavior of liquid jets in transverse electric fields

The stability of a liquid jet subject to a transverse electric field is investigated in the framework of electrohydrostatic theory. It is shown that depending on the magnitude of permittivity ratio of the involved fluids S = ε_i/ε_o (inner to outer) compared to a critical permittivity ratio S_cr ≈ 27.45 the jet exhibits distinct behaviors; for S < S_cr the jet is stable and elongates indefinitely as the electric field is increased, while for S > S_cr it shows hysteresis behavior and becomes unstable beyond a critical electric capillary number Ca_cr. The results suggest that the jets are generally more stable than liquid drops.     

Nonlinear electrohydrodynamic phenomena and droplet generation in charged jets of conducting liquid

Phenomena occurring at the tip of a charged conducting jet are analyzed in detail using numerical methods developed for axially symmetric flows. Universal mechanisms (independent of the method for producing the jet) for droplet formation with different ratios of the Laplace and electrical pressures on the lateral surface are identified. An explanatory analysis is given for all of the nonlinear stages of the classical Rayleigh instability of a charged conducting drop, beginning with the formation of a jet at the surface of the drop and culminating in the generation of a developed jet of secondary droplets. Zh. Tekh. Fiz. 69, 1–9 (November 1999)     

Equilibrium configurations of uncharged conducting liquid jets in a transverse electric field

Solutions for the problem on the equilibrium configurations of uncharged conducting liquid jets in a transverse electric field are obtained. These solutions correspond to finite-amplitude non-axisymmetric azimuthal deformations of the surface of a round jet: the jet is stretched along the field in its cross-section. The range of electric fields is determined for which solutions of the problem exist. If the electric field strength is over some critical value, the electrostatic equations have no solution, and the jet splits. The obtained solutions are qualitatively examined for stability under small azimuthal perturbations.     

Multi-kHz mixture fraction imaging in turbulent jets using planar Rayleigh scattering

In this study, we describe the development of two-dimensional, high repetition-rate (10-kHz) Rayleigh scattering imaging as applied to turbulent flows. In particular, we report what we believe to be the first sets of high-speed 2D Rayleigh scattering images in turbulent non-reacting jets, yielding temporally correlated image sequences of the instantaneous mixture fraction field. Results are presented for turbulent jets of propane issuing into a low-speed co-flow of air at jet-exit Reynolds numbers of 10,000, 15,000, and 30,000 at various axial positions downstream of the jet exit. The quantitative high-speed mixture fraction measurements are facilitated by the use of a calibrated, un-intensified, high-resolution CMOS camera in conjunction with a unique high-energy, high-repetition rate pulse-burst laser system (PBLS) at Ohio State, which yields output energies of ∼200 mJ/pulse at 532 nm with 100-μs laser pulse spacing. The quality, accuracy, and resolution of the imaging system and the resulting image sets are assessed by (1) comparing the mean mixture fraction results to known scaling laws for turbulent jets, (2) comparing instantaneous images/mixture fraction profiles acquired simultaneously with the high-speed CMOS camera and a well-characterized, high-quantum efficiency CCD camera, and (3) comparing statistical quantities such as the probability density function of the mixture fraction results using the high-speed CMOS camera and the CCD camera. Results indicate accurate mixture fraction measurements and a high potential for accurately measuring mixture fraction gradients in both time and space.     

Estimation of SEM imaging resolution of the domain structure of pyroprobe-heated ferroelectrics

The specific contrast of scanning electron microscope (SEM) images of ferroelectric domains observed in the pyrocurrent (pyroprobe) mode is analyzed. Calculations taking into account both the nonuniform heating of domains and the heat diffusion via the domain walls and the crystal boundaries are performed. It is established that the heat diffusion smears the domain images of small domains. Along with the probe diameter, the scan rate is shown to be an important factor determining the character of the SEM image contrast. A decrease in the scan rate may appreciably lower the resolution even in case of a fairly thin probe.     

Backscattered electron imaging of micro- and nanostructures: 5. SEM signal formation model

A semiempirical model describing how images are formed in a scanning electron microscope operating in the backscattered electron collection mode is discussed. The model involves four imaging mechanisms. The model and the experiment are compared for grooves in silicon with rectangular and trapezoidal relief profiles.     

High spatial resolution surface imaging and analysis of fungal cells using SEM and AFM

We review the use of scanning electron microscopy (SEM), atomic force microscopy (AFM) and force spectroscopy (FS) for probing the ultrastructure, chemistry, physical characteristics and motion of fungal cells. When first developed, SEM was used to image fixed/dehydrated/gold coated specimens, but here we describe more recent SEM developments as they apply to fungal cells. CryoSEM offers high resolution for frozen fungal samples, whereas environmental SEM allows the analysis of robust samples (e.g. spores) under ambient conditions. Dual beam SEM, the most recently developed, adds manipulation capabilities along with element detection. AFM has similar lateral and better depth resolution compared to SEM, and can image live cells including growing fungal hyphae. FS can analyze cell wall chemistry, elasticity and dynamic cell characteristics. The integration of AFM with optical microscopy will allow examination of individual molecules or cellular structures in the context of fungal cell architecture. SEM and AFM are complementary techniques that are clarifying our understanding of fungal biology.     

Cosmic jets

We discuss time-dependent gravitational fields that “accelerate” free test particles to the speed of light resulting in cosmic double-jet configurations. It turns out that complete gravitational collapse along a spatial axis together with corresponding expansion along the other two axes leads to the accelerated motion of free test particles up and down parallel to the collapse axis such that a double-jet pattern is asymptotically formed with respect to the collapsed configuration.     

Appearance of poststenotic jets in MRI: dependence on flow velocity and on imaging parameters

A flow model was used to study the appearance of poststenotic jets in MRI. Jets in CuSO4-doped water and bovine blood were imaged by spin-echo (SE) and fast-field-echo (FFE) pulse sequences at different degrees of stenosis and various flow rates. On flow-compensated FFE images, the jets were characterized by signal void if the mean flow velocity within the stenosis exceeded a limit, which was independent of the degree of the stenosis and the type of the fluid. On SE images and on FFE images without flow compensation, signal void occurred at significantly lower flow velocity. The extension of the poststenotic signal void on flow-compensated FFE images was increased by either reduction of the pixel diameter or by prolongation of the echo time. However, it was independent of the orientation of the imaging plane relative to the direction of flow. The results have an impact on attempts to use signal void for the assessment of turbulent jets with MRI.