共查询到18条相似文献,搜索用时 62 毫秒
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Nd:LuVO4晶体的生长及其性能研究 总被引:2,自引:0,他引:2
采用提拉(Czochralski)法生长了Nd:LuVO4晶体.利用液相反应法,以V2O5和NH4OH生成NH4VO3,Nd2O3、Lu2O3和HNO3生成Nd(NO3)3和Lu(NO3)3反应制备多晶料;所生长Nd0.01Lu0.99VO4晶体为16×20×21 mm3,质量超过40g.以X射线荧光分析仪测得其生长中各主要元素的分凝系数.其中Nd3+约为0.91,V3+和Lu3+接近1.还测定了其介电常数ε11=27.2,ε33=33.9(30℃,1kHz),以同步辐射X射线白光形貌术观察了其内部质量. 相似文献
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Nd:GdVO4激光晶体的光谱性质和热学性质 总被引:1,自引:2,他引:1
用提拉法生长了Nd:GdVO4单晶,测量了其室温吸收谱和室温荧光谱,测量了其热扩散系数α和比热Cp,从而得到了其热导率λ。可以看到Nd:GdVO4晶体的吸收波长在808nm附近,与已经商品化的GaAlAs LD的发射波长能很好地匹配,从而增加了吸收效率,并且Nd:GdVO4晶体具有较高的热导率,有望在高功率的激光系统中获得应用。所以Nd:GdVO4晶体是理想的激光材料。 相似文献
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用群论的方法计算了Nd:YbVO4晶体的拉曼活性振动模数目,在室温下测得了其极化拉曼谱线,并指认了在不同几何配置下,各振动模式所对应的频率.同时,测得了室温下晶体的吸收谱,得到了中心波长为808 nm吸收峰的半高宽为12 nm,并在J-O理论的基础上计算了晶体的光学参数,其三个晶场参数分别为Ω2=6.88945×10-20 cm2、Ω4=4.13394×10-20 cm2、Ω6= 4.54503×10-20 cm2,并由此得到4F3/2能级的荧光寿命为178.69 μs,1062 nm处的荧光分支比为48.85;,积分发射截面为2.7867 10-18 cm2.分别在808 nm、940 nm激发下测得晶体室温发射谱,观察到了Nd→Yb以及Nd←Yb间的能量传递现象. 相似文献
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采用提拉法沿a轴和c轴生长出无色透明的GdVO4单晶,质量均超过50g.用X射线荧光分析法测得两个主要元素Gd和V的分凝系数都接近1.室温下测量了GdVO4晶体的X射线粉末衍射图,确定所获GdVO4晶体属于四方晶系,D194h-I41/amd空间群.通过晶体的锥光干涉图确定GdVO4晶体为单轴晶,光轴方向平行于c轴且光学均匀性比较好.利用高分辨X射线衍射仪测量GdVO4晶体的摇摆曲线,结果表明生长的GdVO4晶体的晶格完整性较好.通过浮力法测得其室温下密度为5.478g/cm3.透过波谱表明透过波长大于340nm. 相似文献
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利用商群对称分析法分析了Nd:LuVO4晶体的晶格振动模分类,测量了Nd:LuVO4晶体的红外光谱和拉曼光谱,从测定的谱线中指认了该晶体的振动模,理论与实验符合良好.测量了Nd:LuVO4晶体的热膨胀系数,a向、b向和c向的热膨胀系数分别为 1.7×10-7/K 、1.5×10-7/K和9.1×10-7/K.测量了比热,其值约为0.48J/g·K.测量了热传导率,其值沿<100>方向为6.2W/m·K,沿<001>方向为7.9W/m·K.这些参数显示该晶体是一种热学性能优良的激光晶体. 相似文献
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采用固-液两相混合,使Nd2o3、Y2O3和V2O5在近常温条件下初步合成Nd:YVO4多晶原料,降低固相合成反应温度,减少V2O5在多晶原料制备过程中的挥发。讨论了α方向V单晶生长条件,采用提拉法,以(100)方向进行单晶生长,得到一系列掺杂浓度的Nd:YVO4单晶。 相似文献
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Nd:GdVO_4热常数的测量和激光性能研究 总被引:2,自引:0,他引:2
中频感应加热提拉法生长了低钕掺杂的GdVO_4晶体,用机械分析仪来测量Nd:GdVO_4晶体的热膨胀系数,沿c方向的热膨胀系数为7.42×10~(-6)/K,而沿α方向的热膨胀系数只有1.05×10~(-6)/K,比同比Nd_(0.0045)Y_(0.9946)VO_4晶体样品测量结果小。差示扫描热计法测量了Nd:GdVO_4晶体的比热,298K时为0.52J/g·K。首次用激光脉冲法测量了Nd:GdVO_4晶体的室温热导率。实验表明,Nd:GdVO_4晶体沿<001>方向的热导率数值达11.4W/m·K,比Nd:YAG晶体高(测得10.7W/m·K),其<100>方向的热导率为10.1W/m·K。激光实验显示在较高功率泵浦激光输出上Nd:GdVO_4晶体具有比Nd:YVO_4晶体更加优良的性能。 相似文献
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Nd∶NaY(WO4)2激光晶体生长 总被引:7,自引:0,他引:7
采用提拉法生长出了四方晶系白钨矿结构的Nd:NaY(WO4)2(简称Nd∶NYW)激光晶体,尺寸为20mm×30mm.通过TG-DTA差热分析得到晶体的熔点为1211℃,从XRD分析得到晶胞参数为a=b=0.5212nm ,c=1.1268nm ,晶胞体积V=0.3062nm3.讨论了Nd∶NYW晶体的生长工艺,给出了晶体生长的最佳工艺参数.通过比较Nd∶NaBi(WO4)2(简称Nd∶NBW)和Nd:NYW的XRD、红外光谱和拉曼光谱测试结果,认为二者结构基本相同,为四方晶系白钨矿结构、I(4)空间群. 相似文献
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L. J. Qin X. L. Meng C. L. Du Z. S. Shao L. Zhu B. C. Xu H. J. Zhang 《Crystal Research and Technology》2002,37(9):913-920
A new liquid‐phase method synthesizing Nd:GdVO4 polycrystalline materials was introduced. High optical quality Nd:GdVO4 single crystals have been successfully grown by the Czochralski method. The effective segregation coefficients of Nd ion in Nd:GdVO4 crystal have been measured and discussed. Laser outputs at 1.06 μm and at 1.34 μm were achieved when Nd:GdVO4 crystal samples of 0.52 at% Nd concentration were pumped by a high‐power LD. A maximum output of 14.5 W at 1.06 μm has been obtained when the pump power is to 26 W, giving the slope efficiency of 63%. It is reported the first time that up to 4.64 W power laser at 1.34 μm has been achieved with optical conversion efficiency of 31.4% and slope efficiency of 32.9%. 相似文献
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Donggang Ran Hairui Xia Shangqian Sun Fengqin Liu Zongcheng Ling Wenwei Ge Huaijin Zhang Jiyang Wang 《Crystal Research and Technology》2007,42(9):920-925
A Nd‐doped lutetium orthovanadate Nd:LuVO4 crystal has been grown using a modified Czochralski method. The thermal properties of this crystal have been studied by measuring the thermal expansion, specific heat and thermal diffusivity. The thermal expansion coefficients are α11 = 1.7 × 10‐6, α22 = 1.5 × 10‐6 and α33 = 9.1 × 10‐6/K in the temperature range of 298–573 K along the three respective crystallographic axes. The specific heat is almost linear and increases from 0.442 to 0.498 Jg‐1K‐1 in the measured temperature range. The thermal diffusivity is anisotropic and decreases with increasing temperature from 295 to 548 K. At room temperature the calculated thermal conductivities κ11 and κ33 are 7.96 and 9.77 Wm‐1K‐1, respectively. These thermal parameters of Nd:LuVO4 crystal have indicated that it is an excellent candidate laser material. (© 2007 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
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H. J. Zhang L. Zhu X. L. Meng Z. H. Yang C. Q. Wang W. T. Yu Y. T. Chow M. K. Lu 《Crystal Research and Technology》1999,34(8):1011-1016
Nd:YVO4 crystal has been grown by Czochralski method. The data of thermal expansion and specific heat have been measured. The thermal expansion coefficients along a- and c-axis are a1 = 2.2 x 10-6 /K, and a3 = 8.4 x 10-6 /K respectively. The specific heat is 24.6 cal/mol x K at 330 K. The large anisotropy along c- and a-axis of thermal expansion coefficients is explained by the structure of YVO4 crystal. 921 mW output laser at 1.06 mikrom has been obtained with a 3 mm x 3 mm x 1mm crystal sample when pumped by 1840 mW cw laser diode, and the slope efficiency is 55.5%. 相似文献
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