基于包层模的光纤布拉格光栅折射率传感特性

提出了基于光纤布拉格光栅(FBG)包层模式的折射率传感方案。实验中,利用不同浓度的丙三醇水溶液作为外界折射率传感溶液,采用氢氟酸溶液化学腐蚀的方法来减小光纤包层的直径以增大包层模式对外界折射率的敏感度,研究了腐蚀后光纤布拉格光栅包层模式的耦合波长对外部折射率的变化关系。实验结果表明在1.3300~1.4584的折射率范围内,包层模式耦合波长随外界折射率增大而增大,在接近光纤包层折射率处具有很高的折射率灵敏度,最大达到了172 nm/riu(refractive index unit)。而且,包层模谐振的光谱半峰全宽(约0.07 nm)仅为布拉格纤芯模谐振光谱半峰全宽的1/4,能够获得更好的传感精度。     

Optical refractometer based on large-core air-clad photonic crystal fibers

A large-core air-clad photonic crystal fiber-based sensing structure is described, which is sensitive to refractive index. The sensing head is based on multimodal interference, and relies on a single-mode/large-core air-clad photonic crystal fiber (PCF)/single-mode fiber configuration. Using two distinct large-core air-clad PCF geometries-one for refractive index measurement and the other for temperature compensation, it was possible to implement a sensing head sensitive to refractive index changes in water as induced by temperature variations. The results indicated the high sensitivity of this sensing head to refractive index variations of water, and a resolution of 3.4×10(-5) refractive index units could be achieved.     

Experimental research of liquid refractive index sensing by optical fiber and colloidal crystal's photonic band-gap

We use the changes of colloidal photonic crystal photonic band-gap center wavelength to research the refractive index sensing by experiment. The changes in the center wavelength of the colloidal crystals photonic band-gap are analyzed. A mold is designed to obtain a controllable self-assembly method, colloidal crystals are observed by scan electronic microscope (SEM) and the band-gap is measured by infrared spectrometer. The results are agreed well with the theoretical analysis. An experimental device is designed to test liquid refractive index. The couple of the fibers are used to measure the band-gap of colloidal crystals and the results are also discussed in theory. The results show that the band-gap of colloidal crystals can be used to measure the liquid refractive index. The new sensing mechanism is formed and it provides a new application of colloidal crystals in the sensing.     

A novel plasmonic refractive index sensor based on gold/silicon complementary grating structure

A novel complementary grating structure is proposed for plasmonic refractive index sensing due to its strong resonance at near-infrared wavelength.The reflection spectra and the electric field distributions are obtained via the finite-difference time-domain method.Numerical simulation results show that multiple surface plasmon resonance modes can be excited in this novel structure.Subsequently,one of the resonance modes shows appreciable potential in refractive index sensing due to its wide range of action with the environment of the analyte.After optimizing the grating geometric variables of the structure,the designed structure shows the stable sensing performance with a high refractive index sensitivity of 1642 nm per refractive index unit(nm/RIU)and the figure of merit of 409 RIU^-1.The promising simulation results indicate that such a sensor has a broad application prospect in biochemistry.     

Design of a coated thinly clad chalcogenide long-period fiber grating refractive index sensor based on dual-peak resonance near the phase matching turning point

A novel method for designing chalcogenide long-period fiber grating (LPFG) sensors based on the dual-peak resonance effect of the LPFG near the phase matching turning point (PMTP) is presented. Refractive index sensing in a high-refractive-index chalcogenide fiber is achieved with a coated thinly clad film. The dual-peak resonant characteristics near the PMTP and the refractive index sensing properties of the LPFG are analyzed first by the phase-matching condition of the LPFG. The effects of film parameters and cladding radius on the sensitivity of refractive index sensing are further discussed. The sensor is optimized by selecting the appropriate film parameters and cladding radius. Simulation results show that the ambient refractive index sensitivity of a dual-peak coated thinly clad chalcogenide LPFG at the PMTP can be 2400 nm/RIU, which is significantly higher than that of non-optimized gratings. It has great application potential in the field of chemical sensing and biosensors.     

负折射率材料用于表面波传感的特性分析

利用严格电磁理论分析了负折射材料界面上激励表面波的相关特性,证明两种偏振入射都能在负折射材料与正折射材料界面上激发表面波,并推导出了相应表面波的传播波矢和激发条件.针对负折射材料在表面波传感方面的应用,对膜厚选择,偏振态,测量范围,线性度等性能参量进行了具体分析,与传统的金属表面等离子波传感器相比,使用负折射材料在灵敏度相当的情况下,能有效提高线性度,增大测量范围,提高信噪比.     

基于无芯光纤的多参数测量传感器

设计并制作了一种基于单模-无芯-单模-无芯-单模光纤结构的马赫-曾德尔传感器,可用来同时测量折射率和温度.该传感器中,两处无芯光纤充当输入、输出耦合器,中间单模光纤作为传感臂.利用有限元仿真和理论分析,确定耦合器和传感臂的最优长度为15 mm.在无芯光纤中激发出的高阶模进入单模光纤的包层传输,由于倏逝场的作用,受到环境折射率和温度的影响.选取透射谱不同干涉级次的波谷作为研究对象,实现了折射率和温度的同步测量.实验结果表明:1545 nm附近干涉谷的折射率和温度灵敏度分别为–153.89 nm/RIU(refractive index unit)和0.166 nm/℃;1570 nm附近干涉谷的折射率和温度灵敏度分别为–202.74 nm/RIU和0.183 nm/℃.该传感器在实现折射率和温度同步测量的同时,仍能保持较高灵敏度,在生物医疗等方面有着较好的应用前景.     

表面覆膜波导光栅共振光谱特性及传感机理分析

基于波导光栅共振原理和古斯-汉欣(Goos-Hänchen)位移理论,提出一种表面覆膜波导光栅传感结构,并研究其共振光谱特性。通过在光栅表面涂覆低折射率聚合物功能膜层优化其共振光谱特性,选用多孔硅作为待测物承载单元,可以使光学探针更充分地接触待测样本,从而提高其检测性能。根据波导光栅共振相位条件,建立了共振波长和样本折射率之间的数学模型,通过检测共振位置的改变进而对样本浓度进行检测。研究表明,该表面覆膜波导光栅传感结构具有线型对称和窄线宽的共振光谱特性,可实现高品质因数(Q值)和高灵敏度的传感特性,其Q值为1 488,对折射率的检测极限可达5×10-4 RIU(RIU为折射率单位)。通过检测不同浓度的葡萄糖溶液对其传感特性进行验证分析,结果表明,共振波长与葡萄糖溶液浓度之间具有良好的线性关系,对葡萄糖溶液的检测灵敏度为1.12nm/1%,证明了该表面覆膜波导光栅传感结构的有效性,可以用于对低浓度样本溶液的实时动态监测,并为波长调制型光学折射率传感器的研究提供理论指导。     

The measurement of sucrose concentration by two-tapered all-fiber Mach–Zehnder interferometer employing different coupling structures and manufacture processes

The sucrose concentration measurement and characteristics of light coupling taper structure on sensitivity with various fabrication processes of taper structure for all-fiber Mach–Zehnder interferometer (AFMZI) are presented. Using fusion splicer with electrical discharge, the standard single-mode fiber is employed to be fabricated as conical coupling/decoupling taper structure. The basic two fabrication processes are designed as single fusion-stretching (SFS), multiple fusions without stretching (MF). The third advanced process is composed of SFS and multiple fusions without stretching processes, and called multiple fusions with single stretching (MFSS). Various types of coupling/decoupling taper structures were fabricated based on the three kinds of fabrication processes. The effects of geometry shape including taper waist, taper angle, and sensing length on sensing sensitivity of AFMZIs are estimated. The modifications of fiber core and cladding induced by thermal effect affect the refractive index distributions and shapes of taper structure. The effects of refractive index changes of fiber core and cladding on sensing sensitivity are also discussed. The AFMZI was tested by measuring aqueous sucrose solution of refractive index unit (RIU) from 1.333 to 1.420 RIU. The optical spectrums are measured by a spectrometer. The spectrum dip shifts and sensing sensitivity was measured and calculated, respectively. As shown in results, sensing sensitivities of AFMZIs of taper structure fabricated by MFSS and multiple fusions without stretching processing are generally higher than SFS. The reasons could be aimed on materials modification through thermal effect on blurring fiber core-cladding interface and proper taper angle of taper structure. The more homogeneous refractive index distribution on fiber core-cladding interface, the more detecting light power decoupled through core-cladding interface to interact with exterior environment and enhance the sensing sensitivity. Similarly, an appropriate taper angle also provides a better coupling/decoupling performance. The optimal sensitivities relative to low refractive index, high refractive index, and full refractive index range are 87.62, 133.55, and 104.20 nm/RIU, respectively, and the corresponding sensing length are 30, 50, and 30 mm, respectively, with taper angle of 25° and taper waist of 40 μm.     

工字形太赫兹超材料吸波体的传感特性研究

利用超材料吸波体对材料参数的电磁响应, 可将其应用于传感. 本文设计了一种工字形单元结构的超材料吸波体, 基于频域算法对其在太赫兹频段的传感特性进行数值模拟, 研究了待测样品折射率、厚度及电介质隔层厚度对超材料吸波体传感器的频率灵敏度、振幅灵敏度及品质因数的影响. 研究结果表明:当待测样品厚度为40 μm时, 折射率频率灵敏度可达到153.17 GHz/RIU, 折射率振幅灵敏度可达到41.37%/RIU; 待测样品折射率一定时, 厚度频率灵敏度随其厚度的增大而线性减小; 随着待测样品厚度的增加, RFOM呈增大趋势, 但增大幅度在逐渐减小; TFOM随待测样品厚度的增加而减小.     

长周期光纤光栅的折射率敏感特性

利用光波导的耦合模理论分析了长周期光纤光栅(LPFG)的折射率传感特性,给出了LPFG 的谐振波长相对于环境折射率变化时的漂移量解析表达式.对 LPFG 的折射率传感特性进行了数值模拟.结果表明:在光栅周期不变的情况下,当包层折射率小于且接近外界环境折射率时,波长的漂移量增大,且对应的模次越高、包层半径越小、包层折射率越小,波长漂移量越大,即 LPFG 对应于外界折射率传感灵敏度得到显著提高;当外界环境折射率大于包层折射率时,光栅的谐振波长将近似不变.     

带多孔硅表面缺陷腔的半无限光子晶体Tamm态及其折射率传感机理

结合表面缺陷半无限光子晶体Tamm态与多孔硅光学传感机理,在光子晶体表面缺陷腔中引入多孔硅,并利用其高效的承载机制,提出基于多孔硅表面缺陷光子晶体Tamm态的折射率传感结构.在半无限光子晶体中缺陷腔与原来的周期性分层介质结构的界面上存在Tamm态,通过入射角度调制使其在缺陷腔中实现多次全反射,并在缺陷腔中加入吸收介质,使谐振波长在缺陷腔中完成衰荡,从而在反射谱中得到缺陷峰;调整光子晶体参数,使缺陷峰的半高全宽得到优化,提高其品质因数(Q值);在此基础上,根据Goos-H?nchen相位移与谐振波长的关系,建立由待测样本折射率改变所导致的多孔硅表面吸附层有效折射率变化与缺陷峰值波长漂移之间的关系模型,并分析其折射率传感特性.结果表明,此生物传感结构Q值为1429,灵敏度为546.67 nm/RIU,证明了该传感结构的有效性,可为高Q值和高灵敏度折射率传感器的设计提供一定的理论参考.     

波长调制型表面等离子体共振的传感特性研究

表面等离子体共振(SPR)光学传感器能实现生物医学的快速、 无标记、 高精度检测,是生物化学分析的重要方法。 研制了基于波长调制型的Kretschmann结构表面等离子体共振(SPR)生物传感系统,研究了在体溶液传感方式下的传感性能。 利用不同浓度的乙醇和乙二醇溶液进行体溶液传感测试。 实验结果表明,在折射率低时共振波长对折射率变化响应的灵敏度低,但响应的线性度高;随着折射率增大,共振波长对折射率的响应变化的灵敏度提高。 在1.407 0～1.430 RIU折射率范围内,灵敏度高达11 487 nm·RIU-1。 传感器的共振波长的稳定性为0.213 8 nm,可分辨最小折射率趋近10-6 RIU。 所研制的波长调制型表面等离子共振传感器操作简单、 灵敏度高、 检测范围大,可实现浓度极低生物标记物的有效检测,在化学、 生物传感领域有重要的应用。     

基于SM-NCF反射光谱辨识的液体折射率监测方法

针对分子生物学与环境监测领域高灵敏度特异性检测需求,提出一种基于反射光谱特征辨识的单端反射式光纤折射率传感器模型,并给出了这种基于多模干涉原理的单模光纤-无芯光纤(Single mode fiber-No core fiber, SM-NCF)串接结构传感机理及其理论模型。无芯光纤实质上是一种结构特殊的多模光纤,在实际应用中无芯光纤结构本身作为纤芯,外界环境介质当作包层,构成光波导结构。这与普通多模光纤相比,不需要采用氢氟酸对多模光纤的包层进行化学腐蚀,不会降低光纤的机械性能,也不会破坏芯模传输条件,可以更好的实现对周围环境折射率的传感监测。当无芯光纤所处外界环境折射率发生改变时,其波导结构和包层有效折射率均会发生改变,从而引起传输光信号的纵向传播常数和模场分布也会随之发生改变,最终导致不同波长对应传输光功率的变化。上述效应反映在反射光谱上,即干涉波谷对应的谐振波长、波谷峰值强度以及半波宽度发生相应变化,通过辨识该反射光谱特征就可实现对外界环境折射率的测量。借助光束传播法(BPM),数值模拟得到无芯光纤长度分别为自映像距离和非自映像距离时的SM-NCF内部光场能量分布规律,并制作了无芯光纤长度分别为自映像距离和非自映像距离的SM-NCF光纤折射率传感探头,将作为传感区域的无芯光纤一端与标准单模光纤熔接,采用磁控溅射技术在无芯光纤另一端面镀上金膜,用以提升反射光谱强度。在此基础上,搭建了基于SM-NCF终端反射型的光纤折射率试验系统,并开展了相关实验研究。研究结果表明,当无芯光纤长度是15 mm(自映像距离)时,随着液体折射率从1.331 5依次增大至1.390 2,SM-NCF反射光谱逐渐向长波方向偏移,其反射峰谐振波长对应的折射率灵敏度约为197.57 nm·RIU-1,相关系数为0.93;反射峰值强度也呈现逐渐降低趋势,其折射率灵敏度约为-62.80 dB·RIU-1。当无芯光纤长度是20 mm(非自映像距离)时,随着液体折射率依次增大,SM-NCF反射光谱呈现明显双峰现象,且均逐渐向长波方向偏移,dip2谐振峰波长折射率灵敏度约为133 nm·RIU-1,相关系数为0.96;反射峰值强度也呈现逐渐降低趋势,其折射率灵敏度约为-31.66 dB·RIU-1。对比分析可知,不论是从反射峰谐振波长偏移的角度,还是从反射峰值强度的角度,自映像距离长度对应的 SM-NCF终端反射型光纤传感器均具有较高灵敏度。对于相同折射率液体环境,非自映像距离长度对应的SM-NCF反射光谱半波宽度与自映像距离长度相比,呈现显著变窄趋势。相对于SMS透射型传感结构,当传感区域长度相同时,SM-NCF反射型结构能够实现对光波信号的往返两次调节。这种终端反射型SM-NCF传感器改进了传统透射型折射率传感器不便与待测液体相接触的缺点,具有结构简单、易于制作、抗电磁干扰能力强以及便于远程遥测等优点,能够为后续生化与环保监测领域研究应用提供有益支持。     

基于表面等离子体共振和定向耦合的D形光子晶体光纤折射率和温度传感器

利用光子晶体光纤结构的灵活性和性能的优越性, 设计了一种基于D形光子晶体光纤的折射率和温度传感器. 在D形光子晶体光纤表面抛磨并镀上金纳米薄膜, 作为表面等离子体共振传感通道用来测量液体折射率; 在包层的一个空气孔中填充温敏液体甲苯, 作为定向耦合通道实现对温度的测量. 进一步的数值计算发现, 基于定向耦合效应的温度传感和基于表面等离子体共振的折射率传感相互独立, D形光子晶体光纤同时进行折射率和温度传感检测. 在各向异性的完美匹配层边界条件下利用全矢量有限元法对该传感器特性进行了数值研究, 发现D形光子晶体光纤的空气孔直径决定了定向耦合吸收峰的中心波长和温度传感的灵敏度, 金薄膜的厚度和D形结构的抛磨深度仅影响表面等离子体共振峰的相对强度. 结果表明: 该传感器在-10–80 ℃的温度范围内具有11.6 nm/℃的温度灵敏度, 在1.34–1.44折射率范围内折射率灵敏度最高可达26000 nm/RIU.     

基于单端探测温度和折射率的MZI光纤传感器

提出并演示了一种基于单端探测的光纤传感器,可同时测量温度和折射率。微结构光纤探头由两个玻璃光纤微球拼接在一起,并在该探头的末端利用真空电子束蒸镀一层铝膜以增加反射,从而形成微球结构的马赫-曾德尔型光纤传感头。实验结果表明,该器件的温度灵敏度和折射率可分别达到50.77 pm/℃和-21.94 nm/RIU。这项工作提出了一种低成本、高分辨率的基于光纤方法实现的多功能传感应用。单端探测的马赫曾德尔型光纤传感器小尺寸的优势可应用到小体积气体的测量,而它的全二氧化硅设计提供了高温或化学严酷环境的兼容性。     

Photonic crystal fiber tip interferometer for refractive index sensing

In this paper we present an interferometer based on photonic crystal fiber (PCF) tip ended with a solid silica-sphere for refractive index sensing. The sensor is fabricated by splicing one end of the holey PCF to a single mode fiber (SMF) and applying arc at the other end to form a solid sphere. The sensor has been experimentally tested for refractive index and temperature sensing by monitoring its wavelength shift. Measurement results show that the sensor has the resolution of the order of 8.7×10(-4) over the refractive index range of 1.33-1.40, and temperature sensitivity of the order of 10 pm/°C in the range of 20-100 °C.     

一种新型光谱表面等离子体共振二维探测方法在DNA微阵列中的应用

在此前曾提出过一种新型二维折射率探测方法——并行扫描光谱表面等离子体共振(surface plasmon resonance, SPR)成像方法。在这种方法中,使用线形光照明,CCD得到的图像包含SPR光谱信息和一维空间信息,进而通过计算可得到折射率的一维分布信息。通过一维扫描,就能够得到整个被扫描区域内的折射率二维分布信息。该方法具有高灵敏、高通量的优点,适合微阵列(microarray)的检测, 并完善了这种方法的数据处理过程,使用空气折射率作为参考,消除了无法精确控制入射角的难题。使用该方法对手工点制的军团菌mip DNA探针微阵列进行了检测,证明了这种方法高灵敏无标记地探测微阵列的可行性。我们得到的军团菌mip DNA探针制备浓度与其等效折射率的关系,这对基于SPR的微阵列技术的发展有着重要的参考意义。     

石英毛细管椭球微气泡模式特性及传感技术

利用有限元数值分析方法研究了椭球状石英毛细管微气泡回音壁模式特性及其折射率传感性能.计算分析了不同半径与内壁厚度情况下空芯和液芯椭球形微气泡模式特征,包括品质因数、有效折射率和能量比等,并探讨了微气泡在高灵敏度和高分辨率折射率传感方面的应用潜能.研究结果表明微气泡膨胀至350μm,且内壁厚度为1μm时分辨率和灵敏度最佳;在该厚度范围附近,微气泡分辨率不会因为半径尺寸的改变而发生太大变化;二阶径向模具有较高品质因数,其灵敏度略高于一阶基模,且使用二阶径向模可降低在制造时对结构壁厚控制精度的要求,可用于实际传感应用中.研究结果对微气泡的进一步实验研制具有理论参考价值.     

High-performance refractive index sensor based on guided-mode resonance in all-dielectric nano-silt array

We propose a high-quality refractive index sensing by utilizing the characteristic guided-mode resonance (GMR) excited in a simple one-dimensional all-dielectric nano-slit array. We demonstrate a figure of merit up to 12000, which is higher than that achieved in most plasmonic refractive index sensors. We show that high-quality sensing performance can be sustained over a broadband range in near infrared region with relatively large variations in both grating depth and angle of incidence. Such a GMR-based all-dielectric sensing device with the ease of fabrication is expected to hold great promise for realizing broadband refractive index sensors with high performance and compactness.