共查询到17条相似文献,搜索用时 93 毫秒
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原子吸收光谱法测定蔬菜中的铁、锰、铜、铅和镉 总被引:5,自引:0,他引:5
采用硝酸-高氯酸消解蔬菜样品,火焰原子吸收光谱法测定蔬菜中铁、锰和铜,石墨炉原子吸收光谱法测定蔬菜中的铅和镉。对仪器的工作条件作了探讨。在最佳实验条件下对韭菜、芹菜、洋白菜3种蔬菜进行测定,含量分别为铁:20.01、4.57、5.60μg.g-1,锰:1.445、1.141、1.204μg.g-1,铜:1.031、0.566、0.328μg.g-1,铅:0.106、0.085、0.076μg.g-1和镉:0.012、0.032、0.018μg.g-1。加标回收率为94.0%—106%。该方法简便、准确。 相似文献
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用硝酸、高氯酸混合酸消解样品,采用原子吸收光谱法,测定了野猪肉和家猪肉中的钙、铜、锌、铁的含量,并对其结果进行了分析.各元素在实验范围内,线性关系良好,回收率在98%-102%之间.野猪肉和家猪肉中钙含量分别为5.02μg·g-1和5.01μg·g-1,没有差异;而野猪肉和家猪肉中的Zn、Fe、Cu分别为39.95μg·g-1、27.50μg·g-1、13.62μg·g-1和9.53μg·g-1、Fe10.21μg·g-1、Cu 8.52μg·g-1;显著高于家猪肉.测定结果显示野猪肉含有丰富的Zn、Fe、Cu元素,具有较高的营养和保健价值,应合理开发利用野猪资源. 相似文献
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用石墨炉原子吸收法测定掺质钆镓石榴石单晶中钴、铬、镍的含量,晶体中的钆不影响测定,但镓呈现背景干扰,文中对此进行了讨论。用氘灯扣除背景。钴、铬、镍含量为0.015%、0.037%、0.0057%时,变动系数分别为1.4%、1.9%、2.7%,检出限分别为2.5μg/g、0.87μg/g、2.0μg/g。 相似文献
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李玉洁 《光谱学与光谱分析》1981,(5)
本法采用氢氧化钠、碳酸钠分解法,在5%盐酸溶液中,用电成耦合高频等离子体发射光谱测定矿物、岩石中钡、锶。方法分析灵敏度:钡为0.02μg/ml、锶为0.005μg/ml。相对均方误差:钡±2.0%,锶±2.0%。 相似文献
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顺序注射氢化物发生-原子荧光光谱法测定化肥中砷、汞、锑和硒 总被引:6,自引:1,他引:5
本文建立了一种顺序注射氢化物发生 -原子荧光光谱法测定化肥中 As、Hg、Sb、Se含量的方法。在最佳条件下 ,As、Hg、Sb和 Se的检出限分别为 0 .1 5μg/ L、0 .0 6 1μg/ L、0 .0 4 6μg/ L、0 .2 5μg/ L。测定化肥中 As、Hg、Sb和 Se,回收率均在 94 .6 7%— 1 0 6 .81 %之间。该方法用于检测化肥中 As、Hg、Sb和 Se具有很好的可行性和实用性。 相似文献
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We argue, based on general principles, that topological order is essential to realize fractionalization in gapped insulating phases in dimensions d > or = 2. In d = 2 with genus g, we derive the existence of the minimum topological degeneracy q(g) if the charge is fractionalized in units of 1/q, irrespective of microscopic model or effective theory. Furthermore, if the quasiparticle is either boson or fermion, it must be at least q(2g). 相似文献
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The glass transition temperature is known to increase with decreasing film thickness h for sufficiently thin poly(methyl methacrylate) films supported by silicon oxide substrates. We show that this system undergoes a CO2 pressure-induced devitrification transition, P(g), which is film thickness dependent, P(g)(h)=DeltaP(g)+P(bulk)(g). P(bulk)(g) is the bulk glass transition and DeltaP(g) can be positive or negative depending on T and P. The phenomenon of retrograde vitrification, wherein the polymer exhibits a rubbery-to-glassy-to-rubbery transition upon changing temperature isobarically, is also shown to occur in this system and it is film thickness dependent. 相似文献
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Analytical model of nonlinear, single-mode, classical Rayleigh-Taylor instability at arbitrary Atwood numbers 总被引:1,自引:0,他引:1
Goncharov VN 《Physical review letters》2002,88(13):134502
An analytical model of the nonlinear bubble evolution of single-mode, classical Rayleigh-Taylor instability at arbitrary Atwood numbers (A(T)) is presented. The model is based on an extension of Layzer's theory [Astrophys. J. 122, 1 (1955)] previously applied only to the fluid-vacuum interfaces (A(T) = 1). The model provides a continuous bubble evolution from the earlier exponential growth to the nonlinear regime when the bubble velocity saturates at U(b) = square root of [2A(T)/(1+A(T)) (g/C(g)k)], where k is the perturbation wave number, g is the interface acceleration, and C(g) = 3 and C(g) = 1 for the two-dimensional and three-dimensional geometries, respectively. 相似文献
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The concentration of iron in Substantia nigra, the part of the brain which is involved in Parkinson disease, has been found by Mössbauer spectroscopy (MS) to be ~ 160 μg/g wet tissue and ~ 670 μg/g dry weight, both in control and Parkinson samples. All the iron observed by MS in these samples is ferritin-like iron. In several blood diseases, large amounts of ferritin-like iron have been observed in red blood cells. Desferral removed iron from serum, but not from red blood cells. The iron compound in the malarial pigment of human blood infected by P. falciparum was found to be hemin-like, whereas the pigment iron in rats infected by P. berghei was different from any known iron porphyrin. 相似文献
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A generalization of local commutativity to the fields with an exponential momentum-space growth e
lp is considered. To study the local properties of such fields we associate to each space-time region
a topology (
) on the test function space. It is shown that under any choice of the topology the fields of exponential growth are localizable only in space-time regions large in comparison withl. This happens because not any domain in the space of several complex variables is a domain of holomorphy. However, by specifying the topology through the use of holomorphically convex domains in 4, one can attach certain meaning to local commutativity for arbitrarily close spacelike separated regions of 4. 相似文献
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Lattice models such as Ising or Potts models are very often successfully applied to order-disorder phenomena in solids (e.g., for alloys) or on surfaces (e.g., for physisorption). In this contribution it is shown how to derive such models from a microscopic Hamiltonian in the framework of classical statistical mechanics. Both structural relaxations and thermal fluctuations can be incorporated within the (temperature-dependent) parameters of the lattice model. 相似文献