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1.
Silver nanoparticles (Ag NPs) were efficiently generated by in situ reduction of silver ions via butylated hydroxytoluene
(BHT), in poly(methyl methacrylate). The characterization of Ag/PMMA by TEM, SEM, XRD, and FTIR indicated that Ag NPs with
a face center cubic (fcc) crystal structure and a mean diameter of about 30 nm were dispersed in PMMA matrix with a relatively
uniform distribution. In addition, the results of UV–Vis spectroscopy indicated that optical properties of the nanocomposite
appeared mainly dependent on the reaction time and temperature. Increasing the reaction time and temperature make higher yield
of Ag NPs. A provisional reduction mechanism was also proposed for the formation of the Ag NPs. 相似文献
2.
Xin Jiang Shi Chen Congwen Mao 《Colloids and surfaces. A, Physicochemical and engineering aspects》2008,320(1-3):104-110
Ag/SiO2 nanocomposite was synthesized in a nanoreactor formed by adsorption layer on silica surface. Ag nanoparticles were prepared by the reduction of Ag ion with ethanol at alkaline condition. By using TEM and XRD, the effects of NaOH concentration, water and temperature on the appearance and grain size of Ag particles were analyzed, respectively. The adsorption curve of NaOH was measured by electrical conductivity meter. The experiment result revealed that Ag grain size decreased while increasing NaOH concentration or while increasing water in our system. Ag grain size increased with the increase of temperature. And Ag aggregated seriously when temperature is up to 60 °C. Finally, after exploring the optimum conditions of reaction, we successfully obtained the well-distributed Ag nanoparticles on surface of silica, and average grain size of Ag nanoparticles reached 5 nm. 相似文献
3.
Yu-Chen Tsai Ping-Chieh Hsu Yen-Wen Lin Tzong-Ming Wu 《Electrochemistry communications》2009,11(3):542-545
The work presents a novel surface-enhanced Raman scattering (SERS)-active surface prepared by electrochemical deposition of silver nanoparticles in multiwalled carbon nanotube (MWCNT)–alumina-coated silica (ACS) nanocomposite. The formation of Ag nanoparticles in MWCNT–ACS nanocomposite was investigated by scanning electron microscopy. It shows that Ag nanoparticles with a diameter of about 100–200 nm in the MWCNT–ACS nanocomposite and some Ag nanoparticles aggregated to form interconnected aggregates. The Ag–MWCNT–ACS-coated indium tin oxide substrate has a considerable effect on the Raman spectra with improvements of more than four times of magnitude as compared with the Ag-coated indium tin oxide substrate. The present methodology demonstrates that the composite composed of Ag, MWCNT, and ACS is suitable for potential plasmonic devices. 相似文献
4.
G. V. Mamontov T. I. Izaak O. V. Magaev A. S. Knyazev O. V. Vodyankina 《Russian Journal of Physical Chemistry A, Focus on Chemistry》2011,85(9):1540-1545
Ag/SiO2 and Ag3PO4/SiO2 systems supported on silica aerogel were investigated using temperature-programmed reduction (TPR), UV-visible diffuse reflectance
spectroscopy (UV-vis DRS), and infrared spectroscopy. The formation of highly dispersed silver particles, uniformly distributed
along the surface and stabilized with silanol groups, was observed for Ag/SiO2 system. Phosphate and silanol groups produce two states of silver localization in phosphate-containing system. The addition
of phosphate onto the silica surface leads to the reversible oxidation/reduction of silver in the temperature range of 100–300°C
with transitions of silver (particles 10–30 nm in size) to charged states (ions, clusters stabilized by phosphate groups).
This reversible behavior of silver is stable, and the amount of silver involved in these processes remained constant (∼50%)
for the series of consistent cyclic oxidation/reduction treatments. 相似文献
5.
Nanocomposite ZnO–Ag thin film containing nano-sized Ag particles have been grown on glass substrate by spin-coating technique
using zinc acetate dihydrate as starting precursor in 2-propanol as solvent and monoethanolamine as stabilizer. Silver nanoparticles
were added in the ZnO sol using silver nitrate dissolved in ethanol-acetonitrile. Their structural, electrical, crystalline
size and optical properties were investigated as a function of preheating, annealing temperature and silver content. The results
indicated that the crystalline phase was increased with increase of annealing temperature up to 550 °C at optimum preheating
temperature of 275 °C. Thermal gravimetric differential thermal analysis results indicated that the decomposition of pure
ZnO and nanocomposite ZnO–Ag precursors occurred at 225 and 234 °C, respectively with formation of ZnO wurtzite crystals.
The scanning electron microscopy and atomic force microscopy revealed that the surface structure (the porosity and grain size)
of the ZnO–Ag thin film (the film thickness is about 379 nm) was changed compared to pure ZnO thin film. The result of transmission
electron microscopy showed that Ag particles were about 5 nm and ZnO particles 58 nm with uniform silver nanoclusters. Optical
absorption results indicated that optical absorption of ZnO–Ag thin films decreased with increase of annealing temperature.
Nanocomposite ZnO–Ag thin films with [Ag] = 0.068 M and [Ag] = 0.110 M showed an intense absorption band, whose maximum signals
appear at 430 nm which is not present in pure ZnO thin films. The result of X-ray photoelectron spectroscopy revealed that
the binding energy of Ag 3d5/2 for ZnO–Ag shifts remarkably to the lower binding energy compared to the pure metallic Ag due to the interaction between
Ag and ZnO. 相似文献
6.
UV-photocatalytic oxidation of 2,4-dichlorophenoxyacetic acid (2,4-d) was studied on Silver–TiO2 semiconductors prepared by co-gelling silver acetylacetonate and titanium butoxide (TiO2–Ag) or by incipient impregnation with silver acetylacetonate (0.5 wt% Ag) of bare TiO2 sol–gel and TiO2–P25 supports. The comparative study shows that only a slight modification on the specific surface area was obtained on the
TiO2–Ag sample (60 m2/g) as compared to the TiO2 sol–gel bare support (65 m2/g). XRD patterns of the samples show anatase as the crystalline phase present in the sol–gel TiO2 preparations. By means of HRTEM and HAADF-STEM electron microscopy techniques, silver nanoparticles (<12.0 nm) were identified
which are very small to be detected by XRD. The photocatalytic oxidation of the herbicide 2,4-d used as a model of contaminant show for the kinetic parameter t1/2 values of 45 min for the TiO2–Ag sample, while for the impregnated Ag/TiO2 and Ag/P25 nanomaterials t1/2 was 124 and 66 min, respectively. The higher photoactivity of the TiO2–Ag photocatalyst is attributed to a combined effect of the silver nanoparticles in interaction with the titania semiconductor. 相似文献
7.
G. V. Krylova Yu. I. Gnatyuk N. P. Smirnova A. M. Eremenko V. M. Gun’ko 《Journal of Sol-Gel Science and Technology》2009,50(2):216-228
A variety of Ag nanoparticles/oxide mesoporous films with templated silica, titania, and zirconia was synthesized by sol–gel
method at glass, aluminum, and silicon substrates using metal alkoxides (tetraethoxysilane, titanium tetraisopropoxide, and
zirconium tetrapropoxide) and AgNO3 as precursors of oxide films and Ag nanoparticles, respectively, and Pluronic P123 as a template agent. Oxide films alone
and Ag/oxide composites were characterized using hexane adsorption, X-ray diffraction (XRD), Raman and ultraviolet (UV)/vis
spectroscopies, scanning electron microscopy (SEM) and transmission electron microscopy (TEM) methods. The distribution of
Ag nanoparticles within the films, their sizes, intensity, and position of surface plasmon resonance (SPR) absorbance band
at λ = 400 nm, as well as the textural and structural characteristics of whole films depend on treatment temperature, types of
substrates and oxide matrices, oxide crystallization, and Ag content. Ag nanoparticles form preferably on the outer surface
of the films under lower sintering temperatures if the amount of loaded silver is low. Oxide crystallization (e.g., TiO2) promotes silver embedding into the outer film layer. At higher silver content (≥10 at.%) and higher calcination temperature
(873 K), silver nanoparticles could be entrapped more uniformly along the film profile because of more intensive evaporation
of silver droplets from the outer surface of the films on heating. 相似文献
8.
Laser ablation of a solid target material in a liquid environment provides with an easy, straightforward and environmentally
friendly method for nanoparticles synthesis as well as with the unique possibility of directly controlling the type of the
nanoparticles surface ligands through the liquid choice. In this paper, laser ablation (10.4 ps, 1064 nm and 50 kHz) of a
bulk silver target in deionized water, was carried out for nanoparticles synthesis. The synthesised nanoparticles are either
pure Ag or A2O3 or a mixture of the two materials. Their size distribution follows log-normal function with a statistical median diameter
of ≈5 nm. The nanoparticles colloidal solutions were directly mixed after synthesis, with the polymer solution poly(3,4-ethylenedioxythiophene):poly(4-styrenesulfonate)
(PEDOT:PSS) for the formation of polymer-nanoparticles nanocomposite. The nanoparticles readily form bonds with the sulphur
atom of PEDOT which results in their uniform distribution within the polymer matrix as well as in a replacement by the nanoparticles
of the PSS− as the counteranions to the PEDOT+. These effects result in the reduction of the effective insulation of the polymer blend particles by the insulating PSS and
furthermore in the electrical conductivity of the nanocomposite becoming higher (by ∼1.5 times) as compared with that of the
pure polymer. 相似文献
9.
《应用有机金属化学》2017,31(8)
A facile, green and efficient approach was applied to synthesize multi‐walled carbon nanotubes (MWNTs) decorated with silver nanoparticles (MWNT‐Ag) for further potential application. Oxidized MWNTs were decorated with silver nanoparticles (Ag NPs) via a method combining ultraviolet irradiation‐induced reduction and conventional silver mirror reaction without any reducing agent. The obtained product was characterized using various methods. X‐ray diffraction proved that the Ag NPs were synthesized successfully. Moreover, Ag NPs with a diameter of 80 nm, attached onto MWNTs, could be clearly observed in field emission scanning electron microscopy images, which also confirmed Ag NPs. Energy‐dispersive spectroscopy and transmission electron microscopy also indicated the presence of Ag NPs. Furthermore, thermogravimetric analysis was used to measure the content of Ag NPs in MWNT‐Ag, the result indicating that the weight content of Ag NPs was up to 31.88%. UV–visible absorption spectroscopy was adopted to evaluate the dispersion property of MWNT‐Ag. The result illustrated that MWNT‐Ag had a good dispersibility and stability in water. Characterization was also carried out through Fourier transform infrared spectroscopy, Raman spectroscopy and dynamic light scattering analysis. 相似文献
10.
Brigita Tomšič Barbara Simončič Boris Orel Lidija Černe Petra Forte Tavčer Mateja Zorko Ivan Jerman Aljaž Vilčnik Janez Kovač 《Journal of Sol-Gel Science and Technology》2008,47(1):44-57
Multifunctional, water and oil repellent and antimicrobial finishes for cotton fibres were prepared from a commercially available
fluoroalkylfunctional water-born siloxane (FAS) (Degussa), nanosized silver (Ag) (CHT) and a reactive organic–inorganic binder
(RB) (CHT). Two different application procedures were used: firstly, one stage treatment of cotton fabric samples by FAS sol
(i), as well as by a sol mixture constituted from all three precursors (Ag–RB–FAS, procedure 1S) (ii), and secondly, two stage
treatment of cotton by Ag–RB sol and than by FAS sol (Ag–RB + FAS, procedure 2S) (iii). The hydrophobic and oleophobic properties
of cotton fabrics treated by procedures (i)–(iii) before and after consecutive (up to 10) washings were established from contact
angle measurements (water, diiodomethane and n-hexadecane) and correlated with infrared and XPS spectroscopic measurements. The results revealed that even after 10 washing
cycles cotton treated with Ag–RB + FAS (2S) retained an oleophobicity similar to that of the FAS treated cotton, while the
Ag–RB–FAS (1S) cotton fibres exhibited a loss of oleophobicity already after the second washing, even though fluorine and
C–F vibrational bands were detected in the corresponding XPS and IR spectra. The antibacterial activity of cotton treated
by procedures (i)–(iii) was tested by its reduction of the bacteria Escherichia coli and Staphylococcus aureus following the AATCC 100-1999 standard method and EN ISO 20743:2007 transfer method. The reduction in growth of both bacteria
was nearly complete for the unwashed Ag–RB and Ag–RB–FAS (S1), but for the unwashed Ag–RB + FAS (S2) treated cotton no reduction
of S. aureus and 43.5 ± 6.9% reduction of E. coli was noted. After the first washing, the latter two finishes exhibited nearly a complete reduction of E. coli but for the Ag–RB treated cotton the reduction dropped to 88.9 ± 3.4. None of the finishes retained antibacterial properties
after 10 repetitive washings. The beneficial and long-lasting low surface energy effect of FAS finishes in the absence of
Ag nanoparticles, which led to the “passive” antibacterial properties of FAS treated cotton fabrics, was established by applying
the EN ISO 20743:2007 transfer method. The results revealed a reduction in bacteria of about 21.9 ± 5.7% (FAS), 13.1 ± 4.8%
(Ag–RB–FAS (S1)) and 41.5 ± 3.7% (Ag–Rb + FAS (S2)), while no reduction of the growth of bacteria was observed for cotton
treated with Ag nanoparticles after 10 repetitive washings. The physical properties (bending rigidity, breaking strength,
air permeability) of finished cotton samples were determined, and showed increased fabric softness and flexibility as compared
to the Ag–RB treated cotton, but a slight decrease of breaking strength in the warp and weft directions, while air permeability
decreased for all type of finishes. 相似文献
11.
Michael Coto Giorgio Divitini Avishek Dey Satheesh Krishnamurthy Najeeb Ullah Cate Ducati R. Vasant Kumar 《Materials Today Chemistry》2017
A highly efficient black TiO2-Ag photocatalytic nanocomposite, active under both UV and visible light illumination, was synthesized by decorating the surface of 25 nm TiO2 particles with Ag nanoparticles. The material was obtained via a rapid, one-pot, simple (surfactant and complexing agent free) chemical reduction method using silver nitrate and formaldehyde as a metal salt and reducing agent, respectively. The nanocomposite shows an increase of over 800% in the rate of photocatalytic methylene blue dye degradation, compared to commercial unmodified TiO2, under UV-VIS illumination. Unlike pure TiO2, the nanocomposite exhibits visible light activation, with a corresponding drop in optical reflectance from 100% to less than 10%. The photocatalytic properties were shown to be strongly enhanced by post-reduction annealing heat treatments in air, which were observed to decrease, rather than coarsen, silver particle size, and increase particle distribution. This, accompanied by a variation in the silver surface oxidation states, appear to dramatically affect the photocatalytic efficiency under both UV and visible light. This highly active photocatalyst could have wide ranging applications in water and air pollution remediation and solar fuel production. 相似文献
12.
Silver nanoparticles preparation and the aggregation stability of the particles was investigated in lamellar liquid crystalline
systems. A liquid crystal of HDTABr/pentanol/water was first prepared. The water content was next increased while keeping
the mass ratio of HDTABr and pentanol constant. Silver nanoparticles were produced by replacing the aqueous phase by Ag sols
of various concentrations (0.5–5×10–3 mol/l) or by an in situ preparation method, i.e., interlamellar reduction of Ag+ ions in the liquid crystalline phase. The stability of the silver nanoparticles was monitored by UV-VIS spectroscopy and
TEM. The particle size ranged from 5 to 44 nm. The kinetic of silver nanoparticle aggregation was investigated. The effect
of nanoparticles on structural ordering in liquid crystals was studied by XRD measurements and it was established that the
lamellar distance (dL) was only slightly altered.
Electronic Publication 相似文献
13.
Magdalena Stevanović Igor Savanović Vuk Uskoković Srečo D. Škapin Ines Bračko Uroš Jovanović Dragan Uskoković 《Colloid and polymer science》2012,290(3):221-231
A simple and green chemical method has been developed to synthesize stable bare and capped silver nanoparticles based on the
reduction of silver ions by glucose and capping by poly(α,γ,l-glutamic acid) (PGA). The use of ammonia during synthesis was avoided. PGA has had a dual role in the synthesis and was used
as a capping agent to make the silver nanoparticle more biocompatible and to protect the nanoparticles from agglomerating
in the liquid medium. The synthesized PGA-capped silver nanoparticles in the size range 5–45 nm were stable over long periods
of time, without signs of precipitation. Morphological examination has shown that the silver nanoparticles had a nearly spherical,
multiply twinned structure. The effects of the reaction temperature and the reaction time during the synthesis were investigated
too. The biocompatibility of the PGA-capped silver nanoparticles is discussed in terms of in vitro toxicity with human intestinal
Caco-2 cells. The samples were characterized by UV–Visible spectroscopy, field emission scanning electron microscopy, transmission
electron microscopy, and zeta potential measurements. 相似文献
14.
Hossein Mahdavi Ozra Rahmani Ahmad Reza Shahverdi 《Journal of the Iranian Chemical Society》2017,14(1):37-46
In this study, preparation and characterization of polyacrylamide/reduced graphene oxide-Ag (PAM/rGO-Ag) nanocomposites as a new nanocomposite film were investigated. First, PAM/GO nanocomposite was synthesized by in situ polymerization strategy. Afterward, highly stable and uniformly distributed silver nanoparticles (Ag NPs) have been obtained with PAM/GO nanocomposite as nanoreactors via in situ reduction of silver nitrate (AgNO3) using sodium borohydride (NaBH4) as reducing agent. In addition, the prepared PAM/rGO-Ag nanocomposite was thermally annealed in order to achieve high-performance nanocomposite film with antimicrobial activities. The prepared nanocomposite was characterized by XRD, FT-IR, SEM, TEM and TGA. The obtained results demonstrate that the silver nanoparticles were well decorated and dispersed on the graphene oxide nanosheets. In fact, the GO nanosheets and polyacrylamide chains act as a support and stabilize the Ag nanoparticles. Moreover, antimicrobial activities of the films were also examined, and the films containing well-dispersed and stabilized Ag nanoparticles showed outstanding antibacterial activity. 相似文献
15.
Cinnamon zeylanicum bark extract and powder mediated green synthesis of nano-crystalline silver particles and its bactericidal activity 总被引:1,自引:0,他引:1
M. Sathishkumar K. Sneha S.W. Won C.-W. Cho S. Kim Y.-S. Yun 《Colloids and surfaces. B, Biointerfaces》2009,73(2):332-338
The exploitation of various plant materials for the biosynthesis of nanoparticles is considered a green technology as it does not involve any harmful chemicals. The present study reports the synthesis of silver (Ag) nanoparticles from silver precursor using the bark extract and powder of novel Cinnamon zeylanicum. Water-soluble organics present in the plant materials were mainly responsible for the reduction of silver ions to nano-sized Ag particles. TEM and XRD results confirmed the presence of nano-crystalline Ag particles. The pH played a major role in size control of the particles. Bark extract produced more Ag nanoparticles than the powder did, which was attributed to the large availability of the reducing agents in the extract. Zeta potential studies showed that the surface charge of the formed nanoparticles was highly negative. The EC50 value of the synthesized nanoparticles against Escherichia coli BL-21 strain was 11 ± 1.72 mg/L. ThusC. zeylanicum bark extract and powder are a good bio-resource/biomaterial for the synthesis of Ag nanoparticles with antimicrobial activity. 相似文献
16.
《先进技术聚合物》2018,29(3):1107-1116
Carbopol‐silver nanocomposites, CP‐Ag‐NCs, were prepared by a chemical reducing method by using formaldehyde as a reducing agent (nanocomposite F), and formaldehyde in the presence of an alkaline medium resulting from the addition of Na2CO3 (nanocomposite FC), or NaOH (nanocomposite FO) to enhance the rate of reduction of the silver ions. The UV‐visible spectra showed the appearance of bands centered around 275, 286, and 274 nm for the nanocomposites F, FC, and FO, respectively, attributed to small silver nanoparticles (Ag‐NPs) with an average size less than 10 nm. Other bands centered around 405 and 470 nm for the nanocomposites F and FC, respectively, were attributed to large Ag‐NPs with an average size greater than 50 nm. The absence of large Ag‐NPs in the nanocomposites FO makes them as the materials of choice for the preparation of selective ultrasmall Ag‐NPs with an average size less than 3 nm. Furthermore, photoluminescence was observed upon blue excitation of the ultrasmall colloidal Ag‐NPs. Scanning electron microscopy images showed a good dispersion of the metallic Ag‐NPs in the polymer matrix. Moreover, X‐ray diffraction patterns showed peaks corresponding to the face‐centered‐cubic of the Ag‐NPs. The nature of the interaction between carbopol and Ag‐NPs was further studied by attenuated total reflectance‐Fourier transform infrared spectroscopy, and the mechanism of reduction of the silver ions was proposed. The antimicrobial activities of the CP‐Ag‐NCs were examined against Escherichia coli and Candida albicans microorganisms. The results demonstrate that the CP‐Ag‐NCs can provide new applications of these nanocomposites as efficient sensors and antimicrobial materials. 相似文献
17.
Saswati Sarkar Prasanta Kumar Biswas Sunirmal Jana 《Journal of Sol-Gel Science and Technology》2012,61(3):577-584
We report the fabrication of nano silver coated patterned silica thin film by sol–gel based soft lithography technique. Initially,
silica gel film on soda lime silica glass was prepared by dipping technique from a silica sol of moderate silica concentration.
A PolydimethylSiloxane elastomeric stamp containing the negative replica of the patterns of commercially available compact
disc was used for embossing the film and the embossed film was cured up to 450 °C in pure oxygen atmosphere for oxide film.
Finally, a precursor solution of AgNO3 in water containing polyvinyl alcohol as an organic binder was made and used for coating on the patterned silica film by
dipping technique and cured the sample up to 450 °C in reducing gas atmosphere to obtain nano silver layer. The formation
of only cubic silver (~4.0 nm) and both cubic silver (~5.2 nm) and silver oxide (~3.6 nm) crystallites at 350 and 450 °C film
curing temperatures respectively were confirmed by XRD measurements. The % of nano silver metal and silver oxide were 75.4
and 24.6 respectively. The nano-structured surface feature was visualized by FESEM whereas AFM revealed the high fidelity
grating structure of the films. Presence of both spherical and rectangular structure (aspect ratio, 2.37) of nano silver/silver
oxide was confirmed by TEM. The films were also characterized by UV–Vis spectral study. The patterned film may find application
in chemical sensor devices. 相似文献
18.
《Journal of Saudi Chemical Society》2022,26(4):101505
In this study, silver nanoparticles (Ag NPs) were decorated on the surface of magnetic nanoparticles in an eco-friendly pathway applying Mentha extract as reducing/stabilizing agent. The morphological and physicochemical features of the prepared Ag/Fe3O4nanocomposite were determined using several advanced techniques. Hence, our protocol is green and advantageous in terms of- i) biochemical modified biocompatible nanocomposite; ii) nanomaterial providing high surface area and larger number reactive sites; iii) very simplistic synthetic procedure; vi) very low load of metal in the composite and v) high yield in short time. In the medicinal part, the anticancer properties of Ag/Fe3O4 nanocomposite against lung cancer cell lines were determined. The free radical for the antioxidant effects was DPPH. The IC50 of Ag/Fe3O4 nanocomposite was 200 µg/ml in the antioxidant test. The IC50 of the Ag/Fe3O4 nanocomposite were 183, 176, 169, and 125 µg/mL against lung cancer (NCI-H661, NCI-H1975, NCI-H1573, and NCI-H1563) cell lines, respectively. In addition, the current study offer that Ag/Fe3O4 nanocomposite could be a new potential adjuvant chemopreventive and chemotherapeutic agent against cytotoxic cells. 相似文献
19.
Jing-Jing Yu Shuang Lu Jiang-Wen Li Fa-Qiong Zhao Bai-Zhao Zeng 《Journal of Solid State Electrochemistry》2007,11(9):1211-1219
This study reports the preparation and characterization of gold nanoparticles deposited on amine-functioned hexagonal mesoporous
silica (NH2–HSM) films and the electrocatalytic oxidation of glucose. Gold nanoparticles are fabricated by electrochemically reducing
chloroauric acid on the surface of NH2–HSM film, using potential step technology. The gold nanoparticles deposited have an average diameter of 80 nm and show high
electroactivity. Prussian blue film can form easily on them while cycling the potential between −0.2 and 0.6 V (vs saturated
calomel electrode) in single ferricyanide solution. The gold nanoparticles loading NH2–HSM-film-coated glassy carbon electrode (Au–NH2–HSM/GCE) shows strong catalysis to the oxidation of glucose, and according to the cathodic oxidation peak at about 0.16 V,
the catalytic current is about 2.5 μA mM−1. Under optimized conditions, the peak current of the cathodic oxidation peak is linear to the concentration of glucose in
the range of 0.2 to 70 mM. The detection limit is estimated to be 0.1 mM. In addition, some electrochemical parameters about
glucose oxidation are estimated. 相似文献
20.
Marek Jasiorski Anna Leszkiewicz Stefan Brzeziński Gabriela Bugla-Płoskońska Grażyna Malinowska Beata Borak Iwona Karbownik Agnieszka Baszczuk Wiesław Stręk Włodzimierz Doroszkiewicz 《Journal of Sol-Gel Science and Technology》2009,51(3):330-334
The aim of this study was to investigate antimicrobial activity of textiles doped with silver in different forms. Three types
of textiles were prepared and examined: textiles doped with commercially available Ag nanoparticles, textiles doped with commercial
colloidal silver and textiles doped with silver silica SiO2/Ag spheres. The specimens of silica submicron spheres were synthesized by the sol–gel method as a matrix for biological active
silver. The results of microbiological tests revealed that among three kinds of Ag doped textiles only these doped with SiO2/Ag spheres are bacteriostatically active. During the experiments minimal inhibiting bacteria growth concentration of active
SiO2/Ag spheres added to textiles was determined. 相似文献