基于PASCO平台的透明材料折射率的测量

将迈克耳孙干涉仪和PASCO实验平台相结合,设计了一种高精度、高效率测量透明材料折射率的方法.首先分析PASCO迈克耳孙干涉仪测量材料折射率的原理,然后利用高性能PASCO传感器和计算机对干涉条纹进行图像采集和数据处理,得到待测透明材料的折射率信息.最后对材料折射率的不确定度进行探究.实验结果表明,旋转角度θ对折射率的不确定度影响最大,厚度d次之,干涉条纹计数K影响最小.PASCO实验平台配合迈克耳孙干涉仪可以准确、高效的记录干涉条纹在"吞吐"时光强的变化,降低条纹计数测量的不确定度,从而提高透明材料折射率的计算精度.同时该方法还可用于和透明材料折射率相关的其他特性的测量.     

使用红外干涉仪测量红外材料折射率

使用自行研制的泰曼型红外干涉仪测量红外材料的折射率.在干涉仪的测试臂中加一个旋转台,将被测件放在旋转台上旋转,在旋转过程中经过被测件的光程发生改变,导致干涉条纹发生移动,通过测量条纹的移动数和被测件的旋转角度来计算出被测件的折射率.测量结果显示,25°C时在10.6μm波段处锗单晶的折射率为4.003,硫系玻璃锗砷硒(GeAsSe)的折射率为2.494.折射率测量的误差在10-3量级,增加被测件的厚度会进一步提高折射率的测量准确度,待测红外材料的折射率越低,测量准确度越高.     

使用红外干涉仪测量红外材料折射率

使用自行研制的泰曼型红外干涉仪测量红外材料的折射率.在干涉仪的测试臂中加一个旋转台,将被测件放在旋转台上旋转,在旋转过程中经过被测件的光程发生改变,导致干涉条纹发生移动,通过测量条纹的移动数和被测件的旋转角度来计算出被测件的折射率.测量结果显示,25 °C时在10.6 μm波段处锗单晶的折射率为4.003,硫系玻璃锗砷硒（GeAsSe）的折射率为2.494.折射率测量的误差在10－3量级,增加被测件的厚度会进一步提高折射率的测量准确度,待测红外材料的折射率越低,测量准确度越高.     

利用白光的双缝干涉测量介质薄膜的折射率

利用白光双缝干涉测定介质膜折射率,在双缝前加装待测介质薄膜,通过测微目镜中零级白色条纹在加装前后的位移,测定待测介质薄膜的折射率.此方法有现象明显、操作简便的优点.     

干涉法测量光学材料非线性折射率的方法研究

提出了一种基于楔形平板等厚干涉原理测量光学玻璃非线性折射率变化的方法。在理论分析的基础上,建立了变形的等厚干涉条纹变化△e／e与待测玻璃平片（K9玻璃）折射率变化量△nb之间的数学模型;在选取一定的实验条件下,获得等厚干涉实验测量干涉图样,并利用MATLAB对实验所得的干涉图进行图像数据处理分析计算,恢复出非线性变化光学玻璃材料的折射率变化量△nb该方法的测量精度可达10^-6。     

掠射法测液体折射率的视场分析

根据薄膜光学理论,分析了掠射法测液体折射率实验的视场.研究结果表明:本实验的视场是分界线附近亮区有明暗相间干涉条纹的准半阴视场;越靠近分界线,条纹间距越小,条纹锐度越大,临界光线对应于最细的亮条纹.进一步准确描述了该实验的实验现象.结合理论分析,测定了自来水的折射率.     

利用牛顿环装置测量平玻璃折射率

在牛顿环实验装置半透半反镜和移测显微镜物镜之间垂直光路位置放置待测平玻璃,改变平玻璃倾角,使干涉条纹产生水平位移,测量水平位移和倾角之间的关系,通过数据拟合测出平玻璃折射率的大小.该方法的关键是平玻璃倾角和水平微小位移的准确测量.实验中充分利用实验室现有条件组装角度测量仪测量倾角,利用牛顿环高精度移测显微镜以干涉环为参照读取微小位移,实现了对折射率较高精度的测量.     

工字形太赫兹超材料吸波体的传感特性研究

利用超材料吸波体对材料参数的电磁响应, 可将其应用于传感. 本文设计了一种工字形单元结构的超材料吸波体, 基于频域算法对其在太赫兹频段的传感特性进行数值模拟, 研究了待测样品折射率、厚度及电介质隔层厚度对超材料吸波体传感器的频率灵敏度、振幅灵敏度及品质因数的影响. 研究结果表明:当待测样品厚度为40 μm时, 折射率频率灵敏度可达到153.17 GHz/RIU, 折射率振幅灵敏度可达到41.37%/RIU; 待测样品折射率一定时, 厚度频率灵敏度随其厚度的增大而线性减小; 随着待测样品厚度的增加, RFOM呈增大趋势, 但增大幅度在逐渐减小; TFOM随待测样品厚度的增加而减小.     

用于透明平板平行度和均匀性测量的单元件干涉仪

提出了一种基于单元件干涉的用于检测透明介质平整度和均匀性的干涉仪.该干涉仪的核心元件是一个菱形分光棱镜.激光光源的平面波光束的一半光束透过待测样品,另一半光束直接透过空气,然后分别入射到菱形分光棱镜的两垂直面并在分光面相遇、相干.通过旋转待测样品改变相干的两束光光程差,从而使干涉条纹发生移动.形成的相干光被分光板分成两束,一束进入光电探测器用于探测干涉条纹移动数的整数部分,另一束则进入电荷耦合探测器用于采集干涉条纹图来计算干涉条纹移动数的小数部分.通过计算条纹移动数反推出光程差的变化量,再结合折射率或样品厚度信息则可以计算出样品厚度或折射率的分布,从而检测出透明介质的平行度和均匀性.模拟仿真和光学实验均证明了本方法的可行性、准确性和稳定性.     

掠入射法测量液体折射率实验现象分析

掠入射法是基于全反射定律,采用几何光学原理来测量液体折射率的一种方法.文中对掠入射法测量透明液体折射率实验中出现的干涉条纹进行了定量分析,认为在分光计望远镜中观察到的干涉条纹是光线进入辅助透镜和直角棱镜间被测薄液膜干涉形成的,通过定义干涉条纹疏密度,对于薄膜引起的光程差与干涉明纹(或暗纹)间距两者间的关系进行讨论,其讨论的结果与实验结果一致.     

Quasi-real time bio—Tissues monitoring using dynamic laser speckle photography

Joint development of a laser monitor for the real-time bio-tissue analysis is presented. The monitor is based on the digital dynamic laser speckle photography and deals with soft and hard bio-tissues. In soft tissues, the dynamic bio-speckles are formed in a scattered from a tissue laser light. An optically transparent model of hard bio-tissue was prepared and preliminary analysis of a stress field in the stressed model was performed using the dependence of the refractive index of transparent solids upon the state of stress and the double exposure speckle photography data. The refractive index of the stressed material was evaluated and the state of stress was reconstructed using the stress-optical law.     

Propagation soliton et auto-confinement de faisceaux laser par non linearité optique de kerr

An experimental demonstration is presented of the stable monomode self-trapping of laser beams with adequate shape and power when they are propagating through homogeneous transparent dielectrics whose refractive index exhibits fluctuations proportional to the local intensity. The field evolution in such material is governed by a nonlinear scalar wave equation, that possesses stable solutions called solitons. Those solutions correspond to the exact balance of the natural diffraction divergence of the beam by the convergence of the self-induced refractive index gradient.     

干涉法测量液体膨胀系数的讨论

液体的折射率和液体的密度有直接关系,液体密度又与温度有关,根据已有关于透明介质的折射率公式,可得液体的膨胀系数的测量方法.迈克耳孙干涉法是测量液体折射率的温度系数的简捷的手段.用此方法得出了液体的膨胀系数,进而讨论了关于液体折射率的2个不同公式的精确程度.     

简易浓度测定方法的研究

浓度是反映溶液性质的一个重要参数,现有的各种测量方法各有其特点。文献［１］是根据光学原理,运用显微镜调焦方法提出了测量透明材料厚度和折射率的方法;在此基础上,根据不少溶液的折射率和浓度均有定量对应关系的特点,提出测定浓度的简易方法。该测量方法有下列特点：非接触测量,采样液体少,对液体无特殊要求,适用面广,装置简单。实验结果得出,百分浓度的测量可精确到０１％。用该方法同一些常规方法相比,测量误差在１％左右,能满足有关生产和工作中的使用要求。     

利用光子晶体测量透明液体折射率

设计了用反Opal结构光子晶体测量透明液体折射率的实验.根据布拉格公式推导了用反Opal光子晶体测量透明液体折射率的公式.利用紫外-可见分光光度计分别测得光子晶体处于空气和透明液体中的透射谱,由透射谱分别确定光子晶体处于2种介质中的禁带中心波长,将中心波长代入测量公式即可得到透明液体折射率.实验测量了水和甘油的折射率,得到了与公认值相吻合的结果.     

Two-photon polymerization of titanium-containing sol–gel composites for three-dimensional structure fabrication

In this work, we have synthesized and characterized a novel, titanium-containing hybrid material that can be structured three-dimensionally using two-photon polymerization. We investigate the effect on the structurability of the increase of titanium isopropoxide and methacrylic acid in this photosensitive composite. We show that while it is possible to make transparent thin films with a titanium isopropoxide molar content as high as 90%, three-dimensional structures can be made only when the titanium isopropoxide molar content is less than 50%. We measure the refractive index of films with different titanium isopropoxide: methacrylic acid concentrations and we show that while the refractive index increases linearly with the titanium isopropoxide, the increase of the methacrylic acid content does not affect the refractive index of the material.     

Optical refractometry based on Fresnel diffraction from a phase wedge

A method that utilizes the Fresnel diffraction of light from the phase step formed by a transparent wedge is introduced for measuring the refractive indices of transparent solids, liquids, and solutions. It is shown that, as a transparent wedge of small apex angle is illuminated perpendicular to its surface by a monochromatic parallel beam of light, the Fresnel fringes, caused by abrupt change in refractive index at the wedge lateral boundary, are formed on a screen held perpendicular to the beam propagation direction. The visibility of the fringes varies periodically between zero and 1 in the direction normal to the wedge apex. For a known or measured apex angle, the wedge refractive index is obtained by measuring the period length by a CCD. To measure the refractive index of a transparent liquid or solution, the wedge is installed in a transparent rectangle cell containing the sample. Then, the cell is illuminated perpendicularly and the visibility period is measured. By using modest optics, one can measure the refractive index at a relative uncertainty level of 10(-5). There is no limitation on the refractive index range. The method can be applied easily with no mechanical manipulation. The measuring apparatus can be very compact with low mechanical and optical noises.     

How to improve transmissive optics in the very far infrared?

Conclusion We have presented the possibility to make optical coatings on quartz in the FIR and we have got a transmission coefficient as high as 97% at room temperature. It will rise probably close to 100% at liquid helium temperature where the quartz two-phonon difference processes are frozen. The use of polyethylene or TPX is also possible to make plates and lenses. The reflectivity losses are smaller because the refractive index is much smaller, but they cannot be further reduced by any coating because there is no transparent material with n1.2 in the FIR. These lenses are very useful in the FIR (except around 60 cm^–1 if they are made of polyethylene). TPX is quite transparent over the whole FIR range, and also in the visible with nearly the same refractive index as in the FIR. Alignments can be made with visible light, and still work in the FIR.     

Investigations into the mid-infrared Christiansen effect of the dispersive materials

The mid-infrared Christiansen effect was found to occur in the KBr pellets in which powder of the dispersive material -SiC was dispersed. The KBr pellet technique is commonly used for infrared transmission (or absorption) spectroscopy of powders, and when we dispersed in KBr powder a moderate amount of a dispersive material, such as -SiC, and pressed them into a pellet, a transmission spectrum with a sharp peak was obtained. The phenomenon is very interesting, and can be explained with the well-known Lorentz dispersion model accurately. Also, it is very useful for making a new type of mid-infrared band-pass filter, e.g. a mid-infrared Christiansen filter. After performing combinations of some other dispersive materials, such as MgO, with some transparent refractive index matching matrices, such as KCl etc, another aspect of the application of this important classical effect is shown, that is, determining the refractive indices of some mid-infrared transparent materials accurately.     

Novel epoxy-silicone thermolytic transparent packaging adhesives chemical modified by ZnO nanowires for HB LEDs

A novel high transparent thermolytic epoxy-silicone for high-brightness light-emitting diode (HB-LED) is introduced, which was synthesized by polymerization using silicone matrix via diglycidyl ether bisphenol-A epoxy resin (DGEBA) as reinforcing agent, and filling ZnO nanowires to modify thermal conductivity and control refractive index of the hybrid material. The interactions of ZnO nanowires with polymers are mediated by the ligands attached to the nanoparticles. Thus, the ligands markedly influence the properties of ZnO nanowires/epoxy-silicone composites. The refractive indices of the prepared hybrid adhesives can be tuned by the ZnO nanowires from 1.4711 to 1.5605. Light transmittance can be increased by 20% from 80 to 95%. The thermal conductivity of the transparent packaging adhesives is 0.89–0.90 W/mK.