Charge density determination in icosahedral AlPdMn quasicrystal using quantitative convergent beam electron diffraction

Charge density distribution in icosahedral AlPdMn quasicrystal has been studied on a single-crystal specimen by using quantitative convergent beam electron diffraction (QCBED) technique. The QCBED systematic row method was used in the refinement of structure factors. To refine the low-order structure factors, the wave-mechanical formulation of electron diffraction dynamical theory was used in the calculation of electron diffraction intensities for the quasicrystal in fitting the experimental intensity line scan profiles. The shapes of atomic surfaces (occupation domains) were described with symmetry-adapted series of surface harmonics. An iterative procedure was used in determination of structure factors of the quasicrystal. The structure factors of nine strongest symmetry inequivalent reflections according to X-ray diffraction experiment were refined with QCBED technique. The average of refinement results for a given reflection performed on several CBED patterns, which were slightly different in orientation and sample thickness, and on different line scans, was taken as the value of structure factor for the reflection. The obtained structure factors for electrons were transformed into X-ray structure factors with Mott formula. The bonding charge density map for the quasicrystal was constructed with the obtained nine structure factors. Assuming that the atoms are spheres, the gain or loss of electrons for different atoms were calculated. It shows that identical atoms can have different valences at different kinds of positions. The bonding charge is localized along certain directions.     

Determination of the standard deviation of height on a rough surface using interference microscopy

When a rough surface is viewed in an interference microscope with tilt fringes introduced, the effect of the roughness is to reduce the average visibility of the tilt fringes. The relationship between the standard deviation of surface height and the average visibility of the tilt fringes is derived, and experimental results are presented of measurements made on ground glass surfaces using a Linnik interference microscope.     

Surface profile measurement using laser-scanning angle deviation microscopy

Laser-scanning angular deviation microscopy based on the small angle measurement using surface plasmon resonance (SPR) phase detection technique is proposed. The phase shift coming from a SPR sensor is measured by a common-path heterodyne interferometry. This phase deviation is proportional to the beam converging or diverging angle, due to the specimen departing from the focal plane of objective lens. Using the phase deviations, one can calculate the surface profile by use of numerical method. The specimen could be scanned in real-time and the axial-resolution could be better than 1 nm. PACS 07.79-v; 68.37.-d; 73.20.Mf; 42.30.Wb; 42.62.Eh     

Study of normal ocular thermogram using textural parameters

Ocular surface temperature (OST) has been studied with numerous approach and Infrared (IR) thermography has proved to be the best way to capture temperature distribution over some surfaces. It is applied to a number of biomedical applications including studies in the field of ophthalmology. However, the analysis of an ocular thermogram is largely in nascent stage, and is usually achieved by first-order texture analysis. This current study conducted second-order texture analysis on ocular thermal images, mainly by cross co-occurrence matrix together with first-order texture analysis, moments and difference histogram. It was found that, for subjects aged above 35 years old their interocular difference in median, textural contrast, moment 2 and moment 3 (in absolute value) were significantly higher than younger peers. Several significant linear correlations among investigated features were observed. The features extracted from cross co-occurrence matrix may play an important role in the diagnosis of ocular diseases.     

The quantitative analysis of a two-medium mixture using holographic interferometry: the determination of the size corresponding to circular- and rectangular-column voids in a two-medium mixture

The purpose of this paper is to extend the holographic technique to the optical measurement of a two-medium mixture. Assume there exists a void in medium A and the void contains medium B, an experimental technique and the corresponding theories are proposed in this paper, in order to quantitatively determine the size of void in the two-medium mixture. Then the amount of medium B can be determined. An empty glass container was simulated as a void in the mixture. Two different types of glass containers were used and the corresponding theories were derived. The test results show that the errors were in a reasonable range and support the application of holography in the quantitative optical measurement of a two-medium mixture.     

A quantitative determination of magnetic fluctuations in CuGeO3

A polarised neutron scattering investigation has been carried out on a powder sample of CuGeO₃ within the temperature range of 1.5 K to 600 K. The magnetic scattering has been separated from all other contributions by using polarised neutrons and polarisation analysis and placed onto an absolute scale. At low temperatures the long wavelength components of the paramagnetic response are suppressed consistent with the formation of Cu dimers in which the magnetic moments are correlated antiferromagnetically. This form of the scattering persists to temperatures well above the dimerisation temperature T _sp ∼ 14 K. However as the temperature is raised the intensity of the long wavelength spin fluctuations increases and above ∼150 K they are the dominant feature in the wave vector dependence of the response. At all temperatures the observed scattering extrapolates smoothly to the Q = 0 value given by the uniform susceptibility. Consequently the thermal variation of the uniform susceptibility arises from the evolution of the long wavelength magnetic fluctuations. At large wave vectors the energy dependence of the scattering revealed that the response occurs below 16 meV in agreement with the reported maximum magnetic excitation energy at the zone boundary in the ground state. However the total magnetic scattering is significantly less than that expected for a local moment system suggesting that the spectrum of thermal and quantum fluctuations overlap. Received 30 May 2000 and Received in final form 22 March 2001     

ICP-MS: a powerful technique for quantitative determination of gold nanoparticles without previous dissolving

A direct and simple inductively coupled plasma mass spectroscopy (ICP-MS) method for the determination of gold nanoparticles (AuNP) with different particle sizes ranging from 5 to 20 nm and suspended in aqueous solutions is described. The results show no significant difference compared to the determination of the same AuNPs after digestion, as claimed by the literature. The obtained limit of quantification of the method is 0.15 μg/L Au(III) that corresponds to 4.40 × 10⁹ AuNP/L, considering spherical AuNPs 15 nm sized. Spike recovery experiments have shown that the sample matrix is a significant factor influencing the accuracy of the measurement. Spike recoveries from 93% to 95% are found for AuNP samples prepared in trisodium citrate, while for deionized H₂O a spike recovery of around 80% was obtained. The sample preparation mode along with the ICP-MS parameters have been optimized and found to be crucial so as to achieve the required accuracy for the direct quantification of AuNP suspensions. The effect of the nanoparticle size upon the ICP-MS signal also was studied, and only significant differences due to the chemical environment and not to the AuNPs size were found.     

A method of background determination in quantitative auger spectroscopy

A method for automatically determining a structureless background in a measured line spectrum is presented. The model assumptions for the background are given by the sign of the first three derivatives only, and the whole procedure is based on a smoothing spline algorithm. The method is especially designed for background determination in quantitative Auger spectroscopy, but may be modified to cover other topics. Application to measured Auger spectra is demonstrated and the validity of the method discussed.     

Attempt to perform bistatic radio location of the sun using Venera-16

Radiophysics and Quantum Electronics -     

Qualitative and quantitative analysis of atmospheric methanol using a continuous-wave terahertz spectrometer

We present a specific-window method to subtract the interference of water vapor on terahertz frequency-domain spectroscopy(THz-FDS) at ambient temperature and pressure. A continuous-wave spectrometer based on photomixing was utilized to obtain THz-FDS of methanol vapor in the range of 50–1200 GHz. The distinctly spaced absorption features in the neighborhood of atmospheric windows of transparency were selected to perform linear fitting versus the calculated absorption cross section and obtain the concentration of methanol. Furthermore, the gradually decreased methanol vapor was quantified to demonstrate the reliability of the method.     

Multi-exponential analysis of magnitude MR images using a quantitative multispectral edge-preserving filter

A solution for discrete multi-exponential analysis of T(2) relaxation decay curves obtained in current multi-echo imaging protocol conditions is described. We propose a preprocessing step to improve the signal-to-noise ratio and thus lower the signal-to-noise ratio threshold from which a high percentage of true multi-exponential detection is detected. It consists of a multispectral nonlinear edge-preserving filter that takes into account the signal-dependent Rician distribution of noise affecting magnitude MR images. Discrete multi-exponential decomposition, which requires no a priori knowledge, is performed by a non-linear least-squares procedure initialized with estimates obtained from a total least-squares linear prediction algorithm. This approach was validated and optimized experimentally on simulated data sets of normal human brains.     

Wavelength shift determination using a dual-path heterodyne Mach-Zehnder interferometer

This paper introduces a dual-path heterodyne Mach-Zehnder interferometer adopted for wavelength shift determinations. In this interferometer, two parallel incident beams are separated into two interference pairs which are then recombined to generate two interference signals. A parallel plate is placed on the path of one wave of an interference pair, so the phase difference of the interference signals is a function of the plate and beam wavelength, and the interferometer is thus able to determine the wavelength shift of the incident beam. A setup constructed to realize the proposed interferometer is described, it shows that the interferometer has a resolution up to 1.1 × 10⁻¹⁰ (λ²/nm), and the experimental results of applying this setup not only agree the validity of the interferometer but also indicate that the interferometer has a stability of 6.5 × 10⁻¹⁰ (λ²/nm).     

Non-contact blood flow determination using a laser speckle method

An electro-optical device is described which allows the non-contact determination of the skin blood flow and its temporal course. As the laser light penetrates the skin, it is not only scattered from the epidermis but also from the moving red blood cells in the capillaries. The scattered light is time dependent and can be described in terms of the dynamic laser speckle effect. Measurements at the skin demonstrate that there is a so-called ‘involuntary body movement’ which must be taken into account when the measurement of the blood flow is determined. Theoretical considerations show a way to reduce the influence of this movement. Some measurements demonstrate the response of the device to blood flow variations.     

Effects of a small deviation from fermi statistics

By considering a generalized statistics with occupation numbers between Bose-Einstein and Fermi-Dirac statistics we study the resultant distribution when the states differ by a small factor from a Fermi-Dirac distribution. Both the Fermi energy and any level crossing phenomena are sensitive to such statistics; in particular, the electrical conductivity and the free electron heat capacity of fermions at low temperatures receive corrections due to alterations of Fermi-Dirac statistics.     

Emulated super-resolution using quantitative phase microscopy

In the case of coherent illumination, knowledge of the phase and the amplitude of a light wave constitutes complete information. Phase and amplitude information can now be simply acquired using the technique of quantitative phase microscopy. It has been shown that this information allows other imaging modalities to be emulated. In this paper we consider how this information may be used to perform a form of super-resolution by emulating the effect of an annular pupil.     

创设真实的物理课堂教学的尝试

常见的教学是教师备好课，拿到课堂去“演讲”，学生听得头头是道，但遇到具体的问题仍束手无策，其根本的原因是课堂教学失真。