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Regina Peltzmann Bernd Unterweger Hans Junek 《Monatshefte für Chemie / Chemical Monthly》1979,110(3):739-743
The reaction of tetrahydroxy-benzoquinone with malononitrile is reinvestigated. Spectroscopic and chemical methods establish the structure of the product formed as 2,6-diamino-4,8-dihydro-4,8-dioxobenzo(1,2-b:4,5-b)difuran (2a). Alkylethers of tetrahydroxy-benzoquinone react with malononitrile to give tetraalkoxytricyanovinyl-phenols (5). 相似文献
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Formation of a Highly Explosive Valence Isomer of Indene from Dilithiopentalene and Chlorocarbene The principal product of the reaction of dilithiopentalene ( 3 ) with methyllithium and methylene chloride is shown by difference-FT-NMR, spectroscopy to be tetracyclo[4.3.0.03,5.04,6]nona-1,7-diene ( 8 ). This laterally bridged benzvalene derivative explodes violently at temperatures as low as ?40° when concentrated. Controlled rearrangement in diluted solution gives indene ( 4 ). The key step in the formation of the tetracyclic C9H8-compound 8 is suggested to be an intramolecular 1,4-carbene addition. 相似文献
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G. Chancel und F. Parmentier 《Fresenius' Journal of Analytical Chemistry》1886,25(1):118-119
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