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1INTR0DUCTIONa-Thiocarbonylthioformamideshavebeensynthesizedsince1980[l-23,however,thereisn0reP0rtofthesecomP0undsrelatedtheirpropertiesandreactivities(3).Ac-cordingtothepublishedpapers('-",adithioketone,adithioesterandadithioth-ioesteraresnitablefort4 2JcycloadditionwithalkenicandacetylenicdienophileS.Wewanttoknowwhethera-thiocarbonylthioformamideshavethesamecharacters,thereforethereactionofathiobenzoylthioformmorpholine(1)withdiethylacetylenedicarboxylate(2)wasexplored.Theredultsshowth… 相似文献
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J.-C. Wallet E. M. Gaydou J. Jaud A. Baldy 《Acta Crystallographica. Section C, Structural Chemistry》1990,46(8):1536-1540
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John Nicolson Low Antonio Marchal Manuel Nogueras Manuel Melguizo Adolfo Sánchez 《Acta Crystallographica. Section C, Structural Chemistry》2001,57(2):178-179
The title compound, C15H21N5O2, lies on a crystallographic mirror plane and is hydrogen bonded to neighbouring molecules by infinite chains formed by combinations of strong N—H⃛N and soft C—H⃛O hydrogen bonds. The pyrimidine moiety shows extensive delocalization. 相似文献
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