共查询到20条相似文献,搜索用时 15 毫秒
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N. N. Romanova V. A. Budylin G. V. Grishina V. M. Potapov V. N. Torocheshnikov M. L. Demchuk Yu. G. Budel' 《Chemistry of Heterocyclic Compounds》1984,20(12):1354-1357
Phase-transfer catalyzed cyclization of racemic and optically active N-substituted -aminoacids has given racemic and optically active 2-azetidinones, the spatial structures of which have been established by NMR spectroscopy. The original -aminoacids were obtained by adding -phenylethylamine to substituted acrylic acids.Deceased.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 12, pp. 1644–1647, December, 1984. 相似文献
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The 1,3-dipolar cycloaddition reaction of 1-methyl- and 1-(2-phenylethyl)-1,2,3,4-tetrahydropyridines 7 with organic azides 8 afforded the respective 1-substituted-piperidylidene-2-sulfon(cyan)amides 9. Nitration of the 1-(2-phenylethyl) analogue 9o yielded the 1-[2-(4-nitrophenyl)ethyl] derivative 9r which on reduction with palladium-on-charcoal and hydrazine gave the 1-[2-(4-aminophenyl)ethyl] analogue 9s. 相似文献
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Six new 2-(2-phenylethyl)chromones from Agarwood 总被引:1,自引:0,他引:1
Six new chromones, 6-methoxy-2-[2-(3-methoxy-4-hydroxyphenyl)ethyllchromone (2), 6,8-dihydroxy-2-(2-phenylethyl)chromone (3), 6-hydroxy-2-[2-(4-hydroxyphenyl)ethyl]chromone (4), 6-hydroxy-2-[2-(2-hydroxyphenyl)ethyl]chromone (5), 7-hydroxy-2-(2-phenylethyl)chromone (6), and 6-hydroxy-7-methoxy-2-(2-phenylethyl)chromone (7) were isolated from the ether extract of agarwood in addition to a known compound, 2-(2-phenylethyl)chromone or flidersiachromone (1). Their structures were determined by spectroscopic methods including UV, IR, and NMR spectral data and comparisons with the calculated values using the hydroxyl and methoxyl substituent increments of the chromone ring. 相似文献
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《Tetrahedron: Asymmetry》2005,16(5):949-952
An efficient oxidation of (2′R)-(−)-2′-phenyl-2′-(piperidin-1-yl)ethanol 2 with bromine to generate the corresponding piperidin-2-one 3 in 96% is described. In addition, starting from 3, (2′S,3R)-(+)-stenusine 8 was synthesized in 70% overall yield. The X-ray analysis of piperidine 6·HCl is also reported. 相似文献
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ZHANG Lan-ping WANG Ya-lou 《高等学校化学研究》2010,(2):245-248
5-Hydroxy-2-(2-phenylethyl)chromone(1) was synthesized from 2,6-dihydroxyacetophenone(7) obtained via four-steps resorcinol-reacting with phenylpropionic acid,the procedures involved are Baker-Venkataraman rearrangement and cyclization which are easy to conduct,the overall yield is 32%. 相似文献
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2-(2-Phenylethyl) chromone (PEC), an uncommon class of chromones, possesses a phenylethyl substituent at the C2 position. They have been isolated from a few plant species. They have promising biological activities such as neuro-protective, cytotoxic, acetylcholinesterase inhibitory, antibacterial and anti-inflammatory. This review focuses on the naturally occurring PEC derivatives, their sources, physical and spectral data, as well as biological activities. 相似文献
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Benito Alcaide Carmen Lopez-Mardomingo Rafael Perez-Ossorio Joaquin Plumet 《Journal of heterocyclic chemistry》1982,19(1):45-48
Treatment of the diastereoisomeric N-(1-phenylethyl)-1,2-diphenyl-2-aminoethanols with benzaldehyde yields stereospecifically N-(1-phenylethyl)-2,4,5-triphenyloxazolidines with four chiral centers. The configurations of these oxazolidines are established through their ring-opening reactions with methylmagnesium iodide and subsequent oxidation with lead tetracetate. 相似文献
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