晶粒大小分布对纳米晶磁体Pr2Fe14B剩磁和矫顽力的影响

用微磁学有限元法计算了纳米晶磁体Pr2Fe14B的退磁曲线，文中模拟了三种具有不同晶粒大小分布的样品。计算结果表明，剩磁增强与磁体的晶粒尺寸分布情况无关而依赖于平均晶粒直径。晶粒尺寸分布对矫顽力的影响与磁体中的晶间交换耦合作用密切相关。     

纳米复合永磁材料中软磁性相交换硬化的研究

本文就纳米复合永磁材料中软磁相被交换硬化问题,从一维模型和三维模拟计算进行了分析研究. 一维和三维各向异性样品研究表明,在相同微结构下,当硬磁相的各向异性降低时,除矫顽力降低外,在磁矩全部反转之前退磁曲线是一样的. 因此,硬磁相各向异性的降低不会导致最大磁能积(BH)_max增大和剩磁增加. 对于三维各向同性样品的模拟计算表明,降低硬磁相的各向异性会使剩磁和(BH)_max都明显降低. 因此,增强硬磁相的各向异性并增大硬磁相晶粒尺寸是提高 关键词： 纳米复合永磁 矫顽力 剩磁 磁能积     

C掺杂FePt铁磁薄膜光诱导超快退磁动力学研究

FePt合金薄膜由于具有较强的磁各向异性而在磁信息和磁光信息存储中具有重要的应用.C掺杂可精确调控薄膜的磁各向异性,从而可有效地改变薄膜的矫顽场.通过超短激光脉冲与铁磁薄膜相互作用,可以获得非平衡状态下电子、自旋和晶格等自由度之间的动态耦合参数,这是研究超快磁记录材料的物理基础.本文基于瞬态磁光Kerr效应,研究了两种C掺杂浓度下FePt薄膜的超快磁光响应.实验结果表明:瞬态Kerr信号与外加磁场正相关,磁场反向,Kerr信号反号,而瞬态反射率与外加磁场无关;不同C掺杂的FePt薄膜的矫顽场不同,软磁的退磁时间显著小于硬磁薄膜的退磁时间.我们还观测到超快激光在铁磁薄膜中诱导频率约为49 GHz的相干声学声子,该声子的频率与外加磁场无关.实验结果为设计和研制新型磁光薄膜提供了实验依据.     

Ti(Cr)缓冲层对用于垂直磁记录材料CoCrTa介质磁特性和微结构的影响

利用直流对靶磁控溅射技术在单晶Si衬底上制备了C/CoCrTa/X (X=Cr，Ti)介质材料.分别采用振动样品磁强计、X射线衍射仪、扫描探针显微镜对样品的磁性、微结构等进行了测试分析.研究发现，Ti缓冲层有利于样品中Co晶粒的易轴垂直于膜面生长.以Ti为缓冲层的样品，颗粒尺寸和表面粗糙度较小，而且磁畴明显，说明以Ti为缓冲层的薄膜样品更适宜做垂直磁记录. 关键词： CoCrTa 垂直磁记录 缓冲层 微结构     

通过磁化曲线计算磁熵值

在恒定低磁场下测量磁性物质的M T 曲线,可以确定其居里点;在居里点附近测量一系列等温磁化曲线M H,根据磁化曲线并借助于磁系统的热力学关系式,通过数值计算方法得到磁性材料在施加或撤去外磁场过程中的磁熵变化值.     

霍尔法磁化曲线与磁滞回线实验仪的退磁技巧

针对用HM-1霍尔磁化曲线和磁滞回线实验仪对实验样品铁磁材料退磁过程中退磁难的问题,采用对称退磁法.即在退磁过程中,视铁磁样品中剩磁的方向、剩磁值的多少,加上相应值的反向磁场即矫顽磁力,构成逐渐缩小且最终趋于原点的循环退磁曲线,从而达到给铁磁样品快速退磁的目的,提高了实验教学质量.     

纳米晶永磁材料晶间交换耦合作用的模拟计算研究

利用微磁学有限元法，模拟计算了单相和复相各向同性纳米晶磁体的起始磁化曲线、退磁曲线和回复曲线.验证了用δm(H)曲线的正峰值来衡量纳米晶磁体晶间交换耦合作用的有效性.计算 结果表明，纳米晶单相和复相磁体的晶间交换耦合作用都随晶粒尺寸的增加而降低，当晶粒尺寸过大时 复相磁体表现出两相行为，其δm(H)曲线出现了两个正峰值.分析表明，外场较小的正峰值是软磁相与硬磁相晶粒之间交换耦合作用的结果，而外场较大的正峰值是硬磁相晶粒之间交换耦合作用的结果. 关键词： 纳米晶永磁 晶间交换耦合 δm(H)曲线     

陶瓷超导体的磁化强度和临界电流密度

假定晶内临界电流密度 Jc 为常量(Bean 模型),由磁化强度定义直接计算了四种形状的晶粒的不可逆磁化强眨 M 与 Jc 的关系,得到了相应的 Jc(△M)中的几何因子修正量.对第二类超导体,退磁场和退磁因子在 Meissner 态和H_(c1)附近的混合态仍是重要的,在其余磁场中都可以忽略.对氧化物陶瓷超导块,由于弱连接,晶间磁场近似等于外场.讨论了块样中非超导部分对实验测量的磁化强度■及 Jc 估算的影响.     

晶粒易轴取向度对纳米晶永磁Pr2Fe14B磁性的影响

构造了立方和不规则形状晶粒的各向异性纳米晶单相Pr₂Fe₁₄B磁体 .利用微磁学的有限元法，模拟计算了样品的磁滞回线.计算结果表明，随着磁体晶粒易轴取向度的变差， 磁体的剩磁、矫顽力均随之下降.不同晶粒尺寸的纳米晶单相Pr₂Fe_{14B磁体，其磁 性能随取向度的变化快慢不同，原因在于磁体中的晶间交换作用 (IGEC) 的强弱不同.随着 晶粒取向度的提高，纳米晶单相磁体的矫顽力逐渐增加，这完全不同于烧结磁体. 关键词： 纳米晶磁体 矫顽力 剩磁}     

各向同性纳米结构Fe-Pt薄膜的结构和磁性

采用直流溅射和热处理技术制备了两个各向同性的纳米结构Fe-Pt永磁合金薄膜系列,并研究了它们的结构和磁性.研究表明,在富Fe双相纳米结构Fe-Pt永磁合金薄膜中,仅由硬磁的FePt相与软磁的Fe₃Pt相组成;在同一系列中,随Fe层厚度的增加,饱和磁极化强度和剩磁明显增大.由Kelly-Henkel图研究指出,在上述Fe-Pt纳米结构永磁合金薄膜中,磁相互作用主要由近邻纳米晶粒间的铁磁交换相互作用控制. 关键词： 磁性薄膜 纳米结构 矫顽力     

Measurement of inter-particle interactions in a single magnetic ink aggregate

Using an alternating gradient force magnetometer, remanence curves have been recorded from a single aggregate of a commercial ink used in magnetic particle inspection. The aggregates were typically 100x30x30 μm³ size. Analysis of the isothermal and demagnetization remanence magnetization shows that inter-particle interactions within the aggregates act always to lower the magnetization of the aggregate.     

The demagnetization tensor of a cylinder

All independent components of the demagnetization tensor of a cylinder are expressed by means of tabulated functions. That allows to determine the demagnetizing field of a cylinder homogeneously magnetized along an arbitrary direction. As an example the demagnetizing field is computed over the endface of a cylinder homogeneously magnetized perpendicular to its axis of rotation.     

Magnetization distribution in magnetic films studied with Larmor-encoding

Additional information about the magnetization distribution in magnetic films is obtained with a 3D-polarimetry set-up. A pilot experiment was performed with the neutron polarization aligned perpendicular to the surface of a Fe-film in a magnetic field parallel to its surface. The Larmor-precession in the magnetic field between two current sheets was used to adjust the neutron polarization perpendicular to the sample surface. This new polarization-magnetization configuration was probed with a Fe-film in specular and off-specular scattering. The off-specular scattering is created by the magnetic domain structure of the Fe-film in remanence. The results of specular and off-specular scattering are reproduced by calculations for the configuration of the incoming neutron polarization parallel to the sample surface and the magnetic field and for the configuration of the incoming neutron polarization perpendicular to the sample surface and the magnetic field.     

Phase distribution and computed magnetic properties of high-remanent composite magnets

Numerical micromagnetic calculations using finite-element techniques allow a quantitative treatment of the correlation between the microstructure and the basic magnetic properties of two-phase permanent magnets such as the remanence, the coercive field and the maximum energy product. For the investigation of (A) the role of the amount of the soft magnetic phase, and (B) the effect of grain shape, realistic three-dimensional grain arrangements have been used. The numerical results show that both short-range exchange and long-range magnetostatic interactions determine the magnetic properties. The optimal microstructure of an isotropic nanocrystalline permanent magnet was found to consist of soft magnetic particles with a large spontaneous magnetization embedded between hard magnetic grains. Exchange interactions than enhance the remanence of isotropic, composite magnets of Nd₂Fe₁₄B and -Fe by about 60%. Because of exchange hardening the soft magnetic phase can be increased up to 50% without a significant loss of coercivity. A uniform grain structure suppresses strong demagnetizing fields and this increases coercivity by 30% as compared with irregular shaped particles.     

Influence of the demagnetizing factor on the magnetization of an ensemble of Stoner-Wohlfarth particles

The influence of the demagnetizing factor on the coercivity of a sample of oriented uniaxial Stoner-Wohlfarth particles is investigated in the approximation of a relaxation model with a self-consistent determination of the demagnetization field. The demagnetizing field is shown to change the particle magnetization reversal conditions and to reduce the blocking temperature and coercivity, for which, despite allowance for the demagnetizing field, the Neel-Brown relation holds. It is also shown that under the demagnetizing field, the internal magnetic field in which the particles are located is not stationary but varies with time concordantly with the time sweep of the temperature during magnetization in a constant external field after zero-field cooling (ZFC). Nonstationarity of the internal field in the ZFC regime causes the interval of transition temperatures of the ensemble particles from a blocked state to a state with equilibrium magnetization to increase.     

磁头-磁盘接触作用力对磁记录层信息强度影响规律的定量研究

磁存储密度的持续增长会导致磁头-磁盘的间距不断减小, 这样, 极有可能引起磁头-磁盘接触退磁的发生, 从而造成磁记录层存储数据的丢失. 为了明确退磁过程中的相应作用关系, 本文通过磁力显微镜的相位成像原理直接给出了磁盘退磁的定量测量方法. 并且依据此方法, 利用纳米划痕实验研究了磁头-磁盘接触作用力对磁记录层信息强度的影响规律. 结果表明:当磁头-磁盘接触作用力超过临界退磁载荷时, 磁记录层的信息强度与磁头-磁盘接触作用力之间存在减函数关系; 在低接触载荷区域中, 即使磁记录层表面没有划痕产生, 磁盘退磁现象仍旧可能发生; 对于任意磁头-磁盘接触作用力, 磁盘表面的破坏区域总是会大于磁记录层的退磁区域; 当磁头反复划刮磁盘的同一位置时, 磁记录层的表面划痕处将出现弹性安定状态, 对应地, 磁记录层的信息强度会趋近于某一定值.     

Remanence due to wall magnetization and counterintuitive magnetometry data in 200-nm films of Ni

200-nm-thick Ni films in an epitaxial Cu/Ni/Cu/Si(001) structure are expected to have an in-plane effective magnetic anisotropy. However, the in-plane remanence is only 42%, and magnetic force microscopy domain images suggest perpendicular magnetization. Quantitative magnetic force microscopy analysis can resolve the inconsistencies and show that (i) the films have perpendicular domains capped by closure domains with magnetization canted at 51 degrees from the film normal, (ii) the magnetization in the Bloch domain walls between the perpendicular domains accounts for the low in-plane remanence, and (iii) the perpendicular magnetization process requires a short-range domain wall motion prior to wall-magnetization rotation and is nonhysteretic, whereas the in-plane magnetization requires long-range motion before domain-magnetization rotation and is hysteretic.     

Interface biquadratic coupling and magnon scattering in exchange-biased ferromagnetic thin films grown on epitaxial FeF2

The magnetic anisotropy of ferromagnetic (FM) Ni, Co, and Fe polycrystalline thin films grown on antiferromagnetic (AF) FeF(2)(110) epitaxial layers was studied, as a function of temperature, using ferromagnetic resonance. In addition to an in-plane anisotropy in the FM induced by fluctuations in the AF short-range order, a perpendicular (biquadratic) magnetic anisotropy, with an out-of-plane component, was found which increased with decreasing temperature above the AF Neél temperature (T(N) = 78.4 K). This is a surprising result given that the AF's uniaxial anisotropy axis was in the plane of the sample, but is consistent with prior experimental and theoretical work. The resonance linewidth had a strong dependence on the direction of the external magnetic field with respect to in-plane FeF(2) crystallographic directions, consistent with interface magnon scattering due to defect-induced demagnetizing fields. Below T(N), the exchange bias field H(E) measured via FMR for the Ni sample was in good agreement with H(E) determined from magnetization measurements if the perpendicular out-of-plane anisotropy was taken into account. A low field resonance line normally observed at H ≈ 0, associated with domain formation during magnetization in ferromagnets, coincided with the exchange bias field for T < T(N), indicating domain formation with the in-plane FM magnetization perpendicular to the AF easy axis. Thus, biquadratic FM-AF coupling is important at temperatures below and above T(N).     

磁性纳米颗粒系统偶极相互作用的Monte Carlo研究

采用局域Monte Carlo方法模拟不同易轴分布的简单立方排列单分散单畴Fe纳米颗粒系统的ZFC-FC曲线及磁滞回线.结果表明：随着偶极相互作用的增强，系统的阻塞温度T_B逐渐增大，且ZFC曲线的峰变宽.说明偶极相互作用使得系统的有效能垒提高，分布宽度增加.研究FC曲线磁化强度的倒数与温度关系，发现偶极相互作用系统中存在反铁磁有序.系统的阻塞态及超顺磁态的磁滞回线表明，极低低温下，随着偶极相互作用的增强，系统的矫顽力和剩磁减小，偶极相互作用阻碍系统的磁化；系统处于超顺磁态，各向异性作用及偶极相互作用使得系统的磁化曲线偏离Langevin曲线且偶极相互作用展现出退磁相互作用效应.偶极相互作用增强，系统磁化曲线与Langevin曲线偏差量的最大值向低场移动.在偶极相互作用下，易轴与外场夹角为45°的磁性纳米颗粒系统的平均有效能垒和有效能垒分布宽度较易轴随机分布系统的大.