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利用在硫酸条件下香草醛与黄芪甲甙的荧光反应测定黄芪口服液中的黄芪甲甙,黄芪甲甙与香草醛反应产物的最大激发波长为λex=368nm,最大发射波长λem435nm。黄芪甲甙在0.0-30.0mg/L范围呈良好的线性关系,最低检出限为0.3μg/mL,测定样品的回收率为96.72%-103.30%。 相似文献
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中草药黄芪中6种微量元素的溶出率研究 总被引:8,自引:2,他引:6
火焰原于吸收法测定了中草药黄芪原生药及汤剂中6种微量元素Cu、Zn、Mn、Fe、Mg、Sr的含量,并对其溶出率进行了计算。结果发现,6种元素的溶出率存在一定差异,Sr溶出率最大,为24.8%;Fe元素溶出率最小,为3.42%。该结果为黄芪的有效成分研究提供了基础数据。 相似文献
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HPLC测定黄芪药材中的毛蕊异黄酮葡萄糖苷 总被引:1,自引:0,他引:1
采用高效液相色谱法(HPLC)对我国7个省68个黄芪样品进行了毛蕊异黄酮葡萄糖苷成分的含量测定.以毛蕊异黄酮葡萄糖苷含量作为衡量优劣指标,建立了黄芪药材质量标准,研究不同产地黄芪药材的质量.7个省68个黄芪药材样品检测结果表明,不同产地黄芪药材毛蕊异黄酮葡萄糖苷成分的含量差异较大,其中:山西>内蒙>甘肃>辽宁;不同品种黄芪药材毛蕊异黄酮葡萄糖苷成分的含量差异较大,其中:栽培品种<野生品种;生长年限不同,毛蕊异黄酮葡萄糖苷成分的含量也不同,其中:二年生>五年生>三年生>四年生.采用HPLC进行黄芪药材的质量评价切实可行,为制药企业选用黄芪药材提供科学、可靠的依据. 相似文献
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建立黄芪药材质量标准,研究不同产地黄芪药材的质量.采用高效液相色谱法(HPLC),对我国7个省68个黄芪样品进行了芒柄花素成分的含量测定,以芒柄花素含量作为衡量优劣指标.7个省68个黄芪药材样品检测结果表明,不同产地黄芪药材芒柄花素成分的含量差异较大,其中:山西>内蒙>甘肃>辽宁;不同品种黄芪药材芒柄花素成分的含量差异较大,其中:栽培品种<野生品种;生长年限不同,芒柄花素成分的含量也不同,其中:二年生>四年生>五年生>三年生.采用HPLC进行黄芪药材的质量评价切实可行,为制药企业选用黄芪药材提供科学、可靠的依据. 相似文献
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本文报道了掺钬镱离子的氟氧化物玻璃陶瓷的一级和二级红外量子剪裁的比较研究.研究发现当0G5能级到0&能级及之间的能级被激发的时候,大多数的粒子数容易无辐射弛豫到(5F4^5S2)能级.在(0F40&)能级,由很强的ET7-ETaYb{5F4(Ho)→5I6(Ho),2F7/2(Yb)→2F5/2(Yb))交叉能量传递渠道,导致Ho3+离子的粒子数被无损耗的交叉能量传递到5I6能级,同时Yb3+离子从基态2F7/2能级被激发到2F5/2能级,它导致了两个能被晶体硅有效吸收的红外光子,即一个(1153am,1188am)的红外光子和另一个(973.0nm,1002.0nm)的红外光子,因此出现了显著的双光子一级红外量子剪裁.最后,该文计算了Ho(0.5)Yb(1):FOV和Ho(0.5)Yb(10.5):FOV的交叉能量传递效率为ηtr,1%Yb(5FS2)=29.2%,‰,10.5%Yb(5F4^5S2)=99.2%和它们的共合作能量传递效率为ηtr,1%Yb(5F3)=4.18%,ηtr,10.5%Yb(5F3)=75.3%;而它们的双光子量子剪裁效率的理论上限值依次为ηCR,1%Yb(5F4^5S2)=129.2%,ηCR,10.5%Yb(5F4^5S2)=199.2%和ηCO,1%Yb(5F3)=104.18%,ηCO,10.5%Yb(5F3)=175.3%.因此发现了一级红外量子剪裁有比二级红外量子剪裁高较多的概率.该项研究对太阳能电池效率的提高很有意义. 相似文献
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Guided-Wave Two-Dimensional Acousto-Optic Scanner Using Proton-Exchanged Lithium Niobate Waveguide 总被引:1,自引:0,他引:1
Two-dimensional scanning of a 0.6328 mum guided-light beam has been realized using noncolinear acousto-optic (AO) coplanar Bragg diffraction together with colinear AO guided-mode to substrate radiation-mode conversion in a Z-cut Xpropagation LiNbO3 proton-exchanged (PE) waveguide. The two surface acoustic (SAW) waves utilized are at the center frequencies of 500 and 200 MHz, propagating in the Y and X axes, respectively. Two-dimensional scanning of approximately 720 resolvable light beam spots, namely, 18 40 (horizontal vertical) scanning, has been demonstrated using a light beam of 1.0 mm aperture. The total number of resolvable beam spots can be greatly increased from 720 by simply utilizing SAW transducers of larger bandwidth and a light beam of greater aperture. It should also be possible to significantly increase the diffraction efficiency from 3 % by optimizing the parameters of the PE waveguide and the SAWs. 相似文献
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A review of schemes for multiple access in fiber optic networks shows that a hybrid of wavelength and code division multiple access (WCDMA) combines the best features of both. In particular, the hybrid scheme retains the large information carrying capacity of wavelength division multiple access (WDMA) and flexibility of code division multiple access (CDMA). In this paper WDMA, optical CDMA (OCDMA), and WCDMA networks are discussed. In OCDMA networks, concept of incoherent and coherent coding including inverse decoding and matched filter is introduced. The delay performance of both WDMA and WCDMA networks, under the simple suboptimum access protocols based on cyclic search, is computed. It has been shown quantitatively that tuning delay significantly affects the delay performance of both WDMA and WCDMA networks. Futhermore, delay performance of WCDMA networks is always better than the WDMA networks for the same tuning delay, load, and number of users. 相似文献
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S. G. Nedel’ko M. A. Krysyuk A. L. Apanasenko L. N. Lymarenko Z. T. Moroz 《Journal of Applied Spectroscopy》1997,64(1):55-61
Results of a study of the effect of γ-radiation on the spectral luminescence properties of cadmium tungstate crystals doped
with silver, bismuth, and molybdenum cations are presented. Spectral characteristics of the nondnnnoped crystals are briefly
described. Absorption and photo and X-ray luminescence spectra of the crystals taken before and after exposure to γ-radiation
(5.5·104 Gy) are compared. It is found that the spectral characteristics of the crystals doped with silver, bismuth, and molybdenum
cations do not change markedly after the exposure. The relation between the type of impurity-induced defects, individual characteristics
of the impurity cations, and the character of the effect of γ-radiation on the spectral luminescence properties of impure
crystals is analyzed (preliminarily).
Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 64, No. 1, pp. 55–60, January–February, 1997. 相似文献
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A simple technique of pulse compression, based on the linear chirp compensation of self-phase modulation (SPM) spectra in dispersion shifted fibers, is demonstrated. The optimization procedure is carried out, for a short span of a single-mode fiber, using a parabolic law, which describes the behavior of the squared output pulse width versus the pump peak power in the case of Gaussian pulses. The experimental results give a minimum pulse duration of 233 fs, which is in good agreement with the model. Shorter and coherent pulses, down to 90 fs, have been obtained by inserting an interference filter at the optical output. 相似文献
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The Shanghai Synchrotron Radiation Facility(SSRF)booster ring,a full energy injector for the storage ring,is deigned to accelerate the electron beam energy from 150MeV to 3.5GeV that demands high extraction efficiency at the extraction energy with low beam loss rate when electrons are ramping.Closed orbit distortion(COD)caused by bending magnet field uniformity errors which affects the machine performance harmfully could be effectively reduced by bending magnet location sorting.Considering the affections of random errors in measurement,both ideal sorting and realistic sorting are studied based on measured bending magnet field uniformity errors and one reasonable combination of bending magnets which can reduce the horizontal COD by a factor of 5is given as the final installation sequence of the booster bending magnets in this paper. 相似文献
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We measure the waveform and phase curves of short optical pulses before and after transmission over different lengths of fibers by use of the pulse analyzer with the frequency-resolved optical gating (FROG),and numerically simulate pulse evolution under the experimental conditions.The nonlinear coefficient of the fiber is given by comparing the experimental results with the numerical ones.Difference between the experiment and numerical simulation is analyzed. 相似文献
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Resonance scattering of elastic spherical shell and cylindrical shell while the surrounding fluid medium has absorption is studied. The normal mode solution derived using exact elastic theory and the separation of variables is still applicable. However, the scattering form function has to be modified for the absorbing medium, otherwise the unreasonable result would be obtained. The backscattering form function in the absorbing medium is redefined, and the form function of elastic spherical and cylindrical shell with vacuum or solid matter filled is calculated in various absorption conditions. The results show that the absorption of surrounding fluid leads to notable attenuation of the coincidence resonances in the mid-frequency, but it has a little influence on the low-frequency resonance scattering induced by the filler inside the shell. 相似文献
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A versatile and low-cost single-beam self-referenced phase-sensitive surface plasmon resonance(SPR)sensing system with ultra-high resolution performance is presented.The system exhibits a root-mean-square phase fluctuation of ±0.0028.over a period of 45 min.i.e.a resolution of±5.2×10-9 refractive index units.The enhanced performance has been achieved through the incorporation of three design elements:a true single-beam configuration enabling complete self-referencing so that only the phase change associated with SPR gets detected,a differential measurement scheme to eliminate spurious signals not related to the sensor response,and the elimination of retardation drifts by incorporating temperature stabilization in the liquid crystal phase modulato .Our design should bring the detection sensitivity of non-labeling SPR biosensing closer to that achievable by conventional fluorescence-based techniques. 相似文献
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Ta2O5 films are prepared on BK7 substrates with conventional electron beam evaporation deposition.The effects of SiO2 protective layers and annealing on the laser-induced damage threshold (LIDT) of the films are investigated.The results show that SiO2 protective layers exert little influence on the electric field intensity(EFI)distribution,microstructure and microdefect density but increase the absorption slightly.Annealing iS effective on decreasing the microdefect density and the absorption of the films.Both SiO2 protective layers and annealing are beneficial to the damage resistance of the films and the latter is more effective to improve the LIDT.Moreover,the maximal LIDT of Ta2O5 films is achieved by the combination of SiO2 protective layers and annealing. 相似文献