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Analytical and Bioanalytical Chemistry - 相似文献
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《Journal of organometallic chemistry》1987,320(1):129-136
μ3-Allyl-μ1-chloro-bis(triphenylphosphine)dipalladium(I) was obtained by the reaction of (π-C3H5PdCl)2 with P(C6H5)3 and NaOCH3. The X-ray structure analysis of the yellow air-stable crystals confirms the presence of a PdPd bond (2.623 Å) and a bridging μ3-allyl group. The PdC distances to the terminal carbon atoms of the allyl group are 2.07(1) Å. The distances of the Pd atoms to the bridging chloride ion are 2.433(3) and 2.438(3) Å. 相似文献
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《Journal of Coordination Chemistry》2012,65(24):3930-3939
{Cu4Br5[(η 5-C5H4PPh2)(η 5-C5H5)Co]4}[PF6]3, [(η 5-C5H4PPh2)(η 5-C5H5)Co]+ = ((η 5-cyclopentadienyl)[η 5-1-(diphenylphosphino) cyclopentadienyl] cobaltocenium) and {Ag(NO3)(CH3COCH3)[(η 5-C5H4PPh2)(η 5-C5H5)Co]} n [PF6] n have been synthesized and characterized by elemental analyses, infrared spectroscopy, X-ray diffraction techniques, and by cyclic voltammetry. {Cu4Br5[(η 5-C5H4PPh2)(η 5-C5H5)Co]4}[PF6]3 contains four coplanar copper atoms bridged by four μ-Br and one central μ 4-Br occupying the apex of a square pyramid, and {Ag(NO3)(CH3COCH3)[(η 5-C5H4PPh2)(η 5-C5H5)Co]} n [PF6] n affording a 1-D coordination zigzag polymer. 相似文献