四硫代钼酸锌的热稳定性及润滑性能研究

合成了四硫代钼酸锌粉末并考察了其作为固体润滑剂在室温至５００℃下的润滑作用;同时采用热重分析对其热稳定性进行了评价,用Ｘ射线光电子能谱对磨损表面典型元素的化学状态进行了分析。结果表明：四硫代钙酸锌在大气中的第一分解温度为２３５．５℃,第二分解温度为７１０．８℃,分解产物为ＺｎＭｏＯ４;在Ｎ２中的分解温度为３６２．８℃和５０７．８℃,产物分别为ＺｎＭｏＳ２和ＺｎＭｏＳ．摩擦磨损试验结果表明,Ｓｉａｌ     

硫代钼酸镍的热稳定性及其摩擦学性能研究

采用X射线衍射和电子探针鉴定了硫代钼酸镍的结构及其经不同温度加热或高温摩擦磨损试验后磨损表面产物的结构和成分,用热重法对其热稳定性进行了评价。在四球摩擦磨损试验机和硝-盘式高温摩擦磨损试验机上考察了其作为油品剂及固体润滑剂的摩擦学特性,探讨了其作为固体润滑剂在升温过程中可能发生的化学变化及其对润滑性能的影响。结果表明：硫代钼酸镍的氮气流中表现出较好的热稳定性。在空气中于350℃左右开始变化氮化分解;其高温氮化分解产物MoO3和MoS2具有明显的减摩作用,因此硫代钼酸镍可用作室温到高温（20～800℃）下的固体润滑剂。     

石墨对聚四氟乙烯镶嵌轴承摩擦学性能的影响

作者利用端面摩擦试验机考察了几种石墨与聚四氟乙烯复合固体润滑剂镶嵌锡青铜材料的摩擦磨损性能，发现石墨的添加不仅可以提高聚四氟乙烯镶嵌铀承的耐磨性，而且还可以降低和稳定摩擦系数。通过Ｘ射线衍射、Ｘ射线光电子能谱和电子探针等对摩擦表面转移膜的化学组成和主要元素含量的变化及表面形貌的分析观察，作者认为石墨的减摩作用是其促进聚四氟乙烯向摩擦表面转移并使之在轴承表面形成均匀覆盖的固体润滑剂转移膜，从而有效地     

用XPS对银基自润滑复合材料摩擦磨损特性的考察

作者用X-射线光电子能谱(XPS)考察了几种制备工艺对银比二硫化钼为90比10的自润滑复合材料表面的硫、钼、银等化学元素的价态的影响,并用XPS和光学显微镜重点考察了不同温度下的上述自润滑复合材料与两种对摩偶件的摩擦、磨损特性。结果表明:对摩偶件摩擦面上的转移膜的固体润滑剂中钼的价态变化是影响该自润滑复合材料摩擦磨损特性的主要因素。     

二硫代二苯甲酸二异辛酯作为铜、铝合金润滑剂的摩擦学性能及机理研究

以具有特殊双硫醚结构的二硫代二苯甲酸和异辛醇为原料合成了酯类润滑油二硫代二苯甲酸二异辛酯(Phe-S-C_i8).采用微动摩擦磨损试验机对其在不同摩擦副上的润滑性能进行评价，使用X射线光电子能谱及扫描电镜对磨斑表面形貌及元素状态进行了表征，对影响其摩擦学性能的因素进行了深入探究.研究结果表明，与参照样1088和Phe-3C_i8相比，Phe-S-C_i8具有更好的氧化安定性及热稳定性，其作为钢/铜摩擦副的润滑剂，具有一定的减摩抗磨效果；作为钢/铝摩擦副的润滑剂，具有较好的减摩抗磨性能.Phe-S-C_i8在以上两种摩擦副上表现出显著优于参照样的极压承载能力.通过对磨斑表面元素进行分析可知，Phe-S-C_i8在钢/铜摩擦副上的减摩抗磨性能主要归因于润滑剂分子在摩擦副表面的物理吸附作用，其在钢/铝摩擦副间的减摩抗磨性能主要归因于Phe-S-C_i8与摩擦界面间的化学反应.     

锡青铜镶嵌固体润滑剂轴承的摩擦学特性

在栓－盘式端面摩擦磨损试验机上于常温干摩擦条件下，对锡青铜轴承和镶嵌固体润滑剂（ＰＴＦＥ和石墨等复合物）的锡青铜轴承进行了摩擦学性能的对比试验研究．结果表明，几种固体润滑剂嵌入量不同的镶嵌轴承的摩擦系数都明显降低，耐磨性均比对照轴承的高２个数量级，其中以固体润滑剂嵌入面积分数为３０％的轴承的摩擦磨损性能最好．利用Ｘ射线微区分析仪、扫描电子显微镜和能量色散谱仪等，对磨损表面和磨屑的形貌、表面转移膜和元素的面分布等作了观察与分析，指出摩擦界面，尤其轴承金属摩擦表面固体润滑剂转移膜的形成是提高轴承性能的关键，锡青铜镶嵌固体润滑剂轴承以粘着磨损和疲劳磨损为主要磨损机理     

氟代二酮的摩擦学特性及抗磨机理研究

采用Optimal SRV型微动摩擦磨损试验机评价了氟代二酮作为润滑油及其添加剂的摩擦学性能，并通过钢盘磨损表面的X射线光电子能谱和扫描电子显微镜分析探讨了氟代二酮的减摩抗磨作用机理．结果表明，氟代二酮的摩擦学性能受其化学结构和试验载荷的影响；烷基芳基二酮的抗磨效果最好；摩擦过程中氟代二酮在摩擦副表面发生了摩擦化学反应，形成了由化学反应膜和吸附膜构成的边界润滑膜，从而起到减摩抗磨作用．     

季膦盐离子液体对钢/锡青铜的摩擦磨损性能研究

合成了几种三丁基烷基四氟硼酸季膦盐离子液体,用核磁共振氢谱仪表征其结构,用差热分析仪测定其热稳定性,在SRV摩擦磨损试验机上评价其作为润滑剂对钢/锡青铜摩擦副的摩擦磨损性能,并与磷嗪X-1P和2-乙基-3-己基咪唑四氟硼酸盐(L-P206)进行比较,采用X射线光电子能谱仪和扫描电子显微镜分析磨损表面元素的化学状态及其磨斑形貌.结果表明,三丁基烷基四氟硼酸季膦盐离子液体的热稳定性和抗氧化性能较好,作为钢/锡青铜摩擦副润滑剂具有优异的摩擦磨损性能,摩擦系数极低(＜0.05),抗磨性优于常规二烷基咪唑基离子液体.     

WC／Ti合金在水基润滑剂润滑下的摩控磨损机理研究

通过分子改造在添加剂分上入亲水基团,制备出了水溶骨添加剂,在Ｔｉｍｋｅｎ试验机上考究了ＷＣ／Ｔｉ合金体系在水基润滑剂润滑下的摩擦磨损行为及其摩擦化学反应机理。采用扫描电子显微镜和Ｘ射线光电子能谱分析表征ＷＣ涂层磨损表面,结果发现在涂层表面有明显的Ｔｉ转移,并形成多元氧人物,表明在水基润滑条件下摩擦过程中发生摩擦氧化反应,而多元氧化物层的性质是丰磨损行为的主要因素。     

镶嵌用固体润滑剂对锡青铜轴承摩擦学性能影响的研究

用端面摩擦试验机考察了几种镶嵌用固体润滑剂及添加剂在常温条件下对锡青铜轴承摩擦磨损性能的影响,并用X-射线衍射法、俄歇电子能谱法分析了摩擦表面转移膜的化学组成和结合情况。结果表明,几种固体润滑剂的嵌入均可提高轴承的耐磨性,并对减小摩擦系数有一定的作用;摩擦表面固体润滑剂转移膜的形成能够有效地减少摩擦副表面间的粘着现象,是改善轴承摩擦磨损性能的主要原因。     

The 7th International Conference on Fluid Mechanics May 24-27,2015,Qingdao,China

正http://www.icfm7.org First Announcement and Call for PapersThe objective of International Conference on Fluid Mechanics(ICFM)is to provide a forum for researchers to exchange new ideas and recent advances in the fields of theoretical,experimental,computational Fluid Mechanics as well as interdisciplinary subjects.It was successfully convened by the Chinese Society of Theoretical and Applied Mechanics(CSTAM)in Beijing(1987,     

INFORMATION FOR CONTRIBUTORS

Contributions： The Journal, Acta Mechanica Solida Sinica, is pleased to receive papers from engineers and scientists working in various aspects of solid mechanics. All contributions are subject to critical review prior to acceptance and publication.     

Preface

This special issue of PARTICUOLOGY is devoted to the first UK-China Particle Technology Forum taking place in Leeds, UK, on 1-3 April 2007. The forum was initiated by a number of UK and Chinese leading academics and organised by the University of Leeds in collaboration with Chinese Society of Particuology, Particle Technology Subject Group （PTSG） of the Institution of Chemical Engineers （IChemE）, Particle Characterisation Interest Group （PCIG） of the Royal Society of Chemistry （RSC） and International Fine Particle Research Institute （IFPRI）. The forum was supported financially by the Engineering and Physics Sciences Research Council （EPSRC） of United Kingdom,     

基于鲁棒滤波的捷联导引头视线角速度估计方法

针对捷联导引头无法直接获取视线角速度等信息的问题,研究了鲁棒滤波在大气层外飞行器捷联导引头视线角速度估计中的应用。为了建立非线性滤波估计模型,考虑目标视线角速度的慢变特性,采用一阶马尔科夫模型建立了状态方程;推导了视线角速度的解耦模型,并建立了量测方程;考虑到实际应用中存在系统噪声统计特性失准的问题,基于Huber-Based鲁棒滤波方法,设计了视线角速度滤波器,并完成了基于Huber-Based滤波方法和扩展卡尔曼滤波方法的数学仿真。仿真结果表明Huber-Based滤波方法的视线角、视线角速度及视线角加速度估计精度分别达到0.1140'、0.1423'/s、0.0203'/s2,而扩展卡尔曼滤波方法的视线角、视线角速度及视线角加速度估计精度仅分别为0.6577'、0.6415'/s、0.0979'/s~2。仿真结果证明了该方法可以有效地估计出相对视线角速度等信息,并且在非高斯噪声的条件下,依然可获得较高的估计精度,具有一定的鲁棒性。     

Guide for authors

正Each of the sections below provides essential information for authors.We recommend that you take the time to read them before submitting a contribution to Acta Mechanica Sinica.We hope our guide to authors may help you navigate to the appropriate section.How to prepare a submission This document provides an outline of the editorial process involved in publishing a scientific paper in Acta Mechanica     

Use specification of multiscale materials for life spanned over macro-, micro-, nano-, and pico-scale

Multiscale material intends to enhance the strength and life of mechanical systems by matching the transmitted spatiotemporal energy distribution to the constituents at the different scale, say—macro, micro, nano, and pico,—, depending on the needs. Lower scale entities are, particularly, critical to small size systems. Large structures are less sensitive to microscopic effects. Scale shifting laws will be developed for relating test data from nano-, micro-, and macro-specimens. The benefit of reinforcement at the lower scale constituents needs to be justified at the macroscopic scale. Filling the void and space in regions of high energy density is considered.Material inhomogeneity interacts with specimen size. Their combined effect is non-equilibrium. Energy exchange between the environment and specimen becomes increasingly more significant as the specimen size is reduced. Perturbation of the operational conditions can further aggravate the situation. Scale transitional functions and/or f_j/j+1 are introduced to quantify these characteristics. They are represented, respectively, by , and (f_mi/ma,f_na/mi,f_pi/na). The abbreviations pi, na, mi, and ma refer to pico, nano, micro and macro.Local damage is assumed to initiate at a small scale, grows to a larger scale, and terminate at an even larger scale. The mechanism of energy absorption and dissipation will be introduced to develop a consistent book keeping system. Compaction of mass density for constituents of size 10⁻¹², 10⁻⁹, 10⁻⁶, 10⁻³ m, will be considered. Energy dissipation at all scales must be accounted for. Dissipations at the smaller scale must not only be included but they must abide by the same physical and mathematical interpretation, in order to avoid inconsistencies when making connections with those at the larger scale where dissipations are eminent.Three fundamental Problems I, II, and III are stated. They correspond to the commonly used service conditions. Reference is made to a Representative Tip (RT), the location where energy absorption and dissipation takes place. The RT can be a crack tip or a particle. At the larger size scales, RT can refer to a region. Scale shifting of results from the very small to the very large is needed to identify the benefit of using multiscale materials.