Manipulation of speckle fringes for non-destructive testing of defects in composites

A digital speckle pattern interferometer with optical fibres is proposed for composite materials diagnostics in an operative environment. Detection of a variety of flaws, such as disbonds, delaminations and cracks in aircraft components, is reported. Additional fringes are introduced for linearizing the fringe pattern and obtaining quantitative deformation measurements by Fourier transform analysis.     

Application of golay complementary coded excitation schemes for non-destructive testing of sandwich structures

In recent years, InfraRed Thermography (IRT) has become a widely accepted non-destructive testing technique to evaluate the structural integrity of composite sandwich structures due to its full-field, remote, fast and in-service inspection capabilities. This paper presents a novel infrared thermographic approach named as Golay complementary coded thermal wave imaging is presented to detect disbonds in a sandwich structure having face sheets from Glass/Carbon Fibre Reinforced (GFR/CFR) laminates and core of the wooden block.     

The system of double-optical-path ESPI for the vibration measurement

In this paper, a system of double-optical-path electronic speckle pattern interferometry (ESPI) for measuring larger vibration is proposed. This system combines the conventional ESPI optical path for measuring out-of plane vibration and the de-sensitized optical path. It can be used to observe qualitatively and analyze quantitatively the vibration mode. At the same time, the phase unwrapping is avoided. The anti-disturbance capability of this system is high, so it can be used to analyze the vibration characteristics of complex and discontinuous structure in actual engineering.     

Concrete damage diagnosed by using non-classical nonlinear acoustic method

<正>It is known that the strength of concrete is seriously affected by damage and cracking.In this paper,six concrete samples under different damage levels are studied.The experimental results show a linear dependence of the resonance frequency shift on strain amplitude at the fundamental frequency,and approximate quadratic dependence of the amplitudes of the second and third harmonics on strain amplitude at the fundamental frequency as well.In addition,the amplitude of the third harmonics is shown to increase with the increase of damage level,which is even higher than that of the second harmonics in samples with higher damage levels.These are three properties of non-classical nonlinear acoustics.The nonlinear parameters increase from 10~6 to 10~8 with damage level,and are more sensitive to the damage level of the concrete than the linear parameters obtained by using traditional acoustics methods.So,this method based on non-classical nonlinear acoustics may provide a better means of non-destructive testing(NDT) of concrete and other porous materials.     

基于数字散斑相关法的岩石材料力学性能的测试

岩石在外力作用下会发生形变,发现和了解岩石材料的形变、应力分布等对避免灾害会起到重要的预警作用。采用高精度的数字散斑相关技术,对岩石材料形变、应力和应变进行了非接触式测量。为验证实验结果的有效性,电阻应变计贴附于采集区附近并且实验结果与电测结果吻合较好。表明数字散斑相关测量技术能够用于岩石等材料的形变检测,预报变形信息,结果可以定量和定性显示。     

多层结构中脱粘缺陷的超声检测方法

固体火箭发动机多层装药结构中的脱粘类型、位置和尺寸决定了其对整体安全性能构成的威胁程度。该文研究了多层结构中脱粘缺陷的超声检测方法,通过对不同脱粘缺陷超声脉冲回波的特征分析与统计,实现缺陷的定性、定位和定量。首先,采集含有多类脱粘缺陷的粘接结构的超声脉冲回波信号,分析信号中主能量波包所代表的声程,提取五种声程的波峰时刻和幅值作为特征值,组建已知脱粘类型训练样本并输入至BP神经网络,实现特征值域到类别域的非线性映射,即脱粘类型分类;其次,采用阈值法确定缺陷的界面位置;最后,提出分段线性插值-相关性定量法将待检测缺陷的定量结果缩小到±2 mm以内。该文利用COMSOL有限元仿真和实验操作验证了多层粘接结构中脱粘缺陷的定性、定位和定量方法的可行性和可靠性。     

大口径离轴凸非球面系统拼接检验技术

针对大口径离轴凸非球面面形检测的困难,本文将光学系统波像差检验技术与子孔径拼接干涉技术相结合,提出了凸非球面系统拼接检测方法。对该方法的基本原理和具体实现过程进行了分析和研究,并建立了合理的子孔径拼接数学模型。当离轴三反光学系统的主镜和三镜加工完成以后,对整个系统进行装调和测试,并依次测定光学系统各视场的波像差分布,通过综合优化子孔径拼接算法和全口径面形数据插值可以求解得到大口径非球面全口径的面形信息,从而为非球面后续加工和系统的装调提供了依据和保障。结合工程实例,对一口径为287 mm×115 mm的离轴非球面次镜进行了系统拼接测试和加工,经过两个周期的加工和测试,其面形分布的RMS值接近1/30λ(λ=632.8 nm)。     

B型套筒角焊缝缺陷相控阵超声检测定量方法

B型套筒修复作为油气管道修复的主要方式之一,在其修复的焊接过程中,该结构的环形角焊缝内部常常出现以气孔、夹渣为代表的孔型缺陷。这类缺陷由于角焊缝特殊的结构,在利用相控阵超声无损检测技术对其检测时,难以对其进行定量分析。通过数值模拟和实验,发现通过相控阵超声扇扫得到缺陷回波信号峰值与孔型缺陷直径呈正相关,为孔型缺陷的定量分析提供了一种可靠的手段。     

数字散斑相关方法亚像素求解的一种混合方法

亚像素求解是数字散斑相关方法(DSCM)中最重要的技术。亚像素求解算法的精度和效率直接影响DSCM的精度和计算速度。目前广泛应用的两种亚像素求解方法在处理高质量散斑图时都存在一定的缺陷:基于灰度插值的散斑场亚像素恢复方法,其计算精度较高,但计算消耗太大;基于相关系数分布的拟合方法,其计算消耗小,但计算精度较低。在分析两种亚像素求解方法各自优缺点的基础上,提出了一种结合两种算法优势的混合算法。混合算法在保证亚像素求解精度的基础上,可以大大降低整个算法的计算消耗。     

数字图像散斑相关技术的蚁群优化方法

基于蚁群优化方法提出新的数字图像散斑相关算法。该方法模仿了真实蚂蚁从其巢到食物找到最短路径的方式,通过对蚁群优化方法改进,减少迭代次数并改善解的质量。将新的数字图像散斑相关算法应用到计算机模拟的散斑图像和实验获得的散斑图像中,并与广泛使用的Newton-Raphson算法进行了比较。实验结果展示了新算法的精度、可行性和有效性。当数量级为0.01像素,误差离散均方根小于0.002像素。     

Proton-conducting composite membranes from graft copolymer electrolytes and phosphotungstic acid for fuel cells

New organic–inorganic composite membranes based on poly(vinylidene fluoride-co-chlorotrifluoroethylene)-graft-poly(styrene sulfonic acid) [P(VDF-co-CTFE)-g-PSSA] with embedded phosphotungstic acid (PWA) were prepared. Fourier transform infrared spectra indicated the existence of a specific interaction between P(VDF-co-CTFE)-g-PSSA graft copolymer and PWA particles. PWA nanoparticles were well confined in the polymeric matrix up to 20 wt.%, above which they started to be extracted from the matrix, as revealed by scanning electron microscope analysis. Accordingly, Young’s modulus of membranes also increased with PWA concentration up to 20 wt.%, above which it continuously decreased. Upon incorporation of PWA nanoparticles, the proton conductivity of composite membranes slightly decreased from 0.042 to 0.035 S/cm at room temperature up to 20 wt.%, presumably due to strong interaction between the sulfonic acids of graft copolymer and PWA nanoparticles. The characterization by thermal gravimetric analysis demonstrated the enhancement of thermal stabilities of the composite membranes with increasing concentration of PWA.     

基于条纹等值线相关的散斑条纹图处理新方法

在数字散斑干涉术中,通常由物体变形前后得到的两幅原始散斑场用相减方法来得到条纹图,并由相移后的多幅(三幅以上)条纹图来求取相位场。介绍了一种基于条纹等值线相关的条纹图生成新方法,并在此基础上提出了基于单幅干涉条纹图的相位场提取新方法和基于条纹等值线相关的单步相移新方法。实验结果表明,该方法具有良好的结果和发展前景。     

Measurement of speed of sound in poly(lactic acid)-clay composite

We measured longitudinal speed of sound for matrix[poly(lactic acid)]-additive(clay particles) composite rectangular-solid specimen prepared by injection molding. It was found that the speed of sound measured in the direction along the longer side of the specimen was the highest at the middle of the specimen. This trend corresponded with that for crystallinity determined through differential scanning calorimetry (DSC). A cross section view of the specimen parallel to its longer side showed that there was a transverse flow trace of resin in the vicinity of the injection gate while the flow trace along the direction of the longer side spread wider as getting far from the gate toward the middle of the specimen. The high crystallinity appeared in the middle of the specimen was inferred to come from the promotion of crystallization by molecular orientation induced with the above flow trace parallel to the direction along the longer side of the specimen.     

A new method for the characterization of chemical libraries – solely by HPLC retention times

A method has been developed for the assignment of HPLC peaks to their corresponding compounds in libraries of single compounds (parallel syntheses). The basis of the new method is the correlation of the product retention times with the different substituents in the variable positions of the molecule. The correlation is performed automatically by a new algorithm which is part of the computer program LIBFINDER. This practical, easy-to-use tool accelerates the analysis, characterization and purification of chemical libraries, without the need for expensive HPLC-MS equipment.     

大功率发光二极管可靠性和寿命评价试验方法

介绍了发光二极管（LED）的发展简史。提出可能影响LED可靠性的几种因素,主要有封装中的散热问题和LED本身材料缺陷。对于LED可靠性,主要方法是通过测试其寿命来分析其可靠性,一般采取加速实验的方法来测试推导LED寿命。介绍了根据加速应力(主要分为单一加速应力和复合加速应力2种)评价LED寿命的测试方法。在不同加速试验应力条件下测试了大功率LED可靠性,并建立了LED寿命的几种数学模型。最后根据具体实例,通过选择加速应力和试验方法,给出具体推导LED寿命的数学公式。     

核级阀门唇焊焊缝熔深的超声检测方法*

核电阀体唇焊焊缝熔深不足可能导致其在服役期内无预期断裂,由此引起的流质泄露将引起严重的安全事故。因此,极有必要在阀体焊接完成后进行熔深测量以保证足够的焊缝强度。本研究针对阀体唇焊缝粗糙余高曲面声学耦合差、熔深测量难的问题,提出基于喷水式超声聚焦检测技术的唇焊焊缝熔深测量方法。首先,根据核电阀体唇焊焊缝结构特点提出唇焊熔深的超声聚焦测量方法;其次,通过构建检测过程的有限元模型分析焊缝余高曲率对声场聚焦能力的影响,给出余高曲率各异的焊缝检测时的水距修正方法,以便在预定熔深范围内形成高能聚焦声场;最后,分析和提取与唇焊结构相关的检测信号特征,结合金相分析方法修正声速。研究结果显示：通过水距修正可改善焊缝曲率半径变化对聚焦声场的不利影响,曲率半径28.5 mm时焦区声压幅度仅下降11%,基于特征脉冲时间间隔及声速修正可测定焊缝熔深;与金相试验对比,绝对误差小于0.06 mm,满足核电阀门唇焊焊缝熔深测量的需求。     

钚氧化物的分子结构和分子光谱研究

用杂化密度泛函(B3LYP)方法,Pu原子采用相对论有效原子实势(RECP),O原子采用全电子6-311g(d)基组优化了PuO,PuO2,Pu2O3的分子结构,得到了相应的平衡几何构型,并计算了红外振动频率(IR)、Raman光谱.结果表明:PuO,PuO2分子基态几何构型和振动频率与实验值相符.对Pu2O3分子可能的构型和多重性进行结构优化,发现Pu2O3分子基态为11B2的C2v构型,给出了Pu2O3分子基态结构的红外和拉曼光谱数据、力常数等系列数据,并对振动频率的峰值进行了指认.通过自然键轨道(NBO)分析,发现由钚到氧的电荷转移.相对于PuO和PuO2分子,在Pu2O3中形成较弱的Pu—O键.分析自旋布居,发现在这些分子中,自旋磁动量大都由Pu原子的5f电子贡献,而氧原子的2p轨道往往贡献反平行的自旋.     

Two-frame phase-shifting interferometry for retrieval of smooth surface and its displacements

A new two-frame interferometric method with a blind phase shift of a reference wave is proposed for the reconstruction of smooth surface relief areas. In this method, a correlation approach based on the determination of correlation coefficient between intensity distributions of two interferograms is applied for the phase shift extraction. An algorithm for this method realization is developed and its performance is verified on test surfaces. An experimental setup containing a Twiman-Green interferometer was used in the reconstruction of smooth surfaces of metal specimens using the developed algorithm. Surface displacement phase fields were generated in case of a CT-notched specimen made of an aluminum alloy by the interactive procedure of element stitching of two surface reliefs and subtracting the surface relief after cyclic loading from the initial one. The received surface displacement fields allow us to determine the studied specimen fatigue process zone (FPZ) and FPZ size.     

一种基于遗传算法的红外无损检测缺陷的新方法

红外无损检测的本质可归为热传导反问题的求解。利用通过解析法求解热传导正问题得出的结论，提出基于遗传算法优化求解的红外无损检测缺陷信息新方法，该算法采用浮点数编码，并采用多遗传算子并行损作，不仅获得了好的结果，而且维系了种群的多样性。模拟实验验证了算法的鲁棒性和可靠性。     

Active infrared thermographic inspection technique for elevated concrete structures using remote heating system

Conventionally, the inspection of elevated concrete structures requires the use of scaffolding or an aerial truck. In this study, elevated railway structures constructed of reinforced concrete were inspected using active infrared thermography. The inspection area corresponded to half of the middle slab covering an area of 16.8 m²; one inspection was carried out that took about 15 min. A remote heating system consisting of a 6-kW air-cooled xenon arc lamp and a scanner system was developed to detect hidden defects in elevated concrete structures without the need for an aerial truck or scaffolding. The generation of a thermal image and irradiation are carried out simultaneously by the beam scanning. High-contrast infrared thermal images can be obtained by the simple image processing procedure that is proposed.