Experimental study on the transition between stratified and non-stratified horizontal oil-water flow

The effect of oil and water velocities, pipe diameter and oil viscosity on the transition from stratified to non-stratified patterns was studied experimentally in horizontal oil-water flow. The investigations were carried out in a horizontal acrylic test section with 25.4 and 19 mm ID with water and two oil viscosities (6.4 and 12 cP) as test fluids. A high-speed video camera was used to study the flow structures and the transition. At certain oil velocity, stratified flow was found to transform into bubbly and dual continuous flows as superficial water velocity increased for both pipe diameters using the 12 cP oil viscosity. The transition to bubbly flow was found to disappear when the 6.4 cP oil viscosity was used in the 25.4 mm pipe. This was due to the low E?tv?s number. Transition to dual continuous flow occurred at lower water velocity for oil velocity up 0.21 m/s when 6.4 cP oil was used in the 25.4 mm ID pipe, while for U_so > 0.21 m/s, the transition appeared at lower water velocity with the 12 cP oil.The effect of pipe diameter was also found to influence the transition between stratified and non-stratified flows. At certain superficial oil velocity, the water velocity required to form bubbly flow increased as the pipe diameter increased while the water velocity required for drop formation decreased as the pipe diameter increased. The maximum wave amplitude was found to grow exponentially with respect to the mixture velocity. The experimental maximum amplitudes at the transition to non-stratified flow agreed reasonably well with the critical amplitude model. Finally, it was found that none of the available models were able to predict the present experimental data at the transition from stratified to non-stratified flow.     

Carbon dioxide flow boiling in a single microchannel - Part I: Pressure drops

Carbon dioxide two-phase flow pressure drops have been investigated in a single horizontal stainless-steel micro-tube having a 0.529 mm inner diameter. Experiments were carried out in adiabatic conditions for four saturation temperatures of −10; −5; 0; 5 °C and mass fluxes ranging from 200 to 1400 kg/m² s, for inlet qualities up to unity. Measurements have been compared to the predictions of well-known methods. The Müller-Steinhagen and Heck correlation and the Friedel correlation gave the best fit as well as the homogeneous model when the liquid viscosity is used to represent the apparent two-phase viscosity. Further, an analysis based on the homogeneous model has not shown any clear appearance of the laminar or the transition regimes in any given range of Reynolds number. The apparent viscosity of the two-phase mixture was found larger than the liquid viscosity at low vapour qualities, namely at the lowest temperatures. Hence, a new expression to determine the equivalent viscosity was suggested as a function of the reduced pressure. Lastly, the Chisholm parameter from the Lockhart-Martinelli correlation was found lower than expected and also mainly dependent on the saturation temperature.     

Experimental study on oil–water flow in horizontal and slightly inclined pipes

Oil–water two-phase flow experiments were conducted in a 15 m long, 8.28 cm diameter, inclinable steel pipe using mineral oil (density of 830 kg/m³ and viscosity of 7.5 mPa s) and brine (density of 1060 kg/m³ and viscosity of 0.8 mPa s). Steady-state data on flow patterns, two-phase pressure gradient and holdup were obtained over the entire range of flow rates for pipe inclinations of −5°, −2°, −1.5°, 0°, 1°, 2° and 5°. The characterization of flow patterns and identification of their boundaries was achieved via observation of recorded movies and by analysis of the relative deviation from the homogeneous behavior. A stratified wavy flow pattern with no mixing at the interface was identified in downward and upward flow. Two gamma-ray densitometers allowed for accurate measurement of the absolute in situ volumetric fraction (holdup) of each phase for all flow patterns. Extensive results of holdup and two-phase pressure gradient as a function of the superficial velocities, flow pattern and inclinations are reported. The new experimental data are compared with results of a flow pattern dependent prediction model, which uses the area-averaged steady-state two-fluid model for stratified flow and the homogeneous model for dispersed flow. Prediction accuracies for oil/water holdups and pressure gradients are presented as function of pipe inclination for all flow patterns observed. There is scope for improvement for in particular dual-continuous flow patterns.     

Visualization of flow boiling of liquid nitrogen in a vertical mini-tube

The flow boiling patterns of liquid nitrogen in a vertical mini-tube with an inner diameter of 1.931 mm are visualized with a high-speed digital camera. The superficial gas and liquid velocities are in the ranges of 0.01–26.5 m/s and 0.01–1.2 m/s, respectively. Four typical flow patterns, namely, bubbly, slug, churn and annular flow are observed. Some interesting scenes about the entrainment and liquid droplet deposition in the churn and annular flow, and the flow reversal with the indication of negative pressure drop, are also presented. Based on the visualization, the two-phase flow regime maps are obtained. Compared with the flow regime maps for gas–water flow in tubes with similar hydraulic diameters, the region of slug flow in the present study reduces significantly. Correspondingly, the transition boundary from the bubbly flow to slug flow shifts to higher superficial gas velocity, and that of churn to annular flow moves to lower superficial gas velocity. Moreover, time-averaged void fraction is calculated by quantitative image-digitizing technique and compared with various prediction models. Finally, three kinds of oscillations with long-period and large-amplitude are found, possible explanation for the oscillations is given by comparing the instantaneous flow images with the data of pressure, mass flux and temperature recorded synchronously.     

Characteristics of developing vertical bubbly flow under normal and microgravity conditions

The axial development of the void fraction profile, interfacial area concentration and Sauter mean bubble diameter of adiabatic nitrogen-water bubbly flows in a 9 mm-diameter pipe were measured using stereo image processing under normal and microgravity conditions. The flow measurements were performed at four axial locations (axial distance from the inlet, z normalized by the pipe diameter, D, z/D = 5, 20, 40 and 60) and with various flows: superficial gas velocity of 0.00840-0.0298 m/s, and superficial liquid velocity of 0.138-0.914 m/s. The effect of gravity on radial distribution of bubbles and the axial development of two-phase flow parameters is discussed in detail based on the obtained database and visual observation. Following Serizawa-Kataoka’s phase distribution pattern criteria under normal gravity conditions, the phase distribution pattern map was developed. Similar to normal gravity two-phase flows, wall, core and intermediate void peak patterns are observed under microgravity conditions but a transition void distribution pattern is not observed in the current experimental conditions. The data obtained in the current experiment are expected to contribute to the benchmarking of CFD simulation of phase distribution pattern and interfacial area concentration in forced convective pipe flow under microgravity conditions.     

Two-phase flow characteristics in gas–liquid microreactors

Multiphase chemical microreactors require a detailed knowledge of the flow conditions inside the reaction system. This paper reports flow visualization measurements of the two-phase gas–liquid flow pattern and the liquid velocity distribution inside liquid plugs of an intermittent flow. Rectangular cross-section silicon microchannels with hydraulic diameters between 187.5 and 218 μm are fabricated. Laser Induced Fluorescence (LIF) is used to determine the flow pattern. To analyze the influence of the liquid properties and the channel diameter on the two-phase flow pattern, we present flow regime maps using different channel geometries and fluids. A universal flow pattern map based on dimensional analysis is presented. In contrast to microchannel flows, a great number of correlations for flow characteristics for multiphase flow in (round) pipes with diameters >1 mm exist. We compare our experimental results from optical flow visualizations in microreactors with common flow correlations and regime maps for macro- and microchannels. The recirculation motion in the liquid segments of an intermittent gas–liquid flow is analyzed using micron-resolution particle image velocimetry (μPIV). The velocity distribution influences the mixing and the mass transport towards the reactive phase interface dealing with two-phase chemical reactions. For straight microchannels hardly any mass transport over the center line is quantified. For enhanced mixing geometrical adaptations are suggested.     

Viscous oil–water flows in a microchannel initially saturated with oil: Flow patterns and pressure drop characteristics

Immiscible viscous liquid–liquid two-phase flow patterns and pressure drop characteristics in a circular microchannel have been investigated. Water and silicone oil with a dynamic viscosity of 863 mPa s were injected into a fused silica microchannel with an inner diameter of 250 μm. As the microchannel was initially filled with the silicone oil, an oil film was found to always form and remain on the microchannel wall. Different flow patterns were observed and classified over a wide range of water and oil flow rates. A flow pattern map is presented in terms of Re, Ca, and We numbers. Two-phase pressure drop data have also been collected and analyzed to develop a simple correlation for slug, annular and annular-droplet flow patterns in terms of superficial water and oil velocities.     

Two-phase flow laden with spherical particles in a microcapillary

Solid–liquid two-phase flow in a finite Reynolds number range (2 < Re < 12), transporting neutrally-buoyant microspheres with diameters of 6, 10, and 16 μm through a 260-μm microcapillary, is investigated. A standard microparticle-tracking velocimetry (μ-PTV) that consists of a double-pulsed Nd:YAG laser, an epi-fluorescent microscope, and a cooled-CCD camera is used to examine the flow. The solid particles are visualized in view of their spatial distributions. We observe a strong radial migration of the particles across the flow streamlines at substantially small Re. The degree of particle migration is presented in terms of probability density function. Some applications based on this radial migration phenomena are discussed in conjunction with particle separation/concentration in microfluidic devices, where the spatial distribution of particles is of great importance. In doing so, we propose a particle-trajectory function to empirically construct the spatial distribution of solid particles, which is well correlated with our experimental data. It is believed that this function provides a simple method for estimating the spatial distribution of particles undergoing radial migration in solid–liquid two-phase flows.     

In search of physical parameters influenced by flow patterns in a heterogeneous two-phase mixture in microchannels using concomitant measurements

Space transportation systems require high-performance thermal protection and fluid management for systems ranging from cryogenic fluid devices to primary structures, and for propulsion systems exposed to extremely high temperatures, and other space systems, e.g., integrated circuits and cooling/environment control devices for advanced space suits. Although considerable developmental effort is underway to bring promising technologies to a readiness level for practical use, new and innovative methods are still needed. One such method is the Advanced Micro Cooling Module (AMCM), essentially a compact two-phase heat exchanger constructed of microchannels and designed to rapidly remove large quantities of heat from critical systems by incorporating phase transition. This paper describes the results of experimental research in two-phase flow phenomena, encompassing both an experimental and an analytical approach to the incorporation of flow patterns for air–water mixtures flowing in microchannels. Specifically addressed are: (1) design and construction of a sensitive two-phase experimental system which measures both ac and dc components of in situ physical mixture parameters including spatial concentration, using concomitant methods; (2) data acquisition and analysis in the amplitude, time, and frequency domains; and (3) analysis of results including evaluation of in situ physical parameters, and assessment of their validity for application in flow pattern determination.     

Phase split of nitrogen/non-Newtonian fluid two-phase flow at a micro-T-junction

An experimental investigation has been undertaken to understand the phase split of nitrogen gas/non-Newtonian liquid two-phase flow passing through a 0.5 mm T-junction that oriented horizontally. Four different liquids, including water and aqueous solutions of carboxymethyl cellulose (CMC) with different mass concentrations of 0.1, 0.2 and 0.3 wt%, were employed. Rheology experiments showed that different from water, CMC solutions in this study are pseudoplastic non-Newtonian fluid whose viscosity decreases with increasing the shear rate. The inlet flow patterns were observed to be slug flow, slug–annular flow and annular flow. The fraction of liquid taken off at the side arm for nitrogen gas/non-Newtonian liquid systems is found to be higher than that for nitrogen gas/Newtonian liquid systems in all inlet flow patterns. In addition, with increasing the pseudoplasticity of the liquid phase, the side arm liquid taken off increases, but the increasing degree varies with each flow pattern. For annular flow, the increasing degree is much greater than those for slug and slug–annular flows.     

Turbulent cascade modeling of single and bubbly two-phase turbulent flows

The analysis of turbulent two-phase flows requires closure models in order to perform reliable computational multiphase fluid dynamics (CMFD) analyses. A spectral turbulence cascade-transport model, which tracks the evolution of the turbulent kinetic energy from large to small liquid eddies, has been developed for the analysis of the homogeneous decay of isotropic single and bubbly two-phase turbulence. This model has been validated for the decay of homogeneous, isotropic single and two-phase bubbly flow turbulence for data having a 5 mm mean bubble diameter. The Reynolds number of the data based on bubble diameter and relative velocity is approximately 1400.     

Effect of diameter on two-phase pressure drop in narrow tubes

The effect of tube diameter on two-phase frictional pressure drop was investigated in circular tubes with inner diameters of 0.6, 1.2, 1.7, 2.6 and 3.4 mm using air and water. The gas and liquid superficial velocity ranges were 0.01-50 m/s and 0.01-3 m/s, respectively. The gas and liquid flow rates were measured and the two-phase flow pattern images were recorded using high-speed CMOS camera. Unique flow patterns were observed for smaller tube diameters. Pressure drop was measured and compared with various existing models such as homogeneous model and Lockhart-Martinelli model. It appears that the dominant effect of surface tension shrinking the flow stratification in the annular regime is important. It was found that existing models are inadequate in predicting the pressure drop for all the flow regimes visualized. Based on the analysis of present experimental frictional pressure drop data a correlation is proposed for predicting Chisholm parameter “C” in slug annular flow pattern. For all other flow regimes Chisholm’s original correlation appears to be adequate except the bubbly flow regime where homogeneous model works well. The modification results in overall mean deviation of pressure drop within 25% for all tube diameters considered. This approach of flow regime based modification of liquid gas interaction parameter appears to be the key to pressure drop prediction in narrow tubes.     

Flow patterns of n-hexadecane–CO2 liquid–liquid two-phase flow in vertical pipes under high pressure

To promote a better understanding of liquid–liquid two-phase flow behavior, particularly under high pressure, flow patterns of n-hexadecane–CO₂ liquid–liquid two-phase upward flow in vertical stainless steel pipes were experimentally investigated. Observations were made in two 0.0015 m I.D. pipes of different lengths (0.068 m and 0.5 m) under high pressure varying from 10.3 to 29.6 MPa using a high pressure visualization system. The total flow rate was fixed at 2.0 × 10⁻⁶ m³/min, while the flow rate ratio (φ) varied from 0.05 to 19. Bubbly flow, plug flow, slug flow, annular flow, and near-one-phase flow regions were found in both pipes, while stratified flow was observed only in the 0.068 m pipe. Flow pattern maps were constructed in the flow rate ratio versus pressure graph, which demonstrates significant impacts of flow rate ratio, pipe length, and pressure on flow patterns. These impacts are discussed in detail. To the authors’ best knowledge, this work is the first attempt to observe complex liquid–liquid two-phase flow behavior with flow pattern transitions under high pressure, and contributes to a better understanding of liquid–liquid two-phase flow behavior.     

Experimental study on interfacial waves in stratified horizontal oil–water flow

Interfacial wave characteristics were studied experimentally in horizontal oil–water pipe flows during stratified flow and at the transition to dual continuous flow, where drops of one phase appear into the other (onset of entrainment). The experimental investigations were carried out in a stainless steel test section with 38 mm ID with water and oil (density 828 kg/m³and viscosity 5.5 mPas) as test fluids. Wave characteristics were obtained with a high speed video camera and a parallel wires conductivity probe that measured the instantaneous fluctuations of the interface. Experiments were conducted at 2 m and at 6 m from the inlet. Visual observations revealed that no drops are formed when interfacial waves are absent. It was also found that waves have to reach a certain amplitude before drops can detach from their crests. Wave amplitudes are increased as the superficial velocities of both phases increase. In the stratified region, the mean wave amplitude decreases by increasing the oil–water input ratio while mean wavelength increases as the slip velocity between the two-phase decreases. At the onset of entrainment, the mean amplitude and length are found to be a function of the relative velocity between the oil and water layers and of the turbulence in each layer.     

Liquid jet in a high Mach number air stream

The instability of circular liquid jet immersed in a coflowing high velocity air stream is studied assuming that the flow of the viscous gas and liquid is irrotational. The basic velocity profiles are uniform and different. The instabilities are driven by Kelvin–Helmholtz instability due to a velocity difference and neckdown due to capillary instability. Capillary instabilities dominate for large Weber numbers. Kelvin–Helmholtz instability dominates for small Weber numbers. The wavelength for the most unstable wave decreases strongly with the Mach number and attains a very small minimum when the Mach number is somewhat larger than one. The peak growth rates are attained for axisymmetric disturbances (n = 0) when the viscosity of the liquid is not too large. The peak growth rates for the first asymmetric mode (n = 1) and the associated wavelength are very close to the n = 0 mode; the peak growth rate for n = 1 modes exceeds n = 0 when the viscosity of the liquid jet is large. The effects of viscosity on the irrotational instabilities are very strong. The analysis predicts that breakup fragments of liquids in high speed air streams may be exceedingly small, especially in the transonic range of Mach numbers.     

Multiphase drag reduction: Effect of eliminating slugs

Two-phase pressure drop measurements were taken for air/water mixtures in a 0.052-m diameter horizontal pipe with special focus on the superficial liquid velocity range of 0.03–1.2 m/s at superficial gas velocities of 3.8, 5.2, and 6.6 m/s. It was found that the addition of 400 ppm of sodium dodecyl sulfate (SDS) to the water reduced the pressure drop by 25–40% when compared to equal flow rates without SDS. The pressure drop reduction occurred where the SDS eliminated the occurrence of the intermittent flow present with water. It was also found that the same concentration of SDS had virtually no effect on single phase liquid pressure drop. The pressure drop reduction appears to be due solely to the suppression of intermittent flow patterns.     

Macro-to-microchannel transition in two-phase flow: Part 1 - Two-phase flow patterns and film thickness measurements

The classification of macroscale, mesoscale and microscale channels with respect to two-phase processes is still an open question. The main objective of this study focuses on investigating the macro-to-microscale transition during flow boiling in small scale channels of three different sizes with three different refrigerants over a range of saturation conditions to investigate the effects of channel confinement on two-phase flow patterns and liquid film stratification in a single circular horizontal channel (Part 2 covers the flow boiling heat transfer and critical heat flux). This paper presents the experimental two-phase flow pattern transition data together with a top/bottom liquid film thickness comparison for refrigerants R134a, R236fa and R245fa during flow boiling in small channels of 1.03, 2.20 and 3.04 mm diameter. Based on this work, an improved flow pattern map has been proposed by determining the flow patterns transitions existing under different conditions including the transition to macroscale slug/plug flow at a confinement number of Co ≈ 0.3-0.4. From the top/bottom liquid film thickness comparison results, it was observed that the gravity forces are fully suppressed and overcome by the surface tension and shear forces when the confinement number approaches 1, Co ≈ 1. Thus, as a new approximate rule, the lower threshold of macroscale flow is Co = 0.3-0.4 while the upper threshold of symmetric microscale flow is Co ≈ 1 with a transition (or mesoscale) region in-between.     

Experimental investigation of flow boiling characteristics in a cross-linked microchannel heat sink

This paper experimentally investigates flow boiling characteristics in a cross-linked microchannel heat sink at low mass fluxes and high heat fluxes. The heat sink consists of 45 straight microchannels each with a hydraulic diameter of 248 μm and heated length of 16 mm. Three cross-links, of width 500 μm, are introduced in the present microchannel heat sink to achieve better temperature uniformity and to avoid flow mal-distribution. Flow visualization, flow instability, two-phase pressure drop, and two-phase heat transfer measurements are conducted using the dielectric coolant FC-72 over a range of heat flux from 7.2 to 104.2 kW/m², mass flux from 99 to 290 kg/m² s, and exit quality from 0.01 to 0.71. Thermochromic liquid crystals are used in the present study as full-field surface temperature sensors to map the temperature distribution on the heat sink surface. Flow visualization studies indicate that the observed flow regime is primarily slug. Visual observations of flow patterns in the cross-links demonstrate that bubbles nucleate and grow rapidly on the surface of the cross-links and in the tangential direction at the microchannels’ entrance due to the effect of circulations generated in those regions. The two-phase pressure drop strongly increases with the exit quality, at x_e,o < 0.3, and the two-phase frictional pressure drop increases by a factor of 1.6–2 compared to the straight microchannel heat sink. The flow boiling heat transfer coefficient increases with increasing exit quality at a constant mass flux, which is caused by the dominance of the nucleation boiling mechanism in the cross-link region.     

Investigation on heavy crude-water two phase flow and related flow characteristics

In this paper, heavy crude oil–water flows are studied in a horizontal stainless steel test section with 25.4 mm ID and overall length of 50 m. Crude oil (viscosity = 628.1 mPa s, interfacial tension with water = 10.33 mN/m at 60 °C) and water, collected from an oilfield, were used as test fluids. Visual observations, local sampling and pressure drop measurements were used to identify the flow patterns and their transitions. It was found that in all conditions studied there was a water-in-oil emulsion present. At low mixture velocities and water fractions this occupied the whole pipe cross section. As the velocity or the volume fraction increased water appeared to segregate. At high water fractions and mixture velocities annular flow appeared with the water-in-oil emulsion in the core surrounded by a water layer. The results were compared with those from a model oil with the same viscosity. At low water fractions there was a similarity between the patterns observed with the two oil systems characterized by water segregation from an oil continuous dispersion with increasing water fraction or mixture velocity. However, at high water fractions an oil-in-water dispersion formed with the model oil that was not seen with the crude oil. Pressure drop was generally higher for the crude oil system compared to the model one, while in both cases it decreased when water started to segregate and form layers in contact with the pipe wall. The differences between the two oil systems are attributed to the natural surfactants present in the heavy crude oil (such as asphaltenes and resins), which tend to accumulate on the water/oil interface, retard film drainage and maintain the stability of water drops in oil.     

Flow patterns and heat transfer in vertical upward air–water flow with surfactant

Flow patterns, the pressure drag reduction and the heat transfer in a vertical upward air–water flow with the surfactant having negligible environmental impact were studied experimentally in a tube of 2.5 cm in diameter. Visual observations showed that gas bubbles in the air–water solution with surfactant are smaller in size but much larger in number than in pure air–water mixture, at the all flow regimes. The transition lines in the flow regime map for the solution of air–water mixture with surfactant of the 300 ppm concentration are mainly consistent with the experimental data obtained in clear air–water mixture. An additive of surfactant to two-phase flow reduces the total pressure drop and decrease heat transfer, especially in the churn flow regime.