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本文研究了用直流电弧法测定氧化铥中14个稀土杂质的可能性,用正交设计法选择了最佳工作条件,在PGS-2二米平面光栅摄谱仪上摄谱,测定下限分别为:Yb_2O_30.00015%;Eu_2O_3 0.0025%;DY_2O_3、Y_2O_3、Sm_2O_3 0.005%;Tb_4O_7、Ho_2O_3 0.006%;Nd_2O_3、La_2O_3、CeO_2 0.01%;Pr_6O_(11) 0.02%。用logR~logC绘制工作曲线,所得曲线线性良好,回收率为80.5~120.0%,单次测定相对标准偏差为±6.22~17.41%。 相似文献
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煤中微量元素间依存关系的聚类分析 总被引:9,自引:2,他引:9
通过对四种不同类型煤中灰分、硫分和16种微量在不同密度级中呈的R型聚类分析,研究了煤中微量元素间的依存关系。结果表明:煤中碱土 金属Be、Sr、Ba彼此间的依存关系一般较弱,与所研究的其它元素的相关性也较北:稀土元素La、Ce、Y、Se经常相伴而生;V总与灰分显著相关;As、Co、Ni等元素民黄铁矿硫的存在密切相关。 相似文献
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GEOCHEMISTRY OF SEDIMENTS AND ENVIRONMENT IN XIHU LAKE OF GREAT WALL STATION OF CHINA, ANTARCTICA 总被引:3,自引:0,他引:3
The determined results in this paper, which were obtained by the multielement analysis of the 260 cm-deep core sediments under the water of Xihu Lake in the Great Wall Station area, are as follows: The Cenozoic volcanic rocks around Xihu Lake are the main source of sediments in the lake. The chemical differentiation in very fine particles is still detectable. From the variation of ratios of the Cs/Rb, Br/CI and La/Yb in the clay fraction with depth and from the variation or CaCO_3 contained in the sediments, cation replacing amount in the clay grains and the sediment grain sizes in time, it can be seen that since 3600 a. B. P., there has existed the climatic variation of warm-cold-warm, which embodies the advance and retreat history of the ice sheet in this area. 相似文献