钛合金和碳纤维的粘接技术

简述了某空间遥感相机中碳纤维桁架杆与钛合金接头的粘接工艺,通过对粘接剂的选择、粘接表面处理、胶层厚度等粘接强度影响的分析和破坏性力学试验表明,J133胶粘剂适用于钛合金和碳纤维材料的粘接;适当提高粘接表面的粗糙度、用化学法对粘接表面进行处理均可提高粘接强度;对该例的套接形式胶层厚度控制在0.15mm—0.2mm可保证得到好的力学性能和粘接质量。     

低温粘接技术的应用及热应力分析

介绍了低温粘接技术在 SQU ID无磁杜瓦及其它领域中的应用。热应力分析是粘接技术中的一个重要问题 ,文中综述了粘接的热应力分析研究情况     

粘接质量超声检测研究

高波阻抗层下多层低波阻抗层间脱粘的超声检测问题是具有普遍意义又很难解决的检测问题，本文介绍了我们近年来在些方面的一些研究进展，首先从传播特性入手总结出几个有用的特征规律，并结合这些物理特征规律选取相应的信号处理手段，从方法上实现多层界面的脱粘检测，并作了多种技术集成，做出有实际应用价值的检测系统。     

粘接界面特性的超声检测与评价

粘接界面特性的超声检测与评价既是物理学的前沿问题,又是经济建设和国防安全亟需解决的应用问题。高波阻介质下多层低波阻介质界面脱粘检测、滑移界面检测和粘接强度定量评价是粘接质量检测中遇到的三大难题。本文综述了课题组十余年来在攻坚三大难题方面的研究工作：建立了共振匹配理论,发明了六项关键技术并实现了技术集成,研制出全新概念的超声检测设备,解决了第一个难题;成功研制出横波直探头,用纵横波综合判断方法解决了第二个难题;对第三个难题,建立了粘接界面非线性弹簧模型,为利用非线性声学参量评价粘接界面奠定了理论基础,并探索性地利用统计性方法对粘接强度进行了预测,取得较好效果。     

场致发射中金刚石与金属的热粘接技术研究

以分析市场对显示器件的需求为基础,为了寻找适合场致发射的最佳材料,对金刚石粉的晶体结构、颗粒形貌和尺寸进行了分析,得知其微观形貌正好满足场致发射的理论要求.由于制备大面积纳米晶体金刚石薄膜材料的周期很长,且晶体金刚石的电阻率很大并很难掺入杂质,我们选用金刚石纳米粉和能够适合大面积、大批量生产的热粘工艺,从实验上研究并确定了金刚石与金属热粘工艺的可行性,为场致发射器件的研制提供了可靠的实验依据.     

超声在粘接界面的反射和透射

本文讨论了有关超声在两种固体粘接界面上的各种理论模型，介绍了这些模型所假设的界面边界条件以及由此而得到的超声在粘接界面上的反射系数和透射系数。     

超声换能器粘接工艺的球压法研究

在检测用超声换能器的制作工艺中,粘接层是影响换能器性能的一个重要因素.为寻求最佳粘接条件,我们设计了一套加压装置,并采用非均匀加压方法,对陶瓷片几何尺寸(厚度、直径),加压橡胶球参量(直径、硬度)以及施加压力大小三者之间的关系作了一些实验研究,得出了一些有益的实用结果.文中给出了采用非均匀加压方法与一般的均匀加压法制作的换能器性能比较.     

厚胶层复合材料弱粘接结构的超声反射特性

开展了复合材料粘接结构粘接质量的非接触式超声反射特性的仿真与实验研究。首先,建立了水浸环境下纤维增强复合材料(FRP)单层板时域仿真模型,数值分析了不同入射角度下声反射系数频率谱的变化规律,并与已有理论方法进行了对比验证。基于此,建立了含厚胶层的复合材料粘接结构反射特性时域仿真模型,分析了粘接界面弱化程度对超声反射系数频谱特征点的影响规律。基于水浸超声反射特性测量系统,实验萃取了完好粘接状态的FRP粘接结构的超声反射系数频谱,与仿真结果吻合良好。随后,制备了具有不同粘接界面状态特征的FRP粘接结构试样,从实验角度揭示了单/双粘接界面弱化状态与超声反射特性间规律性的偏移特征。基于不同粘接状态与超声反射特性间的规律性分布特征,可为厚胶层复合材料粘接结构的粘接质量评估提供新的研究思路。     

相位校正器粘接局部应力控制技术

通过理论分析,对相位校正器的镜面与支撑结构间的粘接建立模型进行仿真研究,提出了在相位校正器镜片上加工小圆柱,使其粘接应力由镜片本身转移到突出部位的小柱子上,有效改善了相位校正器镜面局部粘接应力,使镜面局部高阶像差得到缓解,并通过试验验证了其有效性。     

相位校正器粘接局部应力控制技术

通过理论分析,对相位校正器的镜面与支撑结构间的粘接建立模型进行仿真研究,提出了在相位校正器镜片上加工小圆柱,使其粘接应力由镜片本身转移到突出部位的小柱子上,有效改善了相位校正器镜面局部粘接应力,使镜面局部高阶像差得到缓解,并通过试验验证了其有效性。     

Ti扩散铌酸锂光波导特性的热固定技术

在Ti扩散铌酸锂光波导中,因光致折变效应而导致光波导特性漂移.在光波相干性的导波光学器件中,光致折变效应的影响尤为严重.本文报道了稳定光致折变效应的热固定技术实验结果;并提出在光波导特性的热固定过程中,不是H~+离子起主导作用这一看法.     

表面黏附导致的接触行为转变

应用大规模分子动力学方法, 模拟了具有不同原子级粗糙形貌的两种刚性球形探头与弹性平面基体的黏附接触行为. 研究了载荷与真实接触面积、接触界面排斥力与真实接触面积, 以及黏附力与真实接触面积之间的关系. 分子模拟得到的载荷与真实接触面积的关系, 与连续力学接触理论预测很好地定性一致. 无论是原子级光滑探头还是粗糙探头, 黏附接触下的排斥力与真实接触面积的关系, 都与无黏附接触时的规律相一致, 即黏附力对接触行为的影响作用, 可以等效为附加在真实外载荷基础上的虚拟载荷, 将对黏附接触行为的分析转变为无黏附接触分析. 两种探头的黏附力随真实接触面积都呈幂函数形式的增长, 但是, 原子级光滑探头的幂指数大于1, 而原子级粗糙探头的幂指数小于1. 关键词： 接触行为 表面黏附 分子动力学模拟     

碳化硅指向反射镜轴的高精度镶接技术研究

碳化硅具有优异的热学性能和机械性能,是高性能空间光学应用中的优选材料。但由于它的硬度很高,使得碳化硅反射镜的高精度加工和装配变得很困难。为了提高碳化硅反射镜与两个镜轴固接后的位置精度,采用了结合衬套修正的偏心轴补偿镶接方案。结果表明,这种方法可以将镶接完成后的两个镜轴的同轴度误差降低到0.005mm。由于在镶接过程中仅需要通用的加工设备和工装夹具,因此可以在保证良好经济性的前提下提高碳化硅反射镜的装配精度。     

Gauge fixing procedure in the extended BRST theory. The example of the abelian 2‐forms

The paper proposes a general procedure to find the form of the gauge fixing term in the extended BRST quantization of the gauge theories, a difficult problem in the standard approach. Our proposal is based on the many level structure of the extended spaces and leads to a simple form of the gauge fixing term. The abelian 2‐form model is completely analyzed as an example.     

Φ256mm大口径锗透镜加工技术

随着红外技术的发展，在其光学系统中，锗材料的应用日趋地多。大口径锗材料在应力、均匀性和作为光学零件要求的精度上，对加工者都有一定难度。本文介绍了目前国内口径最大（Φ２５６ｍｍ）的多晶透镜的加工方法。从零件的特点及技术要求到加工工艺、磨具选择、抛光机理等均有叙述及分析。最后，提出进一步改进加工工艺的设想。     

SH ultrasonic guided waves for the evaluation of interfacial adhesion

Shear-Horizontally (SH) polarized, ultrasonic, guided wave modes are considered in order to infer changes in the adhesive properties at several interfaces located within an adhesive bond joining two metallic plates. Specific aluminium lap-joint samples were produced, with different adhesive properties at up to four interfaces when a glass–epoxy film is inserted into the adhesive bond. EMAT transducers were used to generate and detect the fundamental SH₀ mode. This is launched from one plate and detected at the other plate, past the lap joint. Signals are picked up for different propagation paths along each sample, in order to check measurement reproducibility as well as the uniformity of the adhesively bonded zones. Signals measured for four samples are then compared, showing very good sensitivity of the SH₀ mode to changes in the interfacial adhesive properties. In addition, a Finite Element-based model is used to simulate the experimental measurements. The model includes adhesive viscoelasticity, as well as spatial distributions of shear springs (with shear stiffness K_T) at both metal–adhesive interfaces, and also at the adhesive–film interfaces when these are present. This model is solved in the frequency domain, but temporal excitation and inverse FFT procedure are implemented in order to simulate the measured time traces. Values of the interfacial adhesive parameters, K_T, are determined by an optimization process so that best fit is obtained between both sets of measured and numerically predicted waveforms. Such agreement was also possible by adjusting the shear modulus of the adhesive component. This work suggests a promising use of SH-like guided modes for quantifying shear properties at adhesive interfaces, and shows that such waves can be used for inferring adhesive and cohesive properties of bonds separately. Finally, the paper considers improvements that could be made to the process, and its potential for testing the interfacial adhesion of adhesively bonded composite components.     

Enhancement of adhesion between polyphenylene sulfide and copper by surface treatments

In this paper, we introduce methods which can effectively enhance the adhesion between polyphenylene sulfide (PPS) and bulk Cu. One of the methods involved the thermal evaporation of PPS to form a buffer layer on Cu and the other involved plasma treatment with reactive gases such as O₂, H₂, and N₂ on the PPS buffer layer. The adhesion strength of samples prepared by PPS thin film coating (∼26 MPa) was largely enhanced when compared to that of samples obtained by only etching (∼15 MPa). Among the samples obtained by plasma treatment using various reactive gases, the samples treated using H₂ plasma showed the best adhesion strength (of ∼32 MPa) in comparison to the other samples owing to the adhesion between hydrophobic surfaces.     

Quantifying cell adhesion through forces generated by acoustic streaming

The strength of cell adhesion is important in understanding the cell’s health and in culturing them. Quantitative measurement of cell adhesion strength is a significant challenge in bioengineering research. For this, the present study describes a system that can measure cell adhesion strength using acoustic streaming induced by Lamb waves. Cells are cultured on an ultrasound transducer using a range of preculture and incubation times with phosphate-buffered saline (PBS) just before the measurement. Acoustic streaming is then induced using several Lamb wave intensities, exposing the cells to shear flows and eventually detaching them. By relying upon a median detachment rate of 50 %, the corresponding detachment force, or force of cell adhesion, was determined to be on the order of several nN, consistent with previous reports. The stronger the induced shear flow, the more cells were detached. Further, we employed a preculture time of 8 to 24 h and a PBS incubation time of 0 to 60 min, producing cell adhesion forces that varied from 1.2 to 13 nN. Hence, the developed system can quantify cell adhesion strength over a wide range, possibly offering a fundamental tool for cell-based bioengineering.     

Surface adhesion properties of graphene and graphene oxide studied by colloid-probe atomic force microscopy

Surface adhesion properties are important to various applications of graphene-based materials. Atomic force microscopy is powerful to study the adhesion properties of samples by measuring the forces on the colloidal sphere tip as it approaches and retracts from the surface. In this paper we have measured the adhesion force between the colloid probe and the surface of graphene (graphene oxide) nanosheet. The results revealed that the adhesion force on graphene and graphene oxide surface were 66.3 and 170.6 nN, respectively. It was found the adhesion force was mainly determined by the water meniscus, which was related to the surface contact angle of samples.     

用脉冲紫外激光预处理提高刀具的金刚石涂层的附着强度

采用脉冲紫外激光（XeCl,308nm）表面消融预处理方法以硬质合金为衬底制备了金刚石涂层刀具。利用压痕法对涂层结合强度进行了测试,得到了最佳预处理工艺条件。采用碳化硅增强铝合金材料对制备的金刚石涂层刀具进行了实际切削性能实验。实验结果表明：脉冲紫外激光表面消融预处理方法的采用对刀具的金刚石薄膜涂层附着强度的提高有很大的帮助。