首页 | 本学科首页   官方微博 | 高级检索  
相似文献
 共查询到20条相似文献,搜索用时 76 毫秒
1.
本文从理论和技术上就原子吸收分光光度计用于可见一紫外分光光度分析的可行性加以研究和探讨。并用于实际样品的测定,获得较满意的结果。  相似文献   

2.
本文从理论和技术上就原子吸收分光光度计用于可见-紫外分光光度分析的可行性加以研究和探讨。并用于实际样品的测定,获得较满意的结果。  相似文献   

3.
本文利用紫外分光光度法研究了高碘酸钠氧化甘油的动力学,测定了其动力学方程,探讨了反应机理,同时建立了甘油氧化动力学的紫外分光光度法,该法简单、重现性好、准确度高。  相似文献   

4.
原子吸收分光光度计新应用的探讨   总被引:15,自引:1,他引:14  
本文采用原子吸收分光光度计兼作紫外可见分光光度计使用,开展了应用研究。对其实验技术和分析性能进行了详细的探讨,并用于天然水中微量铁及食用色素的含量测定,结果令人满意。扩大了仪器的分析功能和应用范围。  相似文献   

5.
钟鸣  张月  马慧  陈丽静  赵倩 《光谱实验室》2011,28(2):866-869
通过DAN荧光法,3,3-二氨基联苯胺分光光度法和邻苯二胺紫外分光光度法测定蛹虫草菌丝体中硒的含量,对测得结果进行统计分析,并对其检出限、回收率进行比较研究.研究结果表明,DAN荧光法、3,3-二氨基联苯胺分光光度法和邻苯二胺紫外分光光度法中,硒含量相对标准偏差分别是2.5%,9.2%和6.1%;线性回归系数都大于0....  相似文献   

6.
胃癌患者血清紫外吸收光谱的初步研究   总被引:1,自引:0,他引:1  
胃癌是国内外高发的恶性肿瘤之一,本文以紫外分光光度计对正常人血清与胃癌病人血清进行检测,并把光谱数据进行统计和分析,比较两者之间的差异,从而为紫外分光光度计应用于胃癌的诊断提供了重要的实验依据。  相似文献   

7.
紫外分光光度法测定水中酚   总被引:5,自引:1,他引:4  
张丽莹 《光谱实验室》2006,23(4):890-892
根据酚类在紫外区有吸收光谱的原理,以紫外分光光度法直接测定水中酚.通过实验结果表明,此方法简便快捷并有较高准确度、精密度.  相似文献   

8.
通过对紫外-可见光分光光度计的光源偏振性进行系统测量,并开展了光源偏振性对水体黄色物质和颗粒物光谱吸收系数测量影响的实验研究,结果表明,紫外-可见光分光光度计光源具有显著的偏振性,但分光光度计光源偏振对水体黄色物质光谱吸收系数测量的影响可忽略不计,对水体颗粒物光谱吸收系数测量的影响也较小。  相似文献   

9.
马齿苋总黄酮含量的测定   总被引:26,自引:1,他引:25  
魏循  王仲英 《光谱实验室》2003,20(1):128-129
本文对中草药马齿苋中总黄酮含量进行了提取、分离,用紫外分光光度计进行了测定。  相似文献   

10.
刘氘  陈虹  张启云 《光谱实验室》2009,26(2):300-302
沸水溶解岩盐样品,过滤除去水不溶物,紫外分光光度法分别测定滤液在220nm和275nm处的吸光度值,计算出样品中NO3-含量。结果表明,3种不同类型岩盐样品中NO-3的回收率为98.0%—102.0%,相对标准偏差为1.03%—2.92%(RSD,n=5)。与百里酚分光广度法和离子色谱法相比,紫外分光光度法简单快速,准确度、灵敏度、精密度高,适用于岩盐样品中硝酸盐含量的快速检测。  相似文献   

11.
Two-dimensional scanning of a 0.6328 mum guided-light beam has been realized using noncolinear acousto-optic (AO) coplanar Bragg diffraction together with colinear AO guided-mode to substrate radiation-mode conversion in a Z-cut Xpropagation LiNbO3 proton-exchanged (PE) waveguide. The two surface acoustic (SAW) waves utilized are at the center frequencies of 500 and 200 MHz, propagating in the Y and X axes, respectively. Two-dimensional scanning of approximately 720 resolvable light beam spots, namely, 18 40 (horizontal vertical) scanning, has been demonstrated using a light beam of 1.0 mm aperture. The total number of resolvable beam spots can be greatly increased from 720 by simply utilizing SAW transducers of larger bandwidth and a light beam of greater aperture. It should also be possible to significantly increase the diffraction efficiency from 3 % by optimizing the parameters of the PE waveguide and the SAWs.  相似文献   

12.
A review of schemes for multiple access in fiber optic networks shows that a hybrid of wavelength and code division multiple access (WCDMA) combines the best features of both. In particular, the hybrid scheme retains the large information carrying capacity of wavelength division multiple access (WDMA) and flexibility of code division multiple access (CDMA). In this paper WDMA, optical CDMA (OCDMA), and WCDMA networks are discussed. In OCDMA networks, concept of incoherent and coherent coding including inverse decoding and matched filter is introduced. The delay performance of both WDMA and WCDMA networks, under the simple suboptimum access protocols based on cyclic search, is computed. It has been shown quantitatively that tuning delay significantly affects the delay performance of both WDMA and WCDMA networks. Futhermore, delay performance of WCDMA networks is always better than the WDMA networks for the same tuning delay, load, and number of users.  相似文献   

13.
Results of a study of the effect of γ-radiation on the spectral luminescence properties of cadmium tungstate crystals doped with silver, bismuth, and molybdenum cations are presented. Spectral characteristics of the nondnnnoped crystals are briefly described. Absorption and photo and X-ray luminescence spectra of the crystals taken before and after exposure to γ-radiation (5.5·104 Gy) are compared. It is found that the spectral characteristics of the crystals doped with silver, bismuth, and molybdenum cations do not change markedly after the exposure. The relation between the type of impurity-induced defects, individual characteristics of the impurity cations, and the character of the effect of γ-radiation on the spectral luminescence properties of impure crystals is analyzed (preliminarily). Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 64, No. 1, pp. 55–60, January–February, 1997.  相似文献   

14.
A simple technique of pulse compression, based on the linear chirp compensation of self-phase modulation (SPM) spectra in dispersion shifted fibers, is demonstrated. The optimization procedure is carried out, for a short span of a single-mode fiber, using a parabolic law, which describes the behavior of the squared output pulse width versus the pump peak power in the case of Gaussian pulses. The experimental results give a minimum pulse duration of 233 fs, which is in good agreement with the model. Shorter and coherent pulses, down to 90 fs, have been obtained by inserting an interference filter at the optical output.  相似文献   

15.
The Shanghai Synchrotron Radiation Facility(SSRF)booster ring,a full energy injector for the storage ring,is deigned to accelerate the electron beam energy from 150MeV to 3.5GeV that demands high extraction efficiency at the extraction energy with low beam loss rate when electrons are ramping.Closed orbit distortion(COD)caused by bending magnet field uniformity errors which affects the machine performance harmfully could be effectively reduced by bending magnet location sorting.Considering the affections of random errors in measurement,both ideal sorting and realistic sorting are studied based on measured bending magnet field uniformity errors and one reasonable combination of bending magnets which can reduce the horizontal COD by a factor of 5is given as the final installation sequence of the booster bending magnets in this paper.  相似文献   

16.
17.
We measure the waveform and phase curves of short optical pulses before and after transmission over different lengths of fibers by use of the pulse analyzer with the frequency-resolved optical gating (FROG),and numerically simulate pulse evolution under the experimental conditions.The nonlinear coefficient of the fiber is given by comparing the experimental results with the numerical ones.Difference between the experiment and numerical simulation is analyzed.  相似文献   

18.
Resonance scattering of elastic spherical shell and cylindrical shell while the surrounding fluid medium has absorption is studied. The normal mode solution derived using exact elastic theory and the separation of variables is still applicable. However, the scattering form function has to be modified for the absorbing medium, otherwise the unreasonable result would be obtained. The backscattering form function in the absorbing medium is redefined, and the form function of elastic spherical and cylindrical shell with vacuum or solid matter filled is calculated in various absorption conditions. The results show that the absorption of surrounding fluid leads to notable attenuation of the coincidence resonances in the mid-frequency, but it has a little influence on the low-frequency resonance scattering induced by the filler inside the shell.  相似文献   

19.
A versatile and low-cost single-beam self-referenced phase-sensitive surface plasmon resonance(SPR)sensing system with ultra-high resolution performance is presented.The system exhibits a root-mean-square phase fluctuation of ±0.0028.over a period of 45 min.i.e.a resolution of±5.2×10-9 refractive index units.The enhanced performance has been achieved through the incorporation of three design elements:a true single-beam configuration enabling complete self-referencing so that only the phase change associated with SPR gets detected,a differential measurement scheme to eliminate spurious signals not related to the sensor response,and the elimination of retardation drifts by incorporating temperature stabilization in the liquid crystal phase modulato .Our design should bring the detection sensitivity of non-labeling SPR biosensing closer to that achievable by conventional fluorescence-based techniques.  相似文献   

20.
Ta2O5 films are prepared on BK7 substrates with conventional electron beam evaporation deposition.The effects of SiO2 protective layers and annealing on the laser-induced damage threshold (LIDT) of the films are investigated.The results show that SiO2 protective layers exert little influence on the electric field intensity(EFI)distribution,microstructure and microdefect density but increase the absorption slightly.Annealing iS effective on decreasing the microdefect density and the absorption of the films.Both SiO2 protective layers and annealing are beneficial to the damage resistance of the films and the latter is more effective to improve the LIDT.Moreover,the maximal LIDT of Ta2O5 films is achieved by the combination of SiO2 protective layers and annealing.  相似文献   

设为首页 | 免责声明 | 关于勤云 | 加入收藏

Copyright©北京勤云科技发展有限公司  京ICP备09084417号