超声雾化法制取金属粉末方法研究

本文介绍了利用超声振动能量制取超细金属粉末的超声雾化方法，提出了超声制粉雾化室，等离子枪，阴极、阳极喷咀及换能器振动系统的最佳尺寸和工作参数，给出了实验结果及制得的粉末显微结构照片．实验结果表明，用本文所述方法制得的金属粉末组成为：－80目粉占84呢，－120目粉占63．7啪，而用PREP方法制得的粉末分别占19．5％和11．7％，由此看来，用本方法制取超细金属粉，在粒度组成方面优于PREP方法．文中还对粉末冷却速度做了估算，得到了粉末平均冷却速度大于1×10_5k/5     

Ultrasonic phased array controller for hyperthermia applications

Multiple and mechanically scanned ultrasound transducer systems have demonstrated the efficacy of using ultrasound to produce deep localized hyperthermia. The use of ultrasonic phased arrays has been proposed as an alternative to these systems. A phased array offers a more flexible approach to heating tumours in that the size, shape, and position of its focal region can be altered during the course of treatment in order to achieve the desired temperature distribution. This added flexibility comes at the cost of increased complexity of the hardware necessary to drive the transducer because each element requires its own amplifer with both phase and amplitude control. In order for phased arrays with large numbers of elements to be feasible for hyperthermia applications, the complexity of this circuitry must be minimized. This paper describes a circuit design which simplifies the electronics required to control a phased array transducer system for hyperthermia applications. The design is capable of controlling virtually any type of phased array transducer operating at frequencies less than 2 MHz. The system performance was verified through beam profile measurements using a 48-element tapered phased array transducer.     

Performance and simulation of an on-board guided-wave optical processor for airborne SAR applications

This paper describes the performance and simulation of a compact integrated optical processor for the real-time reconstruction of two-dimensional images in airborne stripmap synthetic aperture radar applications. The functional behavior of the processor is explained in some detail. The design criteria are briefly given. The simulation step allowed the main processor characteristics and properties to be identified. A number of comparisons were obtained in airborne SAR mission scenarios between the predictions of the optical device and those achieved by the modern electronic digital approach, based on the wavefront reconstruction method by matched filtering.     

基于PLC的超声波喷涂系统设计

介绍了一种基于PLC的超声波喷涂系统的设计方案。系统主要分为喷涂模块和加热模块,以PLC为控制中心,对喷涂过程和加热过程进行精确的控制。采用上位机软件,对加热和喷涂过程进行实时的监控,方便操作。本系统适用于物体表面的超声波喷涂处理和加热处理。     

Ultrasonic wave fluctuations through tissue: an experimental pilot study

The fundamental role of the assumption of plane wave ultrasonic propagation in attenuation and scattering measurements on soft tissues is discussed. The evidence for and against the validity of the assumption is shown to be inconclusive. An experimental procedure for direct assessment, by measurement of the ultrasonic amplitude and phase fluctuations occurring after an interrogating plane wave has passed through a tissue specimen, is described. The phase measurements impose significant demands on the mechanical precision, temperature stability and electronic timing capabilities of the measurement system. Measurements are reported on two specimens of fresh beef liver. One exhibited significant fluctuations of amplitude and phase which were reduced by 50% when the effects of thickness variations in the specimen were removed. The other specimen exhibited relatively small fluctuations. The feasibility of making such measurements has been demonstrated and the detailed features of the experimental procedure-which requires considerable care-have been outlined. Although more measurements are needed for definitive conclusions, these will require the development of a reliable technique for determining the presence of gaseous microbubbles in tissue in vitro. The preliminary conclusion that some samples of liver may exhibit low levels of wavefront disruption is consistent with recent evidence in the literature.     

Several applications of laser diagnostics for visualization of combustion phenomena

Several applications of laser diagnostic techniques to visualize combustion phenomena are presented, including reactive Mie scattering for flow, Rayleigh and Raman spectroscopy for major species, laser-induced fluorescence for minor species, and laser extinction, scattering, and laser-induced incandescence for soot. These techniques have been applied to diffusion flame oscillation, a recirculation zone in a burner, laminar and turbulent lifted flames, flame propagation along a vortex tube, and soot zone characteristics, to demonstrate the usefulness of the techniques to provide a better understanding of physical mechanisms.     

超声喷雾共沉淀法制备Eu3+掺杂纳米ZnO粉体

采用超声喷雾共沉淀法技术,以Zn(NO3)23·6H2O和(NH4)CO3,为前驱体制备了ZnO纳米粉体以及ZnO:Eu粉体.研究了超声喷雾条件、反应时间以及化学组分对ZnO纳米粉体的形貌和尺寸的影响,着重研究了氢氧化锌脱水生成ZnO纳米粉体的化学处理条件.在ZnO中掺入Eu3+离子,研究了不同Eu3+掺杂量对纳米Zn...     

在线超声波流量监测系统设计及其应用

为解决地源热泵系统中的进出水流量测量,设计研究基于超声波时差法原理的非接触式在线流量监测装置。系统以STM32F407 ZE为主控制器,定时采集流量、完成数据封包、加密和远端服务器交互任务;以MSP430F2618为流量测量控制器,采用时差法以TDC-GP22精准测量超声波在介质中传播时间,实现管道流体流速、流量实时监测。系统测试结果实现流量数据测量及上传存储到远端服务器,满足地源热泵系统流量监测需求。     

Ultrasonic monitoring of film condensation for applications in reduced gravity

The film condensation of vapor on a cooled, downward-facing surface is a complex dynamic fluid phenomenon. This paper will describe the theoretical basis, instrumentation approach, and experimental results for a method for ultrasonic monitoring of film condensation. The ultrasound measurement system utilizes a 10 MHz broadband contact transducer, operating in pulse-echo mode. By appropriate signal processing, condensation layers over a wide thickness range, from much less than a wavelength to several wavelengths, can readily be measured.     

一种高性能太阳敏感器复合光学系统设计

以夫朗禾费衍射理论为基础,结合微透镜,设计了一种高性能的数字式太阳敏感器复合光学系统。分析了光学系统的组成,建立了光学系统的数学模型,设计了光学系统的焦距、孔径和微透镜参量,并进行了成像的数值仿真。仿真结果表明,与基于掩模的光学系统相比,这种新型的复合光学系统成像光斑能量分布集中,保证计算光斑中心位置的高精度,使敏感器具有大视场和高精度的特点。     

Design and applications of an in situ electrochemical NMR cell

A device using a three-electrode electrochemical cell (referred to as an ECNMR cell) was successfully constructed that could be used in a standard 5mm NMR probe to acquire high-resolution NMR spectra while the working electrode was held at a constant electrical potential. The working electrode was a 20 nm thick gold film thermally coated on the outside of an inner 3mm glass tube. An underlayer consisting of (3-mercaptopropyl)trimethoxy-silane was coated on the glass surface in order to improve its adhesion to gold. Tests showed prolonged life of the gold film. Details of the design and construction of the ECNMR cell are described. The ECNMR cell could be routinely used in a multi-user service high-resolution NMR instrument under oxygen-free conditions in both aqueous and non-aqueous solvents. Different approaches were applied to suppress the noise transmitted between the potentiostat and the NMR spectrometer. These approaches were shown to be effective in reducing background noise in the NMR spectra. The electrochemical and NMR performance of the ECNMR cell is presented. The reduction of 1,4-benzoquinone in both aqueous and non-aqueous solvents was used for testing. The evolution of the in situ ECNMR spectra with time demonstrated that use of the ECNMR cell was feasible. Studies of caffeic acid and 9-chloroanthracene using this ECNMR cell were undertaken to explore its applications, such as monitoring reactions and studying their reaction mechanisms.     

基于LabVIEW的时间反转超声检测系统的开发

时间反转技术在超声无损检测中的应用非常广泛,它可以忽略介质的非均匀性及初始信号源的位置,能够在时间和空间上聚焦超声波,实现对介质缺陷的聚焦检测。基于LabVIEW图形化编程软件,结合计算机、信号发生器、示波器、超声换能器、GPIB等的使用,对超声检测系统实验平台进行了构建,实现了超声信号的发射、接收以及时间反转一系列的信号处理过程。系统工作过程中,采用了三种不同的时间反转技术：经典时间反转技术(Time Reversal：TR)、反向滤波技术(Inverse Filter：IF)及1位处理技术(1Bit Processing),来实现信号的聚焦。实验验证该系统可以有效的实现时间反转超声检测过程中对信号的激励、接收、处理和存储等功能,有良好的精确性和适用性。     

超声红外热像技术及其在无损评价中的应用

本介绍在光热红外检测的基础上发展的超声红外热像技术。该技术利用超声脉冲作为激发源，当超声脉冲在试样上传播的过程中遇到裂纹等缺陷时，缺陷引起超声附加衰减而局部升温。利用红外照相机获取试样表面的温度分布，可显示裂纹等缺陷。超声红外热像技术发挥了超声和红外技术的优点，可实时地检测裂纹等缺陷，在无损评价和检测中有广泛应用。     

Ultrasonic compatibilization of polyelectrolyte complex based on polysaccharides for biomedical applications

In recent years, there has been an increasing interest in the design of biomaterials for cartilage tissue engineering. This type of materials must meet several requirements. In this study, we apply ultrasound to prepare a compatibilized blend of polyelectrolyte complexes (PEC) based on carboxymethyl cellulose (CMC) and chitosan (CHI), in order to improve stability and mechanical properties through the inter-polymer macroradicals coupling produced by sonochemical reaction. We study the kinetic of the sonochemical degradation of each component in order to optimize the experimental conditions for PEC compatibilization. Scaffolds obtained applying this methodology and scaffolds without ultrasound processing were prepared and their morphology (by scanning electron microscopy), polyelectrolyte interactions (by FTIR), stability and mechanical properties were analyzed. The swelling kinetics was studied and interpreted based on the structural differences between the two kinds of scaffolds. In addition we evaluate the possible in vitro cytotoxicity of the scaffolds using macrophage cells in culture. Our results demonstrate that the ultrasound is a very efficient methodology to compatibilize PEC, exhibiting improved properties compared with the simple mixture of the two polysaccharides. The test with murine macrophage RAW 264.7 cells showed no evince of cytotoxicity, suggesting that PEC biomaterials obtained under ultrasound conditions could be useful in the cartilage tissue engineering field.     

导航卫星上行注入与测距性能测试系统设计

导航卫星的上行注入与测距性能是卫星导航系统服务精度一个重要保证,设计了一种导航卫星的上行注入与测距性能测试系统;该系统以控制处理计算机为核心,并结合了专用设计的基准频率发生器模块、基准时间发生器模块、注入信号发生器模块和通用商业化仪器,能实时动态地模拟导航卫星在轨期间接收地面注入信号的情形,完成导航卫星上行注入性能测试中电文信息的生成和比对以及上行测距性能测试;该测试系统稳定、灵活,测量精度高,而且可以通过修改测试软件参数来满足新的测试要求,便于测试系统的升级改造。     

基于时差法的超声波测速向仪设计与实现

介绍了超声波时差法风速测量的基本原理,以及基于MSP430微控制器和MAG3110的风速风向测量系统的实现方法。给出了以MSP430芯片为核心的硬件设计的总体框架图。详细地阐述了各个外围接口电路的设计,以及超声波风速风向测量的软件设计。系统具有结构简单、精度高、功耗低和扩展方便等特点,能够满足大学物理实验教学的风况信息测量。     

Nanocrystalline ruthenium oxide and ruthenium in sensing applications – an experimental and theoretical study

In this project, we have explored RuO₂ and Ru nanoparticles (∼ ∼10 and ∼ ∼5 nm, respectively, estimated from XRD data) to be used as gate material in field effect sensor devices. The particles were synthesized by wet chemical procedure. The capacitance versus voltage characteristics of the studied capacitance shifts to a lower voltage while exposed to reducing gases. The main objectives are to improve the selectivity of the FET sensors by tailoring the dimension and surface chemistry of the nanoparticles and to improve the high temperature stability. The sensors were characterized using capacitance versus voltage measurements, at different frequencies, 500 Hz to 1 MHz, and temperatures at 100–400°C. The sensor response patterns have been found to depend on operating temperature. X-ray photoelectron spectroscopy (XPS) analyses were performed to investigate the oxidation state due to gas exposure. Quantum-chemical computations suggest that heterolytic dissociative adsorption is favored and preliminary computations regarding water formation from adsorbed hydrogen and oxygen was also performed.     

超声喷雾共沉淀法制备的Lu3Al5O12∶Eu3+纳米粉体发光特性

采用新型超声喷雾共沉淀法技术,以Lu2O3、Eu2O3、Al(NO3)3·9H2O为原料,制备了不同浓度Eu3+离子掺杂的Lu3Al5O12纳米粉体.用X射线粉末衍射表征了获得纳米粉体的相,用扫描电镜观察了纳米粒子的形貌.测定了粉体的激发光谱、7F0-5D2声子边带谱与发射光谱.研究了不同高温烧结温度与Eu3+掺杂浓度...     

车用声学材料测量研究性教学实验设计

针对工科高等院校物理实验课设计了车用声学材料测量研究性教学实验.实验结合开设专业和选题自身特点,在传统研究性教学实验设计的基础上,将学生实验前的调研工作从时间、空间上拓展至课堂之外,并将科研工作中自行设计的车用声学材料数据库系统应用于教学,以期实现教学引导科研、科研促进教学,学研结合、教学相长.     

Catalyzed combustion of hydrogen–oxygen in platinum tubes for micro-propulsion applications

The present investigation addresses the need to understand the physics and chemistry involved in propellant combustion processes in micro-scale combustors for propulsion systems on micro-spacecraft. These spacecraft are planned to have a mass less than 50 kg with attitude control estimated to be in the 1–10 mN thrust class. Micro-propulsion devices behave differently than macro-scale devices because of the differences in magnitude of flow rates and heat transfer. Reducing the combustor size increases the relative surface area, increasing the heat loss, and as combustors are continuously reduced in size, they approach the quenching dimensions of the propellants. Combustors of this size are expected to significantly benefit from surface catalysis processes. A miniature flame tube apparatus is chosen for this study because microtubes can be easily fabricated from known catalyst materials, and their simplicity in geometry can be used in fundamental simulations for validation purposes. Experimentally, we investigated the role of catalytically active surfaces within 0.4 and 0.8 mm internal diameter microtubes, with special emphases on ignition processes in fuel rich gaseous hydrogen and gaseous oxygen. Calculations of flame thickness and reaction zone thickness predict that the diameters of our test apparatus are below the quenching diameter of the propellants in most atmospheric test conditions. The temperature and pressure rise in resistively heated platinum microtubes and the exit hydrogen concentration were used as an indication of exothermic reactions. Data on imposed heat flux/preheat temperature required to achieve ignition versus mass flow rate are presented. With a plug flow model, the experimental conditions were simulated with detailed gas-phase chemistry and surface kinetics. Computational results, in general, support the experimental findings.