High strain-rate behavior of ice under uniaxial compression

In the present study, a modified split Hopkinson pressure bar (SHPB) is employed to investigate the dynamic response of ice under uniaxial compression in the range of strain rates from 60 to 1400 s^?1 and at initial test temperatures of ?10 and ?30 °C. The compressive strength of ice shows positive strain-rate sensitivity over the range of strain rates employed; a slight influence of ice microstructure is observed, but it is much less than that reported previously for ice deformation under quasi-static loading conditions [Schulson, E.M., IIiescu, D., Frott, A., 2005. Characterization of ice for return-to-flight of the space shuttle. Part 1 – Hard ice. NASA CR-2005-213643-Part 1]. Specimen thickness, within the range studied, was found to have little or no effect on the peak (failure) strength of ice, while lowering the test temperature from ?10 to ?30 °C had a considerable effect, with ice behaving stronger at the lower test temperature. Moreover, unlike in the case of uniaxial quasi-static compression of ice, the effect of specimen end-constraint during the high rate compression was found to be negligible. One important result of these experiments, which may have important implications in modeling ice impacts, involves the post “peak-stress” behavior of the ice in that the ice samples do not catastrophically lose their load carrying capacity even after the attainment of peak stress during dynamic compression. This residual (tail) strength of the damaged/fragmented ice is sizable, and in some cases is larger than the quasi-static compression strength reported for ice. Moreover, this residual strength is observed to be dependent on sample thickness and the strain rate, being higher for thinner samples and at higher strain-rates during dynamic compression.     

Mechanical behavior of Gamma-Met PX under uniaxial loading at elevated temperatures and high strain rates

Gamma titanium aluminides have received considerable attention over the last decade. These alloys are known to have low density, good high temperature strength retention and good oxidation and corrosion resistance. However, poor ductility and low fracture toughness have been the key limiting factors in the full utilization of these alloys. More recently, a new generation of gamma titanium aluminide alloys, commonly referred to as Gamma-Met PX, has been developed by GKSS, Germany. These alloys have been observed to have superior strength and better oxidation resistance at elevated temperatures when compared with conventional gamma titanium aluminides.The present paper discusses results of a study to understand the uniaxial mechanical behavior in both compression and tension of Gamma-Met PX at elevated temperatures and high strain rates. The compression and tensile tests are conducted using a modified Split-Hopkinson Bar apparatus at test temperatures ranging from room temperature to 900 °C and strain rates of up to 3500 s⁻¹. Under uniaxial compression, in the temperature range from room to 600 °C, the flow stress is observed to be nearly independent of test temperature. However, at temperatures higher than 600 °C thermal softening is observed at all strain rates with the rate of thermal softening increasing dramatically between 800 and 900 °C. The room temperature tensile tests show negligible strain-rate dependence on both yield stress and flow stress. With an increase in test temperature from room to 900 °C, the material shows a drop in both yield and flow stress at all levels of plastic strain. However, the measured flow stress is still higher when compared to nickel based super-alloys and other gamma titanium aluminides under similar test conditions. Also, no anomaly in yield stress is observed up to 900 °C.     

Influence of temperature and strain rate on the mechanical behavior of three amorphous polymers: Characterization and modeling of the compressive yield stress

Uniaxial compression stress–strain tests were carried out on three commercial amorphous polymers: polycarbonate (PC), polymethylmethacrylate (PMMA), and polyamideimide (PAI). The experiments were conducted under a wide range of temperatures (−40 °C to 180 °C) and strain rates (0.0001 s⁻¹ up to 5000 s⁻¹). A modified split-Hopkinson pressure bar was used for high strain rate tests. Temperature and strain rate greatly influence the mechanical response of the three polymers. In particular, the yield stress is found to increase with decreasing temperature and with increasing strain rate. The experimental data for the compressive yield stress were modeled for a wide range of strain rates and temperatures according to a new formulation of the cooperative model based on a strain rate/temperature superposition principle. The modeling results of the cooperative model provide evidence on the secondary transition by linking the yield behavior to the energy associated to the β mechanical loss peak. The effect of hydrostatic pressure is also addressed from a modeling perspective.     

Effect of strain rate,moisture and temperature on the deformation behavior of polymer roll covers

Soft polymer roll covers, which are used in certain positions of paper manufacturing machines, have a vital role in the dynamics of two mating rotating rolls (i.e., nip dynamics). The polymer covers are often used in moist conditions where the loading rates are rather high and temperatures may vary from 45 to 60°C. In this paper, we study the dynamic mechanical behavior of two soft polyurethane composite roll covers under different conditions of temperature, moisture, and loading rate. For the tests in compression, both servohydraulic materials testing machines and the split Hopkinson pressure bar technique were used in the strain rate range of 0.001–1500 s⁻¹. The specimens, which were to be tested under moist conditions, were immersed in paper machine water (pH 4.5) until saturated moisture content was reached. The materials showed remarkable softening as well as decrease in the strain rate sensitivity in moist conditions.     

Synchronous Full-Field Strain and Temperature Measurement in Tensile Tests at Low,Intermediate and High Strain Rates

Tensile tests with simultaneous full-field strain and temperature measurements at the nominal strain rates of 0.01, 0.1, 1, 200 and 3000 s^?1 are presented. Three different testing methods with specimens of the same thin and flat gage-section geometry are utilized. The full-field deformation is measured on one side of the specimen, using the DIC technique with low and high speed visible cameras, and the full-field temperature is measured on the opposite side using an IR camera. Austenitic stainless steel is used as the test material. The results show that a similar deformation pattern evolves at all strain rates with an initial uniform deformation up to the strain of 0.25–0.35, followed by necking with localized deformation with a maximum strain of 0.7–0.95. The strain rate in the necking regions can exceed three times the nominal strain rate. The duration of the tests vary from 57 s at the lowest strain rate to 197 μs at the highest strain rate. The results show temperature rise at all strain rates. The temperature rise increases with strain rate as the test duration shortens and there is less time for the heat to dissipate. At a strain rate of 0.01 s^?1 the temperature rise is small (up to 48 °C) but noticeable. At a strain rate of 0.1 the temperature rises up to 140 °C and at a strain rate of 1 s^?1 up to 260 °C. The temperature increase in the tests at strain rates of 200 s^?1 and 3000 s^?1 is nearly the same with the maximum temperature reaching 375 °C.     

Thermo-mechanical response of nylon 101 under uniaxial and multi-axial loadings: Part I,Experimental results over wide ranges of temperatures and strain rates

A comprehensive study of the thermo-mechanical response of a thermoplastic polymer, nylon 101 is presented. Quasi-static and dynamic compression uniaxial and multi-axial experiments (stress states) were performed at a wide range of strain rates (10⁻⁵ to 5000 s⁻¹) and temperatures (−60 to 177 °C or −76 to 350 °F). The material is found to be non-linearly dependent on strain rate and temperature. The change in volume after plastic deformation is investigated and is found to be negligibly small. The relaxation and creep responses at room temperature are found to be dependent on strain rate and the stress–strain level at which these phenomena are initiated. Total deformation is decomposed into visco-elastic and visco-plastic components; these components have been determined at different levels of deformation. Results from non-proportional uniaxial to biaxial compression, and torsion experiments, are also reported for three different strain rates at room temperature. It is shown that nylon 101 has a response dependent on the hydrostatic pressure.     

A High-frequency High-temperature Optical Strain/Displacement Gage

This paper describes an optical method for measuring strain or crack-opening displacement at high frequencies (20 kHz) and high temperatures (590°C) on a near-real-time basis. Two small reflective markers are placed on a smooth specimen or across a crack. When illuminated with a laser, interference fringes are generated; their motion can be monitored with photomultiplier tubes. The data acquisition system acquires 200 points per 50 microsecond cycle. These are processed, displayed, and stored at a rate of 25 Hz. Applications are in the general area of very high cycle (10⁹ cycles or more) fatigue. Demonstration tests at 20 kHz at room temperature with a strain range of 0.45 percent and at 590°C with a range of 0.2 percent are presented along with room temperature displacements up to 0.7 μm across the center of a 1.4 mm long crack.     

Thermomechanical behavior of casting sands: Experiments and elastoplastic modeling

The thermomechanical behavior of casting sands is discussed from an experimental and a theoretical point of view. Uniaxial compression tests at temperatures ranging from 20°C to 950°C and at different values of strain rate (ϵ = 10⁻² s⁻¹, ϵ = 10⁻³ s⁻¹ and ϵ = 10⁻⁴ s⁻¹) have been performed. They show that casting sands exhibit no strain rate effect in the temperature range 20–600°C, and that an elastoplastic model is well suited to describe the experimental results. Three thermoelastoplastic models, derived from Cam Clay and Hujeux models have been developed. These new models take into account the cohesion of the material. The physical parameters needed for these models have been obtained in the temperature range 20–300°C by using triaxial tests, uniaxial compression tests, isotropic compression tests and die pressing tests. An original triaxial apparatus has been built allowing a temperature of 800°C and a pressure of 4 MPa to be reached. In the temperature at which the parameters have been obtained (20–300°C), two additional triaxial compression tests at different confining pressures are used to check the validity of the thermoelastoplastic models used. The best quantitative results are obtained with the revised modified Cam Clay model.     

Wireless strain and temperature measurement with radio telemetry

A line of miniature strain and temperature telemetry transmitters have been developed for measurements in areas where direct-wire connections are not possible. The units described are 8–16 cu cm in volume (0.5–1.0 cu in.) and operate over a 0°C to 150°C ambient-temperature range with up to 30,000g′s acceleration. Battery life with a battery about the same size as the transmitter ranges from 50 to 200 hr. There is no degradation in accuracy for a 25-percent variation in battery voltage. Two types of strain transmitters have been developed. Both have full-scale ranges adjustable from 500 to 5000 microstrain and accuracies of ±2 percent. The “static” unit has response from dc to 1 KHz and the “dynamic” transmitter handles 30 Hz to 20 KHz. There are also two types of temperature transmitters. One accepts a variety of thermistor sensors for various measurement ranges between ?100°C and +600°C with accuracies of ±1°C. The other accepts various thermocouple inputs and has an accuracy of ±2 percent of range. These transmitters have been employed for a variety of industrial and scientific measurements. Some of the successful applications include transmission of strain and temperature data directly from pistons of reciprocating engines and from the compressor turbines of fan-jet engines.     

超高强度钢AF1410塑性流动特性及其本构关系

在本文中,为揭示超高强度钢AF1410的塑性流动性,并研究其塑性流动本构关系,利用CSS4410电子万能试验机和改进的Hopkinson拉压杆技术,对AF1410钢在温度从100K到600K,应变率从0.001/s到2000/s,塑性应变超过20%的塑性流动特性进行了试验研究。结果表明,拉伸加载下AF1410钢屈服强度低于压缩屈服强度,且随应变率增加,拉压屈服强度差值越来越大;该材料塑性流动应力对应变率敏感性低,而对温度较为敏感;随应变率的提高,该材料拉伸失效应变减小,但温度对失效应变无明显影响。最后基于位错的运动学关系,借助试验数据,获得了AF1410钢的塑性流动物理概念本构模型,并通过与经典J-C模型的结果对比对该物理概念本构模型进行了评估分析,表明该物理概念本构模型在较宽温度和应变率范围能较好的预测AF1410钢的塑性流动应力。     

Strain-rate history and temperature effects on the torsional-shear behavior of a mild steel

Previous investigations on the effects of strain-rate and temperature histories on the mechanical behavior of steel are briefly reviewed. A study is presented on the influence of strain rate and strain-rate history on the shear behavior of a mild steel, over a wide range of temperature Experiments were performed on thin-walled tubular specimens of short gage length, using a torsional split-Hopkinson-bar apparatus adapted to permit quasi-static as well as dynamic straining at different temperatures. The constant-rate behavior was first measured at nominal strain rates of 10^?3 and 10³ s^?1 for ?150, ?100, ?50, 20, 200 and 400°C. Tests were then carried out, at the same temperatures, in which the strain rate was suddenly increased during deformation from the lower to the higher rate at various large values of plastic strain. The increase in rate occurred in a time of the order of 20 μs so that relatively little change of strain took place during the jump. The low strain-rate results show a well-defined elastic limit but no yield drop, a small yield plateau is found at room temperature. The subsequent strain hardening shows a maximum at 200°C, when serrated flow occurs and the ductility is reduced. The high strain-rate results show a considerable drop of stress at yield. The post-yield flow stress decreases steadily with increasing temperature, throughout the temperature range investigated. At room temperature and below, the strain-hardening rate becomes negative at large strains. The adiabatic temperature rise in the dynamic tests was computed on the assumption that the plastic work is entirely converted to heat. This enabled the isothermal dynamic stress-strain curves to be calculated, and showed that considerable thermal softening took place. The initial response to a strain-rate jump is approximately elastic, and has a magnitude which increases with decrease of testing temperature; it is little affected by the amount of prestrain. At 200 and 400° C, a yield drop occurs after the initial stress increment. The post-jump flow stress is always greater than that for the same strain in a constant-rate dynamic test, the strain-hardening rate becoming negative at large strains or low testing temperature. This observed effect of strain-rate history cannot be explained by the thermal softening accompanying dynamic deformation. These and other results concerning total ductility under various strain-rate and temperature conditions show that strain-rate history strongly affects the mechanical behavior of the mild steel tested and, hence, should be taken into account in the formulation of constitutive equations for that material.     

The Effect of Grain Size on Deformation and Failure of Ti<Subscript>2</Subscript>AlC MAX Phase under Thermo-Mechanical Loading

An experimental investigation was performed to analyze the effects of grain size on the quasi-static and dynamic behavior of Ti₂AlC. High-density Ti₂AlC samples of three different grain sizes were densified using Spark Plasma Sintering and Pressureless sintering. A servo-hydraulic testing machine equipped with a vertical split furnace, and SiC pushrods, was used for the quasi-static experiments. Also, a Split Hopkinson Pressure Bar (SHPB) apparatus and an induction coil heating system were used for the dynamic experiments. A series of experiments were conducted at temperatures ranging from 25 °C to 1100 °C for strain rates of 10^?4 s^?1 and 400 s^?1. The results show that under quasi-static loading the specimens experience a brittle failure for temperatures below Brittle to Plastic Transition Temperature (BPTT) of 900–1000 °C and large deformation at temperatures above the BPTT. During dynamic experiments, the specimens exhibited brittle failure, with the failure transitioning from catastrophic failure at lower temperatures to graceful failure (softening while bearing load) at higher temperatures, and with the propensity for graceful failure increasing with increasing grain size. The compressive strengths of different grain sizes at a given temperature can be related to the grain length by a Hall-Petch type relation.     

Compression-impact testing of aluminum at elevated temperatures

This paper presents and experimental technique for determining compressive stress-strain curves well into the plastic range of relatively soft metals at strain rates from 300 to 2000 sec^?1 at six temperatures from 30 to 550° C. More than 100 curves were obtained on annealed 1100° F aluminum. The strain-rate dependence in these tests could be fitted quite well either by a power function (log-log plot) or by a semilogarithmic plot, but the power function gave a better correlation of the present data with that obtained at lower strain rates by Alder and Phillips.¹     

Apparatus for Testing Concrete under Multiaxial Compression at Elevated Temperature (mac2T)

This paper describes a new test facility for determining material mechanical properties of structural concrete. The novel facility subjects 100 mm cubic concrete specimens to true multiaxial compression (σ₁ ≠ σ₂ ≠ σ₃) up to 400 MPa at temperatures of up to 300°C. Forces are delivered through three independent loading frames equipped with servo-controlled hydraulic actuators creating uniform displacement boundary conditions via rigid platens. Specimen deformation is calculated from displacements measured to an accuracy of 10⁻⁶ m using a system of six laser interferometers. The combination of stiff loading frames, rigid platens, an accurate and reliable strain measurement system and a fast control system enables investigation of the material response in the post-peak range. The in-house developed control software allows complex multi-stage experiments involving (i) load and temperature cycling, (ii) small stress probes and (iii) arbitrary (pre-defined) loading paths. The program also enables experiments in which the values of the control parameters and the execution of the test sequences depend on the response of the specimen during the test. The capabilities of the facility are illustrated in this paper by experiments determining the effects of different heat-load regimes on the strength and stiffness of the material and tests identifying the tangent stiffness matrix of the material and the associated changes in the acoustic tensor under multiaxial compression.     

Time-dependent ratchetting experiments of SS304 stainless steel

The time-dependent strain cyclic characteristics and ratchetting behaviours of SS304 stainless steel were investigated by uniaxial/multiaxial cyclic loading tests at room and elevated temperatures (350 and 700 °C). The effects of loading rate, peak/valley strain or stress holds, ambient temperature and non-proportional loading path on the cyclic softening/hardening and ratchetting behaviours of the material were discussed. It is shown that: the cyclic deformation of the material presents remarkable time-dependence at room temperature and 700 °C; the cyclic hardening feature and ratchetting strain depend significantly on straining or stressing rate, hold-time, ambient temperature and the non-proportionality of loading path; the time-dependent ratchetting is resulted from the slight opening of hysteresis loop and visco-plasticity together, and the viscosity is a dominating factor at 700 °C; at 350 °C, abnormal rate-dependence and quick shakedown of ratchetting are observed due to the dynamic strain aging of the material at this temperature. Some significant conclusions are obtained, which are useful to construct a constitutive model to describe the time-dependent ratchetting behaviour of the material. It is also stated that the unified visco-plastic constitutive model discussed here cannot provide reasonable simulation to the time-dependent ratchetting at 700 °C, especially to that with certain peak/valley stress hold, since the effect of the high viscosity on time-dependent ratchetting cannot be properly described by using a unified visco-plastic flow rule.     

A viscoplastic constitutive model for nickel-base superalloy,part 2: modeling under anisothermal conditions

In Part 2 of this study, extensive deformation tests were carried out on the nickel-base polycrystalline superalloy IN738LC under isothermal and anisothermal conditions between 450 and 950 °C. Under the isothermal conditions, the material showed almost no rate/time-dependency below 700 °C, while it showed distinct rate/time-dependency above 800 °C. Regarding the cyclic deformation, slight cyclic hardening behavior was observed when the temperature was below 700 °C and the imposed strain rate was fast, whereas in the case of the temperature above 800 °C or under slower strain rate conditions, the cyclic hardening behavior was scarcely observed. Unique inelastic behavior was observed under in-phase and out-of-phase anisothermal conditions: with an increase in the number of cycles, the stress at higher temperatures became smaller and the stress at lower temperatures became larger in absolute value although the stress range was approximately constant during the cyclic loading. In other words, the mean stress continues to evolve cycle-by-cycle in the direction of the stress at lower temperatures. Based on the experimental results, it was assumed that evolution of the variable Y that had been incorporated into a kinematic hardening rule in Part 1 of this study is active under higher temperatures and is negligible under lower temperatures. The material constants used in the constitutive equations were determined with the isothermal data, and were expressed as functions of temperature empirically. The extended viscoplastic constitutive equations were applied to the anisothermal cyclic loading as well as the monotonic tension, stress relaxation, creep and cyclic loading under the isothermal conditions. It was demonstrated that the present viscoplastic constitutive model was successful in describing the inelastic behavior of the material adequately, including the anomalous inelastic behavior observed under the anisothermal conditions, owing to the consideration of the variable Y.     

Balanced Biaxial Testing of Advanced High Strength Steels in Warm Conditions

The main purpose of the present work is to measure the stress–strain behavior under warm conditions (about 100 °C) of advanced high strength steel (AHSS) sheets up to large strains compared to uniaxial tension. The test equipment consists of two main parts, i.e., a hydraulic bulge tester and a heating device. A mechanical system is attached to the test equipment for measuring the membrane stress and thickness strain at the bulge pole. The stress–strain curves were measured for three kinds of AHSS sheets with the proposed test method for various initial temperatures (10, 50 and 100 °C). The proposed method does not provide isothermal stress–strain curves because the specimen temperature increases during the test due to the effect of deformation-induced heating. A numerical scheme using thermo-mechanical finite element (FE) simulations is suggested to deconvolute the isothermal stress–strain curves.     

Influence of Portevin-Le Chatelier Effect on Shear Strain Path Reversal in an Al-Mg Alloy at Room and High Temperatures

The main objective of this study is to characterize the mechanical behaviour of an Al-Mg alloy in conditions close to those encountered during sheet forming processes, i.e. with strain path changes and at strain rates and temperatures in the range 1.2×10^?3–1.2×10^?1 s^?1 and 25–200°C, respectively. The onset of jerky flow and the interaction of dynamic strain ageing with the work-hardening are investigated during reversed-loading in specific simple shear tests, which consist of loading up to various shear strain values followed by reloading in the opposite direction, combined with direct observations of the sample surface using a digital image correlation technique. Both strain path changes and temperature are clearly shown to influence the occurrence and onset of the Portevin-Le Chatelier (PLC) effect. Moreover, the Bauschinger effect observed in the material response shows that the PLC effect has a major influence on the kinematic contribution to work-hardening as well as its stagnation during the reloading stage, which could open up interesting lines of research to improve theoretical plasticity models for this family of aluminium alloys.     

Cyclic thermo-viscoplasticity of high density polyethylene

Observations are reported in uniaxial cyclic tensile tests (loading–unloading with various maximum strains) on high density polyethylene at temperatures ranging from room temperature up to 90 °C. It is demonstrated that the maximum stress per cycle and an apparent residual strain (measured at the instant when the tensile force vanishes under retraction) strongly decrease with temperature. The latter seems unexpected as the interval of temperatures covers the α-relaxation temperature, which is conventionally associated with activation of additional mechanisms for inelastic flow. A model is developed that captures the decrease in residual strain with temperature. Adjustable parameters in the stress–strain relations are found by fitting the experimental data. The effects of temperature and maximum strain per cycle on residual strains are studied numerically.