共查询到20条相似文献,搜索用时 15 毫秒
1.
S. Yu. Kukushkin P. Yu. Ivanov L. M. Alekseeva K. I. Kobrakov V. G. Granik 《Russian Chemical Bulletin》2004,53(12):2856-2861
Methods for the synthesis of substituted pyrimido [4,5-a]- and pyrido[4,3-a]carbazoles were proposed. Condensation of 2-(dimethylaminomethylene)-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one with guanidine and thiourea afforded 2-amino-8-methyl-6,11-dihydro-5H-pyrimido[4,5-a]carbazole and 8-methyl-3,5,6,11-tetrahydro-2H-pyrimido[4,5-a]carbazole-2-thione, respectively. The reaction of cyano(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-ylidene)acetamide with dimethylformamide dimethyl acetal gave N-(dimethylamino-methylene)cyano(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-ylidene)acetamide. Cyclization of the latter yielded 1-cyano-8-methyl-3,5,6,11-tetrahydro-2H-pyrido[4,3-a]carbazol-2-one.__________Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 12, pp. 2740–2744, December, 2004. 相似文献
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E. V. Nosova G. N. Lipunova M. I. Kodess P. V. Vasil’eva V. N. Charushin 《Russian Chemical Bulletin》2004,53(10):2314-2318
Reactions of 2-aminopyridine and 2-amino-5-methylpyridine with 2,3,4,5-tetrafluorobenzoyl chloride afforded N,N’-diaroylpyridinium salts, which were converted into 6H-pyrido[1,2-a]quinazolin-6-ones by refluxing in toluene in the presence of triethylamine. The angular structure of the tricyclic derivatives obtained was confirmed by 19F and 13C NMR spectroscopy and 2D heteronuclear HetCOR and HMBC experiments.__________Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 10, pp. 2216–2220, October, 2004. 相似文献
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P. A. Slepukhin G. L. Rusinov S. S. Dedeneva V. N. Charushin 《Russian Chemical Bulletin》2007,56(2):345-350
The reactions of 8-chlorotetrazolo[1,5-a]pyrazine with N-, O-, and S-nucleophiles involve the ipso substitution of the chlorine atom. Heating of this compound with benzotriazole or phenyltetrazole results in elimination
of the nitrogen molecule from one of the tetrazole rings to form new annelated azapentalenes.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 2, pp. 334–338, February, 2007. 相似文献
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Kh. S. Shikhaliev D. V. Kryl’skii A. Yu. Potapov M. Yu. Krysin 《Russian Chemical Bulletin》2005,54(12):2903-2904
Three-component condensation of 3-amino-1,2,4-triazole (or its 5-methyl and 5-methylthio derivatives), dimedone (or cyclohexane-1,3-dione),
and dimethylformamide dimethyl acetal afforded 8,8-R, R-8,9-dihydro[1,2,4]triazolo[1,5-a]quinazolin-6(7H)-ones.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 12, pp. 2805–2807, December, 2005. 相似文献
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V. I. Terenin M. A. Butkevich A. P. Pleshkova 《Chemistry of Heterocyclic Compounds》2005,41(10):1327-1333
We have synthesized nitro derivatives of pyrrolo[1,2-a]pyrazines using a nitrating mixture and acetyl nitrate. We have obtained
the products of oxidation of the side chain of 1,6-substituted pyrrolo[1,2-a]-pyrazines.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 10, pp. 1579–1586, October, 2005. 相似文献
12.
V. I. Terenin E. V. Kabanova N. A. Tselishcheva A. S. Ivanov N. V. Zyk 《Chemistry of Heterocyclic Compounds》2007,43(8):1038-1043
A study was carried out on the reaction of pyrrolo[1,2-a]pyrazines containing an alkyl, aryl, or aralkyl substituent at C-1
with trifluoroacetic anhydride. Trifluoroacetylation products may be formed either by reaction in the pyrrole ring or at the
aryl or aralkyl groups at C-1. Products of electrophilic substitution at C-6 are formed in the trifluoroacetylation of pyrrolo[1,2-a]pyrazines
containing at C-1 a substituent bulkier than a methyl group but lacking substituents at C-6 (the α-position of the pyrrole
ring).
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 8, pp. 1226–1233, August, 2007. 相似文献
13.
E. B. Tsupak M. A. Shevchenko V. V. Kostrub Yu. N. Tkachenko 《Russian Chemical Bulletin》2007,56(11):2330-2336
5-Aroyl-1,3,6-trimethyluracils were converted to pyrano[4,3-d]pyrimidinium salts. Reactions of the salts obtained with ammonia, primary amines, and hydrazine were studied.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 11, pp. 2251–2257, November, 2007. 相似文献
14.
R. V. Tyurin E. V. Vorob’ev L. G. Minyaeva V. V. Krasnikov V. V. Mezheritskii 《Russian Journal of Organic Chemistry》2005,41(6):916-921
Formimidic acid esters derived from 1-substituted 5-aminopyrazole-4-carbonitriles reacted with carboxylic acid hydrazides on heating to give 2,7-disubstituted pyrazolo[4,3-e][1,2,4]triazolo[1,5-c]pyrimidine derivatives as a result of double heterocyclization. The same compounds were obtained by thermal recyclization of 1-aroyl-2-(1-R-pyrazolo[3,4-d]pyrimidin-4-yl)hydrazines.__________Translated from Zhurnal Organicheskoi Khimii, Vol. 41, No. 6, 2005, pp. 934–938.Original Russian Text Copyright © 2005 by Tyurin, Vorob’ev, Minyaeva, Krasnikov, Mezheritskii. 相似文献
15.
V. V. Lipson S. M. Desenko M. G. Shirobokova V. V. Borodina V. I. Musatov 《Chemistry of Heterocyclic Compounds》2005,41(4):492-495
The hydrolysis, oxidation, reduction, alkylation, formylation, and nitrosation reactions of 2-methyl-5,7-diphenyl-6,7-dihydropyrazolo[1,5-a]pyrimidine have been studied.__________Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 577–581, April, 2005. 相似文献
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V. V. Lyaskovskyy Z. V. Voitenko V. A. Kovtunenko 《Chemistry of Heterocyclic Compounds》2007,43(3):253-276
Data on methods for the synthesis of isoindolo[2,1-a]benzimidazole and its derivatives and their chemical characteristics
are reviewed. Data from quantum-chemical calculations of certain structures are presented. Possible practical applications
of the compounds are indicated.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 3, pp. 323–351, March, 2007. 相似文献
18.
V. L. Gein N. N. Kasimova L. I. Varkentin G. A. Stashina 《Chemistry of Heterocyclic Compounds》2005,41(8):1041-1044
The reaction of substituted methyl aroylpyruvates with 1-aminomethyl-1,2,3,4-tetrahydroisoquinoline dihydrochloride in the
presence of AcOH gives 3-aroylmethylene-1,6,7,11b-tetrahydro-2H-pyrazino[2,1-a]isoquinolin-4-ones whose structures have been
confirmed by IR, 1H NMR, and mass spectrometry.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 8, pp. 1218–1221, August, 2005. 相似文献
19.
B. S. Fedorov A. N. Utienyshev A. A. Ghidaspov E. V. Kachanovskaya V. V. Bakharev M. A. Fadeev 《Chemistry of Heterocyclic Compounds》2005,41(4):496-502
A new heterocyclic compound, 3-methyl-5-trinitromethyltetrazolo[1,5-a]-1,3,5-triazin-7-one, was synthesized by the reaction of methyl iodide and the silver salt of 5-trinitromethyltetrazolo[1,5-a]-1,3,5-triazin-7-one. An X-ray diffraction structural analysis of this product was carried out and feasibility was demonstrated for the nucleophilic substitution of the trinitromethyl group in this compound by the action of phenol, phenol derivatives, and thiophenol.__________Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 582–588, April, 2005. 相似文献