YBCO带材无阻连接热退火效应研究

超导焊接是第二代高温超导(2G-HTS)带材研究的重要内容,在两根超导带材中间生长超导连接层可实现无阻连接.在超导连接层的生长过程中,原来的两根超导带材需再次经历热处理,目前这方面的研究甚少.本文系统研究了780℃热退火中,时间、气氛对带材性能的影响.分析了样品的显微结构、表面形貌以及临界电流密度(J_c),结果表明:2 h干氮氧气氛有利于提高原始带材的性能;湿氮氧气氛使J_c值降低.这可能是湿气的存在增加了晶粒缺陷,使杂质的扩散通道增加,从而Ba-Cu-O积聚生长,造成YBCO性能恶化.在文中我们还利用XRD进行了应力拟合分析了应力变化.     

高压和热处理对铝青铜微观组织的影响

 借助金相、扫描电子显微镜（SEM）/能谱仪（EDS）及X射线衍射（XRD）等方法,研究了高压和热处理对铝青铜微观组织的影响。结果表明：铝青铜经750 ℃温度、6 GPa压力处理后所获得的α相的晶粒尺寸较经750 ℃温度、常压处理后所获得的α相晶粒尺寸小;当铝青铜经高压处理后再经750 ℃保温2 min常压处理时,组织中出现细条状的α相,且热处理后的冷却速度越大,细条状α相的数量越多,颗粒状α相的数量越少。     

分离式热管换热器传热特性的实验研究

本文在自行设计分离式热管实验装置的基础上,对其传热特性进行了实验研究。其工作温度为170～250℃,热流密度为25～50 kW/m~2。蒸发段和冷凝段构成相同,均是由7根直径30 mm的无缝钢管短管束组成,管长为160 mm,带有紧套的钢帛环形肋片结构尺寸为:外径45 mm、厚1 mm、片间距4 mm。实验结果表明,在本实验条件下,分离式热管的最佳充液率按管束总容量计为18%～38%。根据实验结果拟合了最佳充液率(24%)下蒸发段内部平均沸腾换热系数和冷凝段内部凝结换热努塞尔数综合关系式。     

Effect of Heat Treatment on the Mechanical and Tribological Properties of Polyphenylene Sulfide Fiber Materials

Polyphenylene sulfide (PPS) fiber materials, whose raw fibers had been heat treated previously for 1 to 5 days, were prepared by a hot-pressing method. The tribological properties of PPS resin and fiber materials against an AISI 1045 steel ring were evaluated using a block-on-ring wear tester. The results showed that the sample whose raw fibers had been heated at 240°C for 1 day (S1) exhibited the highest impact strength as well as the lowest friction coefficient and wear rate. The friction coefficient of S1 was 39% lower than that of the PPS resin material, and its wear rate was 1 to 2 orders of magnitude lower than those of the other samples. DSC analysis results indicated that the condensed structure of the samples gradually changed from the crystalline to the amorphous state with the increase of heat-treatment time of the raw fibers. DMA and DSC analysis results proved that severe, oxidative cross-linking reactions occurred when the raw fibers were heated over 3 days. It is concluded that proper heat treatment of the raw fibers is advantageous to improve the degree of crystallinity and appropriate oxidative cross-linking; therefore, the prepared PPS fiber material can exhibit better mechanical and tribological performances.     

Study on Laser Heat Treatment of Cemented Carbide

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颗粒帘换热器中气粒两相换热特性实验研究

根据某1 t/h燃煤工业锅炉空气预热器的热力参数,设计并搭建了一套颗粒帘空气预热器模拟实验系统,研究了不同进气温度Tg0(150~300℃)、进气速度Vg0(0.9~1.5m/s)、颗粒帘进口厚度b0 (60~180 mm)、颗粒粒径dp(150~212μm)以及不同颗粒质量流量ms (550~2150 g/s)工况条件下热空气与进口温度tp0=20℃的硅砂颗粒帘间的换热特性。结果表明:影响颗粒帘换热器中气粒两相换热特性因素的重要性次序为进气温度、进气速度、颗粒质量流量、颗粒粒径、颗粒帘进口厚度;换热端差最低可至4.5℃,最大可达87℃;颗粒帘及颗粒帘出口气流的温度沿颗粒下落方向在前期上升迅速(186~475℃/m)而后期上升比较缓慢(60~108℃/m),并且在0~0.5 m和0.5~1.0 m的高度范围可分别用线性和对数方程来描述。     

Quick Approximate Calculation on the Transient Temperature Field of Laser Heat Treatment

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超大拓展表面三维微肋管换热器的对流换热及抗积灰特性研究

工业烟气含尘的特点易导致换热器积灰,进而制约烟气余热的高效回收。本文针对一种具有超大拓展表面的三维微肋管换热器的对流换热与积灰特性进行了研究。首先,对比研究了光管与三维微肋管的对流换热特性;接着,基于所建立的积灰数值模型,探究了三维微肋管的积灰特性,并揭示了烟气流速与飞灰粒径对其积灰特性的影响规律。结果表明,相对于传统光管,三维微肋管的换热面积可增大约2.9倍;换热性能平均能提高16%;积灰后渐进污垢热阻最大能减小70%;同时,清灰周期更长,运行经济性更佳。综合而言,三维微肋管相比传统光管,在增强换热的同时,还能有效减轻积灰,因此可作为高效的抗积灰传热元件,应用于含尘烟气的余热回收场合。     

热处理和紫外辐射对DNA影响的拉曼光谱研究

检测了鲕鱼精ＤＮＡ纤维和经过４０℃，９１℃，２００℃加热处理的拉曼光谱。研究结果表明，在熔融温度以下热处理对ＤＮＡ构象的影响是轻微的，在熔融温度以上则随温度的升高，对ＤＮＡ分子结构的影响有破坏也逐渐加剧，首先受影响的是腺嘌呤和脱氧核糖。     

矩形微槽横截面换热特性的分析

对矩形毛细微槽中液膜在横截面方向上的换热特性进行了研究。计算结果表明,当弯月面与槽底接触时,不仅在微槽的侧壁面上存在两个蒸发薄液膜区,在槽底还形成了两个蒸发薄液膜区;随着槽底热负荷的增大,薄液膜区域热流密度的峰值随之升高;固液接触角增大,薄液膜区域的热流密度峰值增大;薄液膜区域的高强度蒸发换热是矩形毛细微槽高强度换热的主要原因,占总换热量的80%以上;固液界面接触角对薄液膜换热的影响很大。     

多孔结构毛细芯蒸发器传热特性的实验研究

本文针对不同压力条件下不同换热表面结构的毛细结构蒸发器气(?)液相变传热特性进行了实验研究。选取微槽道结构和烧结丝网结构的换热表面分别在蒸发压力为0.86×10~5 Pa、0.91×10~5 Pa、0 96×10~5 Pa、1.0×10~5 Pa、1.5×10~5 Pa、2.0×10~5 Pa条件下进行了传热特性研究并对其实验结果进行对比,结果表明,压力对换热系数有重要的影响,当压力范围为0.86×10~5～1.0×10~5 Pa时,在过热度相同的条件下,随着压力的增加,换热系数呈上升趋势;在较大压力的条件下,换热系数随着过热度的增加呈先升后降的趋势。     

高压热处理对铝青铜热物理性能的影响

在5 GPa压力下对铝青铜进行750℃、保温15 min的高压热处理,对高压热处理前后铝青铜的电导率以及25～600℃温度范围内的热扩散系数、热容和热导率进行测试,结合显微组织的观察结果,探讨了高压热处理对铝青铜热物理性能的影响。研究表明:高压热处理能增大铝青铜的热扩散系数,减小热容;对热导率而言,温度低于400℃时高压热处理能增大铝青铜的热导率,而温度高于400℃时高压热处理能减小铝青铜的热导率。分析认为,产生变化的主要原因是高压热处理使铝青铜的微观组织发生了变化。     

静水高压处理对水稻植株生理特性的影响

 以75 MPa静水高压处理萌动的水稻种子12 h，成苗后移栽至大田，研究高压处理后植株剑叶光合特性的变化。结果显示，静水高压处理后，粤香占和粤丰占种子的发芽率分别降低了14.4% 和16.6%，成苗率分别降至对照的24.6%和21.9%，生长明显受抑制，幼苗的株高在35天左右才能追赶上对照。高压处理的粤香占剑叶在生育过程中的净光合速率（P_n）和表观量子效率（AQY）的总平均值分别比未处理的对照增加了9.2%和12.4%，而粤丰占则分别增加5.7%和17.4%。高压处理后两个品种的植株叶片不同生长时期的平均光合色素含量均高于未处理的对照，在生长后期的衰老过程中高压处理植株剑叶的色素含量和PSⅡ光化学效率F_v/F_m下降速率较各自的未处理对照缓慢。高压处理后两个水稻品种的生物量和单株产量分别比对照提高了8%~27%及7%~14%。提出高压处理可能作为一种新的选育品种的方法。     

复杂换热网络MINLP中的非线性特性分析

针对复杂换热网络MINLP问题,本文应用多维函数渐变法探索和分析了连续变量和整型变量引起的网络性能非线性和非凸特性。研究表明,当系统规模增大时,不但连续变量的叠加效应将增加系统的非线性,整型变量将使得非线性特性更为严重。     

热处理温度对铜镍镀层的光谱性能的影响

采用电沉积法在镍表面制备铜镍镀层,并将该铜镍镀层在不同温度下进行热处理。分别用扫描电镜法(SEM)、能谱法(EDAX) 和X衍射法(XRD)等对热处理后的铜镍镀层进行表征,研究热处理温度对铜镍镀层的光谱性能的影响。用电镀的方法获得的铜镍镀层表面是由节瘤组成,热处理温度在25~600 ℃范围,随着热处理温度的升高,铜镍镀层表面的节瘤变小;热处理温度在600~900 ℃范围,随着热处理温度的升高,铜镍镀层表面的节瘤变小,铜镍镀层表面的节瘤间的分界线越不明显。热处理温度在25～900 ℃范围,随着热处理温度的升高,铜镍镀层中铜的含量减小,从82.52 at%减小到78.30 at%;镍的含量增加,从17.48 at%增加到21.70 at%。铜镍镀层为Cu_0.81Ni_0.19立方晶型结构,热处理温度在25～300 ℃范围,随着热处理温度的升高,Cu_0.81Ni_0.19的晶型结构更完整;热处理温度在600～900 ℃范围,铜镍镀层中可能有部分的Cu_0.81Ni_0.19立方晶型结构转变为Cu_3.8Ni立方晶型结构;随着热处理温度的升高,有利于Cu_3.8Ni(311)和Cu_0.81N_i0.19(311) 晶面的生长。     

热处理对蛋清卵类粘蛋白过敏原性及构象的影响

采用酶联免疫吸附法(ELISA)、圆二色谱(CD)、ANS荧光探针和紫外光谱(UV)系统研究了热处理对蛋清卵类粘蛋白过敏原性及构象的影响。结果显示,加热处理卵类粘蛋白的过敏原性降低,且随加热温度升高和加热时间延长,不断降低。经不同温度热处理后的卵类粘蛋白二级结构的α-螺旋,β-折叠,β-转角和无规卷曲之间相互转化,分子有序性降低;卵类粘蛋白的表面疏水性随加热温度的升高而降低;随加热的温度的升高,具有紫外吸收的氨基酸残基逐渐暴露,最大吸光度逐渐增大。由此可以推断,卵类粘蛋白的构象改变导致其过敏原性变化。     

Infrared Spectral/Structural Investigation of the Heat Treatment of Tetramethoxysilane/Diethoxydimethylsilane-Derived Gels

Structural changes occurring during the heat treatment of gels that were prepared from binary tetramethoxysilane (TMOS)/diethoxydimethylsilane (DEDMS) mixtures were investigated using infrared spectra. Analysis of the spectral data indicated that the Si-O networks of the heat-treated gels increased their connectivity with increased dehydration due to increased treatment temperature or time. Four- and three-membered (Si-O)_n rings were noted for appropriate heat-treated gel compositions. At higher heat-treatment temperatures, methyl groups were removed from the gel network.     

热交换器表面镀层对传热性能的影响

采用化学镀的方法对热交换器表面进行表面改性,使其换热表面沉积一层表面能不同的均匀镀层。传热实验表明,随着磷含量的增大,凝结传热系数增大。进一步可视化实验研究表明,镀层换热表面均表现为珠膜共存状态,增大镀层的磷含量,换热表面促进珠状凝结的效果更加明显。这归于镀层降低了传热表面的表面能值。     

Discussion for the Semi-infinite Medium Approximation and the Thermal Diffusion Velocity in Laser Heat Treatment

It is a conventional method to regard laser-iradiated object as a semi-infinite medium with invariable thermal physical property parameters for approximate analyses of thermal acting of laser heat treatment. So far, 2 and have been taken as the thermal diffusion distance and the thermal diffusion velocity respectively, at the time t after heat fluctuation in materials with a thermal diffusion coefficient α, and as a result, the feasibility of the approximately estimating method about semi-infinite medium is judged. This paper indicates that, due to quantitative investigation of heat energy diffusion, the thermal diffusion distance of 3 and the thermal diffusion velocity of 1.5 can more accurately describe the physical process of heat conduction. Finally, an applied example of approximately estimating the temperature field of laser heat treatment is presented.     

Cooling Characteristics During Bath Quenching of Test Probe Using Inverse Heat Transfer

It is of engineering importance to accurately predict the surface cooling characteristics in bath quenching of metals and alloys. In this investigation, the surface cooling characteristics in quenching of Wolfson probe are estimated with reasonable accuracy by solving an inverse heat conduction problem. Regularization method is used for smoothening the input temperature measurements at probe center, for superior inversion estimates. The reverse pool-boiling curve is captured on bath quenching characteristic, plotted as cooling velocity versus surface temperature. The prime advantage is the bypassing of convection coefficients, which are uncertain in pool boiling.