Inelastic behavior of an AS4/PEEK composite under combined transverse compression and shear. Part I: experiments

The nonlinear behavior in shear and transverse compression of unidirectional AS4/PEEK and their interaction are investigated experimentally. The composite is rate dependent even at room temperature and its rate exponent is similar to that of neat PEEK. The material is tested under pure shear, pure compression and under biaxial loading histories. The biaxial tests are performed in a custom facility on thin strips of the material. The facility allows freedom to choose the loading path in the biaxial stress and strain spaces of interest. Tests are performed for three biaxial loading paths. In the first, the specimen is sheared then compressed while the shear stress is held constant; in the second, the specimen is compressed then sheared while the compressive stress is held constant; and in the third, the specimen is loaded simultaneously by proportional amounts of compression and shear. It was found that the induced deformation is influenced significantly by the loading history followed. Also, initial loading in shear or compression has only a modest effect on subsequent loading of the other type. An unorthodox yielding behavior for the composite results from this lack of interaction. Finally, the stresses at failure are found to trace an elliptical path in the shear–transverse compression plane, but the failure stress state is not significantly affected by the loading path followed.     

Viscoelasticity of brain corpus callosum in biaxial tension

Computational models of the brain rely on accurate constitutive relationships to model the viscoelastic behavior of brain tissue. Current viscoelastic models have been derived from experiments conducted in a single direction at a time and therefore lack information on the effects of multiaxial loading. It is also unclear if the time-dependent behavior of brain tissue is dependent on either strain magnitude or the direction of loading when subjected to tensile stresses. Therefore, biaxial stress relaxation and cyclic experiments were conducted on corpus callosum tissue isolated from fresh ovine brains. Results demonstrated the relaxation behavior to be independent of strain magnitude, and a quasi-linear viscoelastic (QLV) model was able to accurately fit the experimental data. Also, an isotropic reduced relaxation tensor was sufficient to model the stress-relaxation in both the axonal and transverse directions. The QLV model was fitted to the averaged stress relaxation tests at five strain magnitudes while using the measured strain history from the experiments. The resulting model was able to accurately predict the stresses from cyclic tests at two strain magnitudes. In addition to deriving a constitutive model from the averaged experimental data, each specimen was fitted separately and the resulting distributions of the model parameters were reported and used in a probabilistic analysis to determine the probability distribution of model predictions and the sensitivity of the model to the variance of the parameters. These results can be used to improve the viscoelastic constitutive models used in computational studies of the brain.     

脆性材料在双向应力下的断裂实验与理论分析

研究了脆性材料在双向应力下的断裂特性和失效机理，特别是在平行于裂纹的应力对临界断裂参数的影响方面进行了实验上和理论上的研究．采用玻璃、陶瓷等脆性材料进行了平面双向拉伸和单向拉伸试验，并对实验结果进行比较．观测直通裂纹的启裂和扩展过程，证明了双向应力对裂纹驱动力有明显影响，讨论了裂纹扩展的应变准则．     

Large-deformation properties of wheat dough in uni- and biaxial extension. Part I. Flour dough

Rheological and fracture properties of optimally mixed flour doughs from three wheat cultivars which perform differently in cereal products were studied in uniaxial and biaxial extension. Doughs were also tested in small angle sinusoidal oscillation. In accordance with previously published results the linear region was found to be very small. The rheological properties at small deformations hardly depended on the cultivar. A higher water content of the dough resulted in a lower value for the storage modulus and a slightly higher value for tan . For both uniaxial and biaxial extension a more than proportional increase in stress was found with increasing strain, a phenomenon called strain hardening. In uniaxial extension (i) stresses at a certain strain were higher and (ii) the stress was less dependent on the strain rate than in biaxial extension. This indicates that in elongational flow orientational effects are of large importance for the mechanical properties of flour dough. This conclusion is consistent with published data on birefringence of stretched gluten. Fracture stress and strain increased with increasing deformation rate. The observed time-dependency of fracture properties can best be explained by inefficient transport of energy to the crack tip. Presumably, this is caused by energy dissipation due to inhomogeneous deformation because of friction between structural elements, e.g. between dispersed particles and the network. Differences in the rheological properties at large deformations between the cultivars were observed with respect to (i) stress, (ii) strain hardening, (iii) strain rate dependency of the stress, (iv) fracture properties and (v) the stress difference between uniaxial and biaxial extension.     

Experimental and Numerical Analysis of an In-Plane Shear Specimen Designed for Ductile Fracture Studies

An in-plane shear specimen made of dual phase steel designed for ductile fracture studies is presented and then analyzed experimentally and numerically. In the experiment, digital image correlation (DIC) technique is utilized to measure the deformation of the specimen. Based on the implicit nonlinear FE solver Abaqus/Standard, numerical analysis of the specimen is performed by using plane stress and solid elements respectively. The elongation of the specimen’s gauge length and the shear strain distribution within the shear zone are compared between the experimental and numerical results and a general good agreement is obtained. Thereafter, based on calculated results, the stress state of the shear zone is investigated in detail. It is shown that the shear stress is dominant within the shear zone despite of the emergence of normal stresses. The deformation is concentrated in the shear zone, where the incipient fracture is most likely to occur. The stress triaxiality and the Lode parameter at the fracture initiation are found to be maintained at a relatively low level, which implies that the stress state achieved by the specimen is close to pure shear. The present study demonstrates that the proposed in-plane shear specimen is suitable for investigation of the fracture behavior of high strength materials under shear stress states.     

Non-linear viscoelastic response of magnetic fiber suspensions in oscillatory shear

This paper reports the first study on the large amplitude oscillatory shear flow for magnetic fiber suspensions subject to a magnetic field perpendicular to the flow. The suspensions used in our experiments consisted of cobalt microfibers of the average length of 37 μm and diameter of 4.9 μm, dispersed in a silicon oil. Rheological measurements have been carried out at imposed stress using a controlled stress magnetorheometer. The stress dependence of the shear moduli presented a staircase-like decrease with, at least, two viscoelastic quasi-plateaus corresponding to the onset of microscopic and macroscopic scale rearrangement of the suspension structure, respectively. The frequency behavior of the shear moduli followed a power-law trend at low frequencies and the storage modulus showed a high-frequency plateau, typical for Maxwell behavior. Our simple single relaxation time model fitted reasonably well the rheological data. To explain a relatively high viscous response of the fiber suspension, we supposed a coexistence of percolating and pivoting aggregates. Our simulations revealed that the former became unstable beyond some critical stress and broke in their middle part. At high stresses, the free aggregates were progressively destroyed by shear forces that contributed to a drastic decrease of the moduli. We have also measured and predicted the output strain waveforms and stress–strain hysteresis loops. With the growing stress, the shape of the stress–strain loops changed progressively from near-ellipsoidal one to the rounded-end rectangular one due to a progressive transition from a linear viscoelastic to a viscoplastic Bingham-like behavior.     

横观各向同性介质中椭圆夹杂受非弹性剪切变形引起的弹性场的确定

本文求解了横观各向同性介质中椭圆夹杂内受非弹性剪切变形引起的弹性场。采用各向异性弹性力学平面问题的复变函数解法,结合保角变换,获得夹杂内应变能和基体内边界的应力分布和相应的应变能的表达式。进一步,根据最小应变能原理,获得表征夹杂平衡边界的两个特征剪切应变,从而得到了弹性场的解析解。通过应力转换关系,验证了应力解满足夹杂边界上法向正应力和剪应力的连续条件,表明了该解的正确性。本文解可用于复合材料断裂强度的分析中。     

The effect of load biaxiality on crack growth in non-linear materials

The influence of load biaxiality on the stress field and fracture behavior of a cracked plate is investigated. Considered is a square plate containing a central through the thickness crack and subjected to a biaxial loading perpendicular and parallel to the crack plane. The stress field of the plate is analyzed by a finite element code based on incremental plasticity and the von Mises yield condition. A method based on the strain energy density theory is used to determine the critical stress for crack initiation. It was found that the equi-biaxial loading mode induces the smallest plastic zones, while the critical applied stress for crack initiation becomes maximum. Quite the contrary happens for the shear loading system which causes the largest plastic zones and the minimum applied stress values fro crack growth. Results showing the dependence of the above quantities on the biaxiality of the applied stress are presented in graphical form.     

Nonlinear viscoelasticity of PP/PS/SEBS blends

The nonlinear viscoelastic behavior of polypropylene/polystyrene (PP/PS) blends compatibilized or not with the linear triblock copolymer (styrene-ethylene-/butylene-styrene, SEBS) was investigated. Start-up of steady-shear at rates from 0.1 to 10 s^–1 was carried out using a controlled strain rotational rheometer and a sliding plate rheometer for strain histories involving one or several shear rates. The shear stress and first normal shear stress difference were measured as functions of time, and the morphologies of the samples before and after shearing were determined. For each strain history except that involving a single shear rate of 0.1 s^–1 the blends showed typical non-linear viscoelastic behavior: a shear stress overshoot/undershoot, depending on the history, followed by a steady state for each step. The first normal stress difference increased monotonically to a steady-state value. The values of the stresses increased with the addition of SEBS. The shear stress overshoot and undershoot and the times at which they occurred depended strongly on the strain history, decreasing for a subsequent shear rate step performed in the same direction as the former, and the time at which stress undershoot occurred increased for a subsequent shear rate step performed in the opposite direction, irrespective of the magnitude of the shear rate. This behavior was observed for all the blends studied. The time of overshoot in a single-step shear rate experiment is inversely proportional to the shear rate, and the steady-state value of N₁ scaled linearly with shear rate, whereas the steady-state shear stress did not. The average diameter of the dispersed phase decreased for all strain histories when the blend was not compatibilized. When the blend was compatibilized, the average diameter of the dispersed phase changed only during the stronger flows. Experimental data were compared with the predictions of a model formulated using ideas of Doi and Ohta (1991), Lacroix et al. (1998) and Bousmina et al. (2001). The model correctly predicted the behavior of the uncompatibilized blends for single-step shear rates but not that of the compatibilized blends, nor did it predict morphologies after shearing.     

Interparticle movement and the mechanical behavior of extruded powder aluminum at elevated temperature

This paper proposes a model and a mechanism for explaining the mechanical behavior of extruded powder aluminum at elevated temperature. This behavior is significantly different from that of ingot-cast and drawn aluminum which is subjected to the same tests. Powder aluminum exhibits a strain-softening effect which is evident in a decrease of stress with increasing strain in uniaxial test specimens when the experiment proceeds into the postyield region. Similar behavior is observed in the shear response during biaxial tension-torsion loading. For these tests, the shear stress is additionally reduced with increased axial extension. A model and mechanism are proposed, based on the relative motion of the extruded aluminum particles, to explain this effect. Equations are derived which relate the axial and shear stresses and strains. These equations are fitted to data obtained in a matrix of experiments, which include combined loadings from uniaxial tension to simple shear. Results are presented graphically and are in good agreement with the proposed models.     

A constitutive model in finite viscoelasticity

A new constitutive model is suggested for the viscoelastic behavior of rubber-like materials at finite strains. The model treats a viscoelastic medium as a system with a variable number of purely elastic links, which can arise and collapse due to micro-Brownian motion of molecules.Assuming that the processes of birth and death for elastic links are independent of stresses, we obtain operator linear constitutive equations in finite viscoelasticity. According to this model, elastic and viscous effects may be distinguished and described independently of each other by a relaxation measure and a strain energy density.The potential energy of deformations is assumed to depend on the principal invariants of the relative Finger tensor of strains. Unlike the standard approach, we do not suggest any expression for the strain energy densitya priori, but suppose that this function is presented as a sum of two functions of one variable which are found by fitting experimental data.The proposed approach allows results of several experiments (uniaxial tension, biaxial tension, and torsion) for styrene butadiene rubber and butyl rubber to be predicted correctly.     

A thermodynamic approach to the rheology of highly interactive filler-polymer mixtures. Part II. Comparison with polystyrene/nanosilica mixtures

The dynamic properties as a function of frequency and strain amplitude, steady-state viscosity as a function of shear rate, and transient shear stresses at startup and cessation of shear flow of polystyrene (PS)/fumed silica mixtures of various concentrations were investigated. An abrupt change in the viscoelastic properties was noticed at a concentration above 1% by volume. Observations by means of scanning electron microscopy (SEM) indicate the presence of a three-dimensional network through the bridging of filler particles by the adsorbed polymer. The viscoelastic behavior is simulated utilizing a theory proposed in Part I (Havet and Isayev 2001) based on a double network created by the entangled polymer matrix and the adsorbed polymer with filler concentration taken into account through the bridging density of polymer-filler interactions and a hydrodynamic reinforcement. The steps taken for determining the model parameters required to carry out the simulation are described. The major features of the rheological behavior of highly interactive polymer-filler mixtures are captured qualitatively and in some cases, quantitatively predicted.     

Damage,plasticity and failure of ceramics and cementitious composites subjected to multi-axial state of stress

Experimental data on mechanical behavior of ceramics and cementitious composites subjected to triaxial state of stress and verification of the theoretical model capable to describe deformability and fracture of brittle rock-like materials are presented in the paper. To check the validity of the theoretical model the stress–strain curves and stresses at material fracture determined experimentally for brick and mortar were compared with the theoretical predictions. The limit surface at material fracture obtained experimentally from triaxial tests was used in numerical analysis of masonry specimens subjected to compressive loading. These numerical results obtained by employing the Finite Element Method software package Mafem3D were compared with experimental data available in the literature. Fairly good agreement of numerical predictions with experimental results for masonry specimens was observed.     

An examination of dynamic fracture under biaxial-strain conditions

An experiment to investigate the influence of biaxial strain on the dynamic fracture of metals is outlined. A hollow cylindrical specimen is loaded on the inner diameter by a polyethylene-coated exploding wire which results in a circumferential spallation pattern. Prior to fracture, the spall surface undergoes biaxial deformation with a total hoop strain of the same order of magnitude as the total radial strain. This is in contrast to earlier studies in which fracture induced by stress waves was examined in experiments which are characterized by uniaxial-strain conditions. Comparing the results of the two configurations, it can be shown that the maximum principal-stress history required to cause fracture is the same in both cases, although the stresses normal to the fracture surface are quite different. High-speed photographs of the coated exploding wires and dynamic-flash X-rays of the specimens are included to demonstrate the axisymmetry of both the loading and the spall phenomenon.     

A variational approach to analyze a natural fault with hydraulic fracture based on the strain energy density criterion

A simplified analytical model of the interaction between a hydraulic fracture and an existing natural fault is developed. The mechanical activation of the natural fault as a result of contact with a pressurized fracture is described for plane strain conditions and quasi-static fracture propagation approximation. Using a variational approach, the normal and shear stresses, as well as the boundaries of the open and sliding zones along the fault, are predicted for three stages of the fracturing process (fracture approaching, coalescence, and fluid penetration). An accumulated concentration of shear stress at the tip of the fault’s sliding zone is shown to create sufficient tensile stress to initiate a new tensile crack on the opposite side of the fault, provided either the differential in situ stress is low or the friction coefficient is sufficiently large. The results of direct numerical simulation of the fracture interaction fit the model predictions made from the strain energy density fracture criterion.     

Non-local theory solution for in-plane shear of through crack

A non-local theory of elasticity is applied to obtain the plane strain stress and displacement field for a through crack under in-plane shear by using Schmidt's method. Unlike the classical elasticity solution, a lattice parameter enters into the problem that make the stresses finite at crack tip. Both the angular variations of the circumferential stress and strain energy density function are examined to associate their stationary value with locations of possible fracture initiation. The former criterion predicted a crack initiation angle of 54° from the plane of shear for the non-local solution as compared with about 75° for the classical elasticity solution. The latter criterion based on energy density yields a crack initiation angle of 80° for a Poisson's ratio of 0.28. This is much closer to the value that is predicted by the classical crack tips solution of elasticity.     

Elastic recovery occurring in step-change tests

Step-change stress and strain tests are widely used in fundamental rheological studies of viscoelastic fluids, and their results are important in relation to the potential practical applications of the materials. In this paper, we first give a general review of the experimental and theoretical development of these two tests. Attention is then confined to the creep and recovery (stress) test, which is applied to an implicit rheological fluid model in four different viscometric flows. Numerical solutions, showing the existence of a limiting recoverable strain as a function of stress, are obtained in each of these cases, namely uniaxial extension, simple shear flow, biaxial extension and planar extension. Experimental results of fluid recovery at the relevant high stress levels are not common, but the theoretical results obtained compare favourably with those that are available. Our own experimental results of simple shear flow creep and recovery tests on two polyethylene samples are also used in the comparison.     

Comparison of ductile fracture properties of aluminum castings: Sand mold vs. metal mold

This paper compares mechanical properties of two types of cast aluminum components made in sand molds and cast iron molds, respectively. For each type of the castings, a total of 12 fracture tests are performed under a wide range of stress states including 6 tensile tests on notched and unnotched round bars and 6 biaxial loading tests on butterfly specimens. Using a combined experimental–numerical approach, the plasticity and fracture properties of the components are characterized in terms of the true stress–strain curve and the ductile fracture locus. It is found that the sand-molding component is of higher yield resistance and lower ductility than the metal-molding one. Meanwhile, the fractographic study reveals that there exist two competing failure mechanisms: the internal necking of the matrix at high positive stress triaxialities and void sheeting due to shear at negative stress triaxialities. The transition of the failure modes occurs in the intermediate range. This suggests that a ductile fracture locus formulated in the space of the stress triaxiality and the effective fracture strain consist of three branches rather than a monotonic curve.     

The viscoplastic behavior of hastelloy-X single crystal

A viscoplastic constitutive model for Hastelloy-X single crystal material is developed based on crystallographic slip theory. The constitutive model was constructed for use in a viscoplastic self-consistent model for isotropic Hastelloy-X polycrystalline material, which has been described in a recent publication. It is found that, by using the slip geometry known from the metallurgical literature, the anisotropic response can be accurately predicted. The model was verified by using tension and torsion data taken at 982°C (1800°F). The constitutive model used on each slip system is a simple unified visoplastic power law model in which weak latent interaction effects are taken into account. The drag stress evolution equations for the octahedral system are written in a hardening/recovery format in which both hardening and recovery depend on separate latent interaction effects between the octahedral crystallographic slip systems. The strain rate behavior of the single crystal material is well correlated by the constitutive model in uniaxial and torsion tests, but it is necessary to include latent information effects between the octahedral slip systems in order to obtain the best possible representation of biaxial cyclic strain rate behavior. Finally, it was observed that the single crystal exhibited dynamic strain aging at 871°C (1600°F). Similar dynamic strain aging occurs at 649°C (1200°F) in the polycrystalline version of the alloy.