缺口根部和裂纹尖端残余应力的X射线法测定

X射线法用于缺口根部和裂纹尖端等徽区的残余应力测试的先决条件是解决缩小光束直径、提高衍射束的强度和准确设置试样等技术问题.在X射线衍射仪上借助于自行设计制造的限束对光装置和侧倾对中附件,成功地测定了缺口根部半径为1mm的喷丸残余应力场和板形试样压-压周期载荷下裂纹尖端的残余拉应力场.     

Residual stress analysis near a cold expanded hole in a textured alclad sheet using X-ray diffraction

In this paper we present the methods of determination and the stress obtained at the periphery of a cold expanded hole in a 2024-T3 Alclad aluminum alloy sheet. The measurements in the aluminum clad were performed by the sin²Ψ method, taking experimental precautions to deal with the texture effects. In the core aluminum a special method had to be implemented to determine the stress values in a direction not accessible to the X-ray diffraction. The strains were measured in sample orientations selected according to the texture characteristics and stress factorsF _ij were used to calculate the stress tensor. TheF _ij values were determined assuming a quasi-isotropic material behavior, after concluding that the stress results were not significantly affected by factors calculated for textured material. The residual stress profile, both in the clad and in the sheet, shows a nearly axisymmetric stress state. Compressive stresses were observed near the periphery of the hole, with values that are higher on the exit than on the entrance face. Residual stresses were also higher in the hoop direction than in the radial direction. They decreased with the radial distance to the hole and affected the previous stress state over a distance of 6 mm. The plastic deformation induced by the cold expansion is well evidenced by the FWHM values, which in the affected zone decrease with increasing distance from the hole edge.     

X-ray residual stress measurement on mechanical components with high curvature

In this paper we deal with the definition of an appropriate X-ray diffraction procedure for residual stress determination on samples with high curvature radius. We choose as the application high-strength hot worked coil springs for car suspensions (wire diameterd=12 mm). Different methods of X-ray measurement area limitation are compared, taking into account the measurement errors, for the determination of stress in one and in three directions. After the identification of the irradiated area limits for plane samples, further limits are identified due to the sample curvature (torsion bar). We describe loading devices purposely designed, constructed and calibrated. In each case, the sample is loaded so that the stress state is determined at the same time both by strain gages and by X-ray measurement.     

Simulated microstructure-sensitive extreme value probabilities for high cycle fatigue of duplex Ti-6Al-4V

A newly developed microstructure-sensitive extreme value probabilistic framework to characterize the performance/variability for damage evolution processes is exercised to compare the driving forces for fatigue crack formation (nucleation and early growth) at room temperature for four different microstructure variants of a duplex Ti-6Al-4V alloy. The aforementioned probabilistic framework links certain extreme value fatigue response parameters with microstructure attributes at fatigue critical sites through the use of marked correlation functions. By applying this framework to study the driving forces for fatigue crack formation in these microstructure variants of Ti-6Al-4V, these microstructures can be ranked in terms of relative high cycle fatigue (HCF) performance and the correlated microstructure attributes that have the most influence on the predicted fatigue response can be identified. Nonlocal fatigue indicator parameters (FIPs) based on the cyclic plastic strain averaged over domains on the length scale of the microstructure attributes (e.g., grains, phases) are used to estimate the driving force(s) for fatigue crack formation at the grain scale. By simulating multiple statistical volume elements (SVEs) using crystal plasticity constitutive relations, extreme value distributions of the predicted driving forces for fatigue crack formation are estimated using these FIPs. This strategy of using multiple SVEs contrasts with simulation based on a single representative volume element (RVE), which is often untenably large when considering extreme value responses. The simulations demonstrate that microstructures with smaller relative primary α grain sizes and lower volume fractions of the primary α grains tend to exhibit less variability and smaller magnitudes of the driving forces for fatigue crack formation. The extreme value FIPs are predicted to most likely occur at clusters of primary α grains oriented for easy basal slip. Additionally, surrounding grains/phases with soft orientation shed load to less favorably oriented primary α grains, producing extreme value FIPs.     

激光选区熔化Ti-6Al-4V合金的动态力学性能及其本构关系

为了开展激光选区熔化（SLM）增材制造钛合金的动态力学性能研究,分别采用热模拟材料试验机、分离式霍普金森压杆装置对激光选区熔化钛合金在不同温度下进行了准静态和动态压缩实验,并基于实验结果拟合Johnson-Cook本构模型,同时对钛合金在高温、高应变率下的力学行为进行了有限元模拟。结果表明,相对于铸造或锻造钛合金,激光选区熔化钛合金具有更细小、均匀的组织,使其屈服强度有明显的提升,且表现出明显的应变率强化效应和热软化效应。有限元模拟结果与实验有着较高的重合度,进一步验证了本构参数的有效性,为扩大激光选区熔化技术及其产品的应用提供了理论基础。

     

Ti-6Al-4V弹体破坏模式对冲击反应的影响研究

Ti-6Al-4V材料是武器结构轻量化时的重要替代材料,其冲击反应将可能增加战斗部毁伤威力,但目前缺乏对其冲击反应条件及反应机理的研究。本文将采用试验与理论分析方法,研究结构破坏模式对Ti-6Al-4V材料冲击反应的影响,获得其冲击反应条件及反应机理。设计并开展了钛合金弹（头部与壳体均为钛合金）与复合弹（头部碳/碳复合材料、壳体空心钛合金圆柱）正侵彻混凝土试验,撞击速度在222~1008 m/s之间。钛合金弹激发了剧烈的氧化冲击反应,但复合弹未产生冲击反应。破坏模式宏细观分析显示,钛合金弹侵彻后宏观结构基本完整,仅表面发生摩擦磨损,以细观组织剪切变形为主要失效模式,形成尺寸在微米量级至百微米量级的颗粒碎片,碎片个数可高达3×10⁶。复合弹的钛合金空心圆柱被撕裂成块,撕裂面沿剪切带方向发展,碎块尺寸在毫米或以上量级,个数至多百余个。碎片供氧和供热的效率均与碎片尺寸成反比,而特定供氧与供热条件下,碎片尺寸足够小是Ti-6Al-4V材料发生冲击反应的必要条件,这是钛合金弹发生冲击反应而钛合金空心圆柱无法激发冲击反应的本质原因。在具备冲击反应必要条件的前提下,碎片个数越多,冲击反应烈度越高。

     

高压气瓶工艺残余应力测试和分析

用X射线及磁记忆两种方法对压缩天然气的高压气瓶应力状态进行了系统分析,对一个气瓶整体制造工艺中的残余应力变化用X射线法进行了跟踪检测。考察了气瓶锻造后、淬火后及回火后外表面的残余应力状况,对相同测点进行了三次应力测试。为准确找到测点位置并寻求两种方法之间关系,在每次应力测试之前,均用金属磁记忆方法进行了先期检测。结果表明:锻造后应力水平不高,但磁记忆曲线有小幅波动,显示应力不均匀;淬火后表面具有较大压应力,最大达到0.86σS,且磁场亦有较大变化,个别点有明显应力集中;回火处理有效地消除了淬火残余应力,最大值小于0.17σS,应力均匀化,磁记忆曲线几乎无波动,效果良好。而从定量角度,残余应力和磁记忆两者之间没有明确的对应关系。对于磁记忆所显示的磁场强度变化处,用X射线法进行残余应力测试,结果并没有显示出较高的应力水平。说明两种方法不可互相替代,但以其各自的特点和优势可做互相补充。     

孔洞缺陷对3D打印Ti-6Al-4V合金疲劳试样应力分布的影响

3D打印金属技术因其个性化及可用于加工复杂零件等显著优点,在医用骨植入体领域得到了快速发展,但3D打印金属材料的孔洞缺陷所引起的应力集中现象严重降低了其疲劳强度,限制了3D打印生物金属材料的运用。本文针对3D打印Ti-6Al-4V合金超声疲劳试样,分析了Micro CT扫描试样得到的三维图像,获得了试样内孔洞缺陷的数量与体积;选择体积分数占比最大的孔洞,采用有限元方法分析了三种不同孔洞分布形式下的局部应力集中现象。研究发现,因空间位置的不同,独立的孔洞、接近自由表面的孔洞、相邻的孔洞三种不同孔洞的分布情况的应力集中系数差异显著。研究结果在一定程度上解释了目前EBM技术打印Ti-6Al-4V合金的孔洞缺陷如何对材料受力后的局部应力情况产生影响。     

Residual stress effect on fatigue striation spacing in a cold-worked rivet hole

The residual stress effect due to cold-working is studied in relation to fatigue striation spacing. Cold-working introduces a compressive stress field around the hole reducing the tendency for fatigue cracks to initiate and grow under cyclic mechanical loading. It is known that fatigue lifetime assessment requires a detailed knowledge of the residual stress profile. X-ray diffraction and 3D finite element analysis (FEA) can be used to determine the residual stress profile. Scanning electron microscopy (SEM) measurements were performed for measuring the striation spacing.     

Ti-6Al-4V钛合金表面疏水性复合膜的制备及其微摩擦磨损性能

通过自组装分子膜（SAMs）方法和有机镀膜技术在Ti-6Al-4V钛合金表面成功制备了三嗪硫醇三乙基硅烷（TES）自组装分子膜（TES-SAMs）和含氟官能团的三嗪硫醇（ATP）复合膜（TES-ATP）.采用X射线光电子能谱仪、接触角测量仪、椭圆偏振光谱仪、原子力显微镜、超景深三维显微镜和UMT-2型摩擦磨损试验机评价薄膜结构及其微摩擦学特性.研究结果表明：TES-SAMs自组装分子膜和TES-ATP复合膜的膜厚分别为3.9和22.2 nm,其对蒸馏水的接触角分别为94.5°和130.5°,呈疏水性.TES-SAMs自组装分子膜和TES-ATP复合膜均能有效降低基体的摩擦系数,TES-SAMs自组装分子膜的摩擦系数稳定在0.23,TES-ATP复合膜的摩擦系数为0.17,而空白基体的摩擦系数为0.50;同时TES-ATP复合膜还表现出良好的抗磨性能.     

网纹型表面微结构对Ti-6Al-4V水润滑摩擦学特性的影响

研究了Ti-6Al-4V合金表面网纹型微结构与Si3N4小球对摩时的水润滑摩擦学性能.利用电火花加工技术在Ti-6Al-4V合金表面加工出不同尺寸的网纹结构,运用正交试验设计方法分析了网纹宽度、深度、间宽比和网纹角度对Ti-6Al-4V合金水润滑摩擦学性能的影响.结果表明:具有合适几何参数的网纹结构能够降低摩擦副在水润滑条件下的摩擦系数和磨损量.当网纹角度在45°时,摩擦副的摩擦系数和磨损量能同时降低.网纹宽度对稳态摩擦系数的影响最大,而网纹深度和夹角对摩擦副材料的磨损影响最大.     

Ti-46Al-2Cr-2Nb和Ti6Al4V合金的干摩擦学性能对比研究

本文以商业Ti-6Al-4V合金为参照,考察了Ti-46Al-2Cr-2Nb(原子比)金属间化合物在不同载荷和速率下的干摩擦学行为,结果表明:Ti-46Al-2Cr-2Nb和Ti6Al4V合金的摩擦系数几乎相同,而Ti-46Al-2Cr-2Nb金属间化合物比Ti-6Al-4V具有更好的抗磨性;Ti-46Al-2Cr-2Nb和Ti6Al4V合金的磨损率均随载荷的增加而增加,Ti-46Al-2Cr-2Nb合金磨损率随滑动速率增加而增加,Ti-6Al-4V合金磨损率却随滑动速率增加呈下降直至稳定的趋势;Ti-46Al-2Cr-2Nb合金的磨损机制主要为疲劳磨损,Ti-6Al-4V合金的磨损机制为塑性变形,犁沟和剥落.