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作者用HYY弱碱树脂对链霉素的分离纯化进行了实验,详细地研究了树脂的吸附和脱附性能,吸附量达28万/ml树脂,脱附率达96%,获得了较满意的结果。 相似文献
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树脂吸附法处理对氨基苯酚生产废水的研究 总被引:18,自引:1,他引:18
本文选用CHA-111吸附树脂对对氨基苯酚生产过程中的含酚废水进行了处理和回收,研究了树脂种类、吸附流速和脱附剂的类型、浓度、流速、温度等对CHA-111树脂的吸附、脱附性能的影响,并回收对氨基苯酚取得了满意的效果。 相似文献
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树脂吸附法处理硝基氯苯生产废水研究 总被引:4,自引:2,他引:2
本文研究了树脂吸附法处理硝基氯苯废水的工艺条件。实验结果表明,采用H-103吸附树脂处理该生产废水,硝基氯苯的去除率和CODcr去除率达95%以上,用醇-碱混合液进行脱附,树脂脱附再生性能良好。 相似文献
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树脂吸附法处理水杨酸甲酯生产废水的研究 总被引:7,自引:0,他引:7
采用吸附树脂NDA—99处理水杨酸甲酯生产废水,结果表明该树脂时废水中的5磺基水杨酸及水杨酸均具有良好的吸附—脱附性能.废水经预处理和吸附处理后,CODCr由57000-59000mg/L降至6300mg/L左右,去除率接近89%.用IBV8%NaOH 3BVH2O作脱附剂,在温度为60℃、流量为IBV/h的条件下,脱附率接近100%,树脂可重复使用.高浓度脱附液经酸化、浓缩、冷却结晶,可回收5—磺基水杨酸,回收率为95%左右。纯度为78%。 相似文献
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吸附树脂AB—8对甜菊甙的吸附性能及在其提取纯化中的应用 总被引:4,自引:0,他引:4
考察了大孔吸附树脂AB-8对甜菊甙的吸附性能,和溶液的HP值,洗脱剂的种类及流速对树脂吸附,脱附性能的影响,结果表明,AB-8树脂对甜菊甙吸附量高,循环使用性能好且易于洗脱。 相似文献
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Separation and purification of both tea seed polysaccharide and saponin from camellia cake extract using macroporous resin 下载免费PDF全文
Pengjie Yang Mingda Zhou Chengyun Zhou Qian wang Fangfang Zhang Jian Chen 《Journal of separation science》2015,38(4):656-662
A novel method to separate and purify tea seed polysaccharide and tea seed saponin from camellia cake extract by macroporous resin was developed. Among four kinds of resins (AB‐8, NKA‐9, XDA‐6, and D4020) tested, AB‐8 macroporous resin possessed optimal separating capacity for the two substances and thus was selected for the separation, in which deionized water was used to elute tea seed polysaccharide, 0.25% NaOH solution to remove the undesired pigments, and 90% ethanol to elute tea seed saponin. Further dynamic adsorption/desorption experiments on AB‐8 resin‐based column chromatography were conducted to obtain the optimal parameters. Under optimal dynamic adsorption and desorption conditions, 18.7 and 11.8% yield of tea seed polysaccharide and tea seed saponin were obtained with purities of 89.2 and 96.0%, respectively. The developed method provides a potential approach for the large‐scale production of tea seed polysaccharide and tea seed saponin from camellia cake. 相似文献
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Min Yang Feng Zou Qingxin Shi Simin Ji Xuanyuan Wang Xingliang Xiang 《液相色谱法及相关技术杂志》2018,41(4):188-195
Kuding tea are used as a traditional tea material and widely consumed in China. Isochlorogenic acids are considered to be one of the major functional ingredients. In this study, nine types of resins including six macroporous resins and three MCI-GEL resins were investigated by adsorption and desorption tests toward the isochlorogenic acids. The HP50SS was selected as the optimal one and the effect of several factors were investigated to make optimization of the adsorption and desorption conditions for enrichment of isochlorogenic acids. As a result, 38.50?mg of refined extract including 31.70?mg total isochlorogenic acids could be separated and enriched from 500.0?mg of crude extract in which the content of total isochlorogenic acids was 8.6% and the recovery of isochlorogenic acids reached 73.4%. Meanwhile, under optimal dynamic adsorption and desorption conditions, the final contents of total isochlorogenic acids increased 9.3-fold when compared to that of crude extract in a scale-up enriched experiment. The results demonstrated that the HP50SS MCI-GEL resin was suitable for purification and enrichment of isochlorogenic acids from Kuding tea. The established protocol was high-efficiency, low-cost and environment-friendly, which could afford a potential approach for industrial applications to enrich and concentrate isochlorogenic acids from Kuding tea. 相似文献
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Adsorption resin AAS was used for the separation and purification of milupeinan (M-13)from its mother liquor. The good adsorption property of AAS adsorption resin was found formilupeinan (M-13) compared with the Diaion CHP 20p. When acetone and water (2:1 in volume)were used as desorption reagents, it was found that 3 times of bed volume of the desorption reagentswould make the AAS resin which was saturately adsorpted M-13 desorption completely.Also a macroporous anion exchange resin (Poly-4-vinylpyridine type) D-280 was used for thedecolourization from M-13 solution. Good results was given when the sr=1~2. 相似文献
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ZHANG Yifeng GUO Hong ZHANG Guangming YAN Xiuyun YIN Shougen ZHANG Zhengpu Institute of Taitai Pharmaceutical Co. Ltd Shengzhen China State Key Lab. of Functional Polymeric Materials for Adsorption Separation Institute of Polyme 《Chinese Journal of Reactive Polymers》2002,(1)
1. INTRODUCTION Fig.1 The Chemical Structure of Milupeinan As a new type of antibiotics Milupeinan, not only possesses antibacterial activities against a wide range of Gram-positive and Gram-negative bacteria, but also higgh stability under th… 相似文献
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酚醛型吸附树脂对VB_(12)的吸附性能研究 总被引:2,自引:0,他引:2
研究了酚醛型吸附树脂JDW 1、JDW 2 (自制 )和DuoliteS 76 1对VB12 的静态和动态吸附 .结果表明 ,JDW 1对VB12 的吸附量达 84mg g ,明显优于DuoliteS 76 1;吸附VB12 的初始阶段 ,即达到 4 3%~6 9%平衡吸附时 ,吸附速率数据和半经验速率方程很吻合 ;酚醛型吸附树脂等温吸附VB12 的平衡吸附数据符合Langmuir方程 ,相关系数在 0 99以上 ,因此 ,酚醛型吸附树脂吸附VB12 属单分子层吸附 ;在动态条件下 ,用含甲醇 80 %溶液以 1 1BV h来洗脱吸附VB12 的JDW 2 ,在 4 2、6 4个床体积的洗脱率分别是 92 2 0 %、95 93% ,这表明酚醛型吸附树脂具有良好的洗脱性能 ,用含甲醇为 80 %溶液作洗脱剂从JDW 2洗脱VB12 ,效果很好 相似文献
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RECOVERY OF p-AMINOPHENOL (PAP) FROM AQUEOUS SOLUTION BY HYPER-CROSS-LINKED RESIN AND ITS USE FOR WASTEWATER TREATMENT 总被引:1,自引:0,他引:1
p-Aminophenol (PAP), a typical amphoteric compound, has been widely used as raw chemical material and important interrnediate in various fields. To study on the recovery of PAP, an experimental comparison of the adsorption and desorption properties of PAP onto three types of hyper-cross-linked resins in aqueous solutions was performed. This paper focuses on the static equilibrium adsorption and desorption behaviors, the adsorption thermodynamics, the column dynamic adsorption and desorption, and other influencing factors of adsorption, such as temperature and pH values. All the isothermal data fit well to the Freundlich model. The capacity of equilibrium adsorption for PAP on NG-10 is the highest within the temperature range 288K-318K, which may greatly contribute to the advantage in specific surface area, especially the micropore area, of the adsorbent. While in the desorption experiments, NG-9 achieved relative well regeneration efficiency whether by ethanol or by 4% hydrochloric acid. Furthermore, the results of column tests and field applications were also proved that NG-9 was an effective sorbent for the reclamation PAP from wastewater. 相似文献