共查询到20条相似文献,搜索用时 31 毫秒
1.
Simple and Efficient Synthesis of 1,3-Dithioles with Pyrimidinylidene or Pyrazolylidene Substituents
Ayoob Bazgir Ali Mohammad Astaraki 《Phosphorus, sulfur, and silicon and the related elements》2013,188(9):1916-1921
Abstract 2-Pyrimidinylidene-1,3-dithioles or 2-pyrazolylidene-1,3-dithioles are prepared by a three-component condensation reaction of pyrimidine-tetraone or 1H-pyrazole-4,5-dione, carbon disulfide, and dialkyl acetylendicarboxylates in the presence of tributylphosphine. GRAPHICAL ABSTRACT 相似文献
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Edward E. Nifantyev Elena N. Rasadkina Pavel V. Slitikov 《Phosphorus, sulfur, and silicon and the related elements》2013,188(9):1981-1987
Abstract The phosphorylation of acylated trihydroxybenzene derivatives by amides of phosphorous acid was considered. The possibility of selective phosphorylation of triacetoxy phloroglucin was shown. GRAPHICAL ABSTRACT 相似文献
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Jelem Restrepo José Salazar Simón E. López 《Phosphorus, sulfur, and silicon and the related elements》2013,188(12):2311-2320
Abstract We describe a rapid and convenient methodology for the preparation of diverse 3-aryl and 3-trifluoromethyl 4H-1,2,4-benzothiadiazine-1,1-dioxides in a one-pot microwave-promoted reaction between 2-aminobenzenesulfonamides and benzaldehydes, trifluoroacetic acid or benzoic acids. GRAPHICAL ABSTRACT 相似文献
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Mohammad Bakherad Ali Keivanloo Zahra Kalantar Vahid Keley 《Phosphorus, sulfur, and silicon and the related elements》2013,188(3):464-470
Abstract Reaction of 2-mercaptopropargylquinazoline-4-one with various aryliodides catalyzed by Pd–Cu leads to the regioselective formation of 1-arylsubstituted-5H-[1,3]thiazolo-[3,2-a]quinazoline-5-ones. GRAPHICAL ABSTRACT 相似文献
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Faramarz Rostami Charati Zinatossadat Hossaini Mohammad R. Hosseini-Tabatabaei 《Phosphorus, sulfur, and silicon and the related elements》2013,188(7):1443-1448
Abstract Stable derivatives of oxaphospholes were obtained from the reaction between electron-deficient acetylenic compounds and phenacyl bromide or its derivatives in the presence of triphenylphosphine in acetonitrile as the solvent in excellent yields. GRAPHICAL ABSTRACT 相似文献
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Nicolas Rabasso Antoine Fadel 《Phosphorus, sulfur, and silicon and the related elements》2013,188(8):1811-1819
Abstract Synthesis of a phosphonopentapeptide enkephalin analogue was achieved from heterocyclic aminophosphonates via the coupling of Boc-Tyr-Gly-Gly-OH with phosphonodipeptide. The latter was formed by coupling Boc-Phe-OH with N-terminal α,α-disubstituted heterocyclic α-aminophosphonates. GRAPHICAL ABSTRACT 相似文献
7.
Liqiang Wu Pengli Sun Fulin Yan 《Phosphorus, sulfur, and silicon and the related elements》2013,188(10):2055-2060
Abstract A highly convenient method for the trimethylsilylation of alcohols and phenols via treatment by hexamethyldisilazane in the presence of melamine trisulfonic acid as a catalyst has been developed. A wide variety of hydroxyl groups were selectively protected under solvent-free conditions. GRAPHICAL ABSTRACT 相似文献
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Nihal Onul Wafaa M. Dib Brimo Cemil Ibis 《Phosphorus, sulfur, and silicon and the related elements》2013,188(11):2180-2188
Abstract Substituted perchlorobutadienes were synthesized from the reactions of hexachloro-1,3-butadiene with some thiols in ethanol in the presence of sodium hydroxide. The oxidation products were obtained from the reactions of thioethers with m-chloroperbenzoic acid. The structures of the new compounds were characterized by microanalysis and spectroscopic data. GRAPHICAL ABSTRACT 相似文献
11.
Liqiang Wu Shujun Chao Xiao Wang Fulin Yan 《Phosphorus, sulfur, and silicon and the related elements》2013,188(2):304-310
Abstract Thiocyanation of aromatic ethers, anilines, and indoles have been achieved using ammonium thiocyanate in the presence of poly[4-diacetoxyiodo] styrene (PDAIS) in CH3CN at room temperature. GRAPHICAL ABSTRACT 相似文献
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Maasoumeh Jafarpour Abdolreza Rezaeifard Mahdieh Heidari 《Phosphorus, sulfur, and silicon and the related elements》2013,188(7):1470-1482
Abstract Operationally simple and environmentally benign methods for some organic transformations comprising reductive coupling of sulfonyl chlorides, chemoselective deoxygenation of sulfoxides, and halogenation of alcohols mediated by ZrOCl2·8H2O/MX in water have been developed. GRAPHICAL ABSTRACT 相似文献
14.
S. Ebrahimi A. Mobinikhaldei H. Eibagi 《Phosphorus, sulfur, and silicon and the related elements》2013,188(12):2279-2285
Abstract Without a catalyst and under solvent-free conditions, 2,3-disubstituted-1,3-thiazolidin-4-one 5a–j derivatives were synthesized efficiently via the three-component reaction of aryl hydrazide, aromatic aldehyde, and mercaptoacetic acid. All the newly synthesized compounds were confirmed by IR, 1H NMR, and 13C NMR spectroscopy and elemental analysis. GRAPHICAL ABSTRACT 相似文献
15.
F. Shirini N. Ghaffari Khaligh 《Phosphorus, sulfur, and silicon and the related elements》2013,188(11):2156-2165
Abstract Succinimide-N-sulfonic acid (SuSA) is easily prepared by the reaction of succinimide with chlorosulfonic acid. This reagent is able to efficiently catalyze the chemoselective trimethylsilylation of alcohols and phenols with hexamethyldisilazane (HMDS). All reactions were performed under mild reaction conditions, giving excellent yields. GRAPHICAL ABSTRACT 相似文献
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Issa Yavari Maryam Ghazvini Ashraf S. Shahvelayati Mohammad M. Ghanbari 《Phosphorus, sulfur, and silicon and the related elements》2013,188(1):134-139
Abstract A simple, one-pot synthesis of N-(4-aryl-3-alkylthiazol-2(3H)-ylidene)anilines and N-(4-aryl-3-alkylthiazol-2(3H)-ylidene)benzamides via the reaction of primary alkylamines, α-bromoketones, and phenylisothiocyanate or benzoylisothiocyanate is described. GRAPHICAL ABSTRACT 相似文献
18.
Junyan Jiang Wencun Wang Xiaoxia Wang Xiangming Zhu Zhifang Li 《Phosphorus, sulfur, and silicon and the related elements》2013,188(10):2047-2054
Abstract The acylation of Se-nucleophiles with N-acylbenzotriazoles was investigated. Samarium phenylselenolate and benzylselenolate (RSeSmI2) reacted with N-aroyl and N-alkanoylbenzotriazoles smoothly and afforded the corresponding selenol esters in good yields. Treatment of the RSeSmI2 with α,β-unsaturated N-acylbenzotriazoles afforded the anticipated α,β-unsaturated selenol esters in moderate yields, due mainly to the side reaction of conjugate addition. GRAPHICAL ABSTRACT 相似文献
19.
Il’yas S. Nizamov Ilnar D. Nizamov Farid D. Yambushev Olga V. Bolshakova Gulnur G. Sergeenko Vladimir F. Mironov 《Phosphorus, sulfur, and silicon and the related elements》2013,188(7):1436-1442
Abstract The reactions of geraniol, nerol, and linalool with N,N-diethylamido O,O-propylenephosphite and diethyl chlorophosphite were studied. On the basis of these studies, new dienyl diprenoid phosphite esters were obtained. GRAPHICAL ABSTRACT 相似文献
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Abdolhamid Bamoniri Arash Ghorbani-Choghamarani Bi Bi Fatemeh Mirjalili 《Phosphorus, sulfur, and silicon and the related elements》2013,188(2):381-388
Abstract A wide range of aromatic aldehydes has been selectively converted to 1,1-diacetates using silica chromate (SiO2?O?CrO2?O?SiO2) under solvent-free conditions at room temperature in moderate to good yields. This protocol is mild and efficient compared to other reported methods. GRAPHICAL ABSTRACT 相似文献