Laser carbonitriding of alumina surface

Laser carbonitriding of alumina surfaces is examined. Temperature and stress fields developed during the laser heating of the substrate surface are predicted using the finite element method in line with the experimental conditions. The formation of Al(C, N) and AlN compounds in the surface region of irradiated workpiece is examined using X-ray Photoelectron Spectroscopy (XPS) and X-ray Diffraction (XRD). The microstructural and morphological changes in the laser irradiated region are examined using Scanning Electron Microscope (SEM). The microhardness of the resulting surface is measured and compared with the base material hardness. It is found that high temperature gradient is developed in the irradiated region, which in turn, results in high residual stress levels in this region. XPS and XRD data reveal the presence of Al (C, N) and AlN compounds in the surface region. The microhardness in the surface region of the laser treated workpiece increases significantly.     

Laser surface treatment of Inconel 718 alloy: Thermal stress analysis

Laser heating of Inconel 718 alloy is considered and the resulting temperature and stress fields are predicted using the finite element method (FEM). An experiment is carried out to treat the alloy surface by a laser beam at high pressure nitrogen environment. The metallurgical and morphological changes in the irradiated region are examined using the Scanning Electron Microscope (SEM), optical microscope, and X-ray Diffraction (XRD). It is found that the surface hardness of the alloy improves after the laser heating process, which is due to the microstructural changes and γ-phase nitride formation in the surface region. The maximum value of the residual stress predicted in the irradiated region is close to the yielding limit of the alloy.     

Laser bending of AISI 304 steel sheets: Thermal stress analysis

Laser induced bending of steel sheet is carried out and thermal stress developed in the heated region is examined. Temperature and stress fields are predicted using the finite element model. The microstructural changes in the melted region are investigated through scanning electron microscope, energy dispersive spectroscopy and X-ray diffraction. The residual stress developed at the surface vicinity of the laser treated region is measured using the X-ray diffraction technique, which is then compared with its counterpart predicted from the simulations. It is found that the residual stress at the surface vicinity is compressive and the prediction of the residual stress agrees well with that obtained from the X-ray diffraction technique. In addition, surface temperature predictions are in good agreement with the thermocouple data. The laser treated region is free from major cracks and large cavities.     

Laser gas-assisted processing of carbon coated and TiC embedded Ti-6Al-4V alloy surface

Laser gas-assisted treatment of Ti-6Al-4V alloy surface is carried out. The alloy surface is initially coated by a carbon layer, in which the TiC particles are embedded prior to laser processing of the surface. The carbon coating with the presence of TiC particles on the workpiece surface is expected to result in carbonitride compound in the surface vicinity after the laser treatment process. Optical and scanning electron microscopes are used to examine the morphological and the metallurgical changes in the laser treated layer. The residual stress formed in the surface region after the laser treatment process is critical for the practical applications of the resulting surface. Therefore, the residual stress formed in the laser treated region is predicted from the analytically equation. The X-ray diffraction technique is incorporated to obtain the residual stress formed in the surface region. It is found that the residual stress predicted agrees with the X-ray diffraction data. The dense structures consisting of TiC_xN_1−x, TiN_x, Ti₂N, and TiC compounds are formed in the surface region of the treated layer. This, in turn, significantly increases the microhardness at the surface.     

Laser welding of low carbon steel and thermal stress analysis

Laser welding of mild steel sheets is carried out under nitrogen assisting gas ambient. Temperature and stress fields are computed in the welding region through the finite element method. The residual stress developed in the welding region is measured using the XRD technique and the results are compared with the predictions. Optical microscopy and the SEM are used for the metallurgical examination of the welding sites. It is found that von Mises stress attains high values in the cooling cycle after the solidification of the molten regions. The residual stress predicted agreed well with the XRD results.     

Analytical investigation into laser pulse heating and thermal stresses

Laser pulse heating of metallic surfaces results in rapid rise of temperature in the region irradiated by the laser beam. This in turn results in high temperature gradient in this region. The irradiated substrate material expands as a response to the temperature gradient. Consequently, high thermal stress levels are developed in the region of the high temperature gradient. In the present study, closed form solutions for temperature and stress fields due to a laser pulse decaying exponentially in time are presented. A Laplace transformation method is employed in the analysis. The resulting equations are non-dimensionalized with the appropriate parameters. It is found that temperature rises rapidly during the early heating period in the surface region. In this case, internal energy gain dominates the conduction losses from the surface vicinity. The thermal stress levels attain high values in the surface region. The stress wave developed is compressive and it propagates with a wave speed c₁ inside the substrate.     

Laser hole cutting into bronze: Thermal stress analysis

Laser hole cutting in bronze is carried out and the thermal stress formed in the cutting section is examined using a finite element code. The cut geometry and microstructural changes in the cutting section are examined using optical microscope, scanning electron microscope (SEM), and energy dispersive spectroscopy (EDS). It is found that the high conductivity of bronze increases the cooling rates within the cutting section, which influences the thermal stress field in the cutting region. The residual stress predicted is in the order of 200 MPa within the vicinity of the hole circumference. The striation pattern at the kerf surface changes towards the hole exit, which is associated with the drag forces developed in this region.     

High temperature thermal behaviour modeling of large-scale fused silica optics for laser facility

High temperature annealing is often used for the stress control of optical materials.However,weight and viscosity at high temperature may destroy the surface morphology,especially for the large-scale,thin and heavy optics used for large laser facilities.It is necessary to understand the thermal behaviour and design proper support systems for large-scale optics at high temperature.In this work,three support systems for fused silica optics are designed and simulated with the finite element method.After the analysis of the thermal behaviours of different support systems,some advantages and disadvantages can be revealed.The results show that the support with the optical surface vertical is optimal because both pollution and deformation of optics could be well controlled during annealing at high temperature.Annealing process of the optics irradiated by CO2 laser is also simulated.It can be concluded that high temperature annealing can effectively reduce the residual stress.However,the effects of annealing on surface morphology of the optics are complex.Annealing creep is closely related to the residual stress and strain distribution.In the region with large residual stress,the creep is too large and probably increases the deformation gradient which may affect the laser beam propagation.     

Improved formulation of electron kinetic theory approach for laser shortpulse heating: Thermal stress consideration

Nonequilibrium energy transport between excited electrons and lattice site is re-formulated after considering the ballistic contribution of the electron energy to the energy transport process. The improved formulation of the electron kinetic theory predictions are compared with the previously obtained electron kinetic and two-equation models. Thermal stress developed in the region irradiated by a laser beam is formulated during the heating pulse. Copper with variable properties is used in the simulations. It is found that improved electron kinetic theory model predicts less temperature rise than that corresponding to previously formulated electron kinetic theory and two equation models in the surface region; in this case, electron temperature attains high values. Thermal stress developed is compressive and attains the maximum at some depth below the surface. The thermal stress level is well below the yielding limit of the substrate material.     

Laser cutting of holes in thick sheet metals: Development of stress field

Laser cutting of hole in a mild steel thick sheet metal is investigated. Temperature and stress fields developed around the cutting section are simulated using the finite element method. An experimental is carried out accommodating the simulation parameters. The residual stress developed in the cutting section is measured using the XRD technique and findings are compared with the predictions. Optical microscopy and SEM are carried out to examine the morphological changes in the cutting sections. It is found that temperature decays sharply in the region of the laser heat source, which results in high temperature gradient in this region. This causes the development of high stress levels around the cut edges. The residual stresses predicted are in agreement with the measured results.     

Laser cutting of sharp edge: Thermal stress analysis

Laser cutting of sharp edge and thermal stress development in the cutting section is examined. The finite element method is used to predict temperature and stress fields while the X-ray diffraction (XRD) technique is used to measure the residual stress around the cut edges. A mild steel sheet with 5 mm thickness is used in the simulations and the experiment. The morphological and metallurgical changes around the edges are examined using the optical microscopy and scanning electron microscopy (SEM). It is found that temperature remains high at the sharp edge when the laser beam is located in this region. This, in turn, lowers the cooling rate and reduces von Mises stress in this region. The magnitude of the residual stress is about 90 MPa at the sharp corner while the maximum von Mises stress is in the order of 280 MPa, which occurs away from sharp corner. In addition, the residual stress predicted agrees with the experimental data.     

激光钝化对熔石英修复后损伤性能影响的实验研究

采用10.6 μupm 的 CO₂激光, 对单次激光脉冲辐照修复熔石英存在的烧蚀采用大光斑钝化去除. 经过辐照修复的区域置于前表面测试初始损伤阈值, 结果表明调制造成的损伤得到了一定程度的抑制; 辐照区域置于后表面修复后 熔石英的初始损伤阈值超过了基底的初始损伤阈值. 实验观察到了应力分布外扩, 同时明显减弱. 对损伤增长的测试说明, 经过激光熔融辐照后的损伤点, 当应力释放以后, 损伤扩展初期表现出指数增长趋势, 后期随着辐照次数的增加, 损伤增长不再明显, 并且趋于恒定值.     

An application of Raman spectroscopy on the measurement of residual stress in porous silicon

The porous silicon film, at micron level, and the bulk silicon substrate is a basic structure in MEMS components. The residual stress, due to the lattice mismatch between the film and the substrate, exists on the interface and may cause cracking and damaging on the component. Micro-Raman spectroscopy is an optical measurement method that was rapidly applied into the fields of chemistry, physics, material science and mechanics. In this paper, the method is introduced and applied to the study of the stress problems in porous silicon as follows. (1) In the electrochemical etching technique for porous silicon preparation, the distribution of the tensile residual stress along the transitional region between etched and un-etched area is experimentally studied and the result reveals the stress is continuous across the region. In the etched region it reaches GPa level, and in the transition region the gradient of the stress is high. (2) In chemical etching preparation of porous silicon, the residual stress rises up seriously in the cracked area, up to 0.92 GPa. With the porosity increasing, the tensile stress on the porous silicon film increases accordingly. The appearance of the porous silicon film surface is also given by metalloscope and atomic force microscope. The structure of the micro-pores is expected to have a close relation with the distribution of the residual stress.     

强流脉冲电子束辐照诱发纯钼表面的损伤效应及结构缺陷

利用强流脉冲电子束（HCPEB）装置对纯钼表面进行辐照处理,并利用X射线衍射仪,扫描电子显微镜（SEM）、透射电子显微镜（TEM）详细分析了辐照表面的微观结构和损伤效应. 1次HCPEB辐照后,纯钼表层积聚了极大的残余应力,多次辐照后表面未融化区域出现大量绝热剪切带,且局部区域发生开裂. 微观结构分析显示,辐照后材料表面形成发散状的位错组态和大量空位簇缺陷;绝热剪切带内部是尺寸为1 μm 左右等轴状的再结晶晶粒. 剪切带造成的材料表面局部软化以及间隙原子偏聚于晶界是材料发生开裂的主要原因. 另外,表面熔化区域可形成尺寸为20 nm左右的纳米晶. 关键词： 强流脉冲电子束 纯钼 绝热剪切带 空位簇缺陷     

实验物理与工业控制系统平台在HL-2A主机测控系统中的应用

描述了利用实验物理与工业控制系统(EPICS)平台对HL-2A主机运行参数进行的集中测控系统开发。系统采用s7nodave设备驱动模块,实现了SoftIOC与各PLC的通讯,将各子系统的PLC集成到了EPICS控制系统中。通过对关系型数据库和应用层软件CSS中数据归档及报警等组件的扩展与配置,实现OPI层与各个子系统的实时通信。测控系统成功地将HL-2A主机参数集中在EPICS平台下运行,为下一代装置的主机集中测控系统设计打下了基础。     

强流脉冲电子束辐照诱发金属纯镍中的空位簇缺陷

利用强流脉冲电子束(high-current pulsed electron beam,HCPEB)技术对多晶纯Ni进行了辐照处理,采用透射电子显微镜详细分析了辐照诱发的缺陷结构.HCPEB辐照后,纯镍表层积聚了幅值极大的残余应力,沿{111}晶面形成了稠密的位错墙及孪晶结构,另外还形成了大量的包括位错圈、堆垛层错四面体(SFT)及孔洞在内的空位簇缺陷.SFT缺陷的数量远高于其他空位簇缺陷,其周围区域位错密度很低.孔洞缺陷主要出现在SFT密集区域.HCPEB瞬间的加热和冷却诱发的幅值极大的应力和极高的应变 关键词： 强流脉冲电子束 多晶纯Ni 空位簇缺陷 堆垛层错四面体     

基于神经网络的选区激光熔化残余应力预测

当前对选区激光熔化产生的残余应力预测方法主要为数值模拟,但由于设备、环境、粉末等因素差异性较大,且具有较大不确定性,很难建立符合实际情况的数值模拟模型。利用神经网络在预测多变量、复杂线性信息处理方面能力强的特点,建立适用于预测316L不锈钢粉末选区激光熔化残余应力的模型。使用选区激光熔化技术打印相当数量的不同工艺参数的试样,采用超声波检测其内部残余应力作为神经网络的训练样本,并使用这些样本对神经网络模型进行训练,获得具有预测功能的神经网络,将验证样本的工艺参数输入神经网络,计算出预测的残余应力值,与实际检测值进行对比。实验结果表明,预测值与实际测量值偏差较小,验证了所提方法的有效性。采用神经网络预测残余应力的方法,可以快速确定不同选区激光熔化工艺参数对应的残余应力,避免设置残余应力较高的工艺参数,有效缩短制备高质量工件试样的周期,降低成本。     

Laser cutting of rectangular geometry into alumina tiles

Laser cutting of rectangular geometry into the 5 mm thick alumina tiles is carried out. Temperature and stress fields, which are developed during the cutting process, are simulated in line with the experimental conditions. The morphological changes in the cutting sections are examined using optical and electron scanning microscopes, energy dispersive spectroscopy, and X-ray diffraction technique. The predictions of surface temperature and the residual stress are validated through the experimental data. It is found that von Mises stress attains high values in the region of the mid-thickness of the workpiece. The laser cut sections are free from major cracks and large scale sideways burning. The predictions of surface temperature and residual stress agree well with their counterparts obtained from the experiment.     

HL-2A等离子体边缘极向剩余胁强的研究

首次报导了托卡马克等离子体边缘与湍流相关的极向剩余胁强剖面的测量结果。采用外中平面往复式静电探针阵列对HL-2A托卡马克边缘的极向湍流动量输运进行研究。在没有外部动量注入的欧姆放电下,剩余胁强为有限值、且其空间剖面在等离子体边缘具有明显的径向梯度,表明托卡马克等离子体边缘存在极向动量源。由动量源产生的动量主要以扩散形式向与剩余胁强相反的方向传播,最终的结果是等离子体边缘存在有限的雷诺胁强。在最后闭合磁面以内0.5~2cm区域,剩余胁强的梯度提供自发旋转的力矩,由该力矩引起的动量产生与由速度梯度引起的动量扩散共同导致了雷诺胁强出现负梯度,造成动量沉积,从而驱动极向平衡流。     

双离子束溅射中红外SiO2薄膜热稳定性研究

通过双离子束溅射方法在蓝宝石、硅衬底上制备了单层SiO2薄膜,分析了SiO2薄膜残余应力、表面形貌、微观结构以及光学性能(可见-近红外0.4~1.2 μm和中红外3~5 μm波段)在400 ℃~1 000 ℃温度范围内的演化规律.研究结果表明:在400 ℃附近,SiO2薄膜残余应力存在局部极小值;SiO2薄膜光学性能的演化与膜层表面质量、内部残余应力及微观结构变化密切相关;经1 000 ℃高温处理后,蓝宝石窗口表面SiO2薄膜红外透射性能仍能保持很好的稳定性,且膜层表面没有出现显著的气泡、开裂等损伤形貌.该研究结果可为恶劣环境下光学窗口头罩表面薄膜系统的设计提供指导.