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| 桃金娘烯醇氧化异构化生成紫苏醛 | |
| 引用本文： | 聂丽娟,张玉华,段巨龙,李响敏,秦中.桃金娘烯醇氧化异构化生成紫苏醛[J].南昌大学学报(理科版),2004,28(2):161-162,166. |
| 作者姓名： | 聂丽娟 张玉华 段巨龙 李响敏 秦中 |
| 作者单位： | 1. 南昌大学,中德联合研究院,南昌,330047 2. 江西省医药学校,南昌,330001 3. 江西教育学院,南昌,330029 |
| 摘 要： | 桃金娘烯醇在催化剂的作用下，氧化异构化生成紫苏醛。在此反应中。筛选了较为理想的催化剂-合金铜锌催化剂；考察了温度、真空度、进料速度、氧气量等对反应的影响；探讨了几种产品纯化的方法。反应产率达48％。实验表明此合成工艺简单，易于工业化生产。 |
| 关 键 词： | 桃金娘烯醇 紫苏醛 氧化 异构化 |
| 文章编号： | 1006-0464(2004)02-0161-02 |
SYNTHESIS OF PERILLALDEHYDE BY OXIDATION AND ISOMERIZATION OF MYRTENOL |
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| NIE Li-juan,ZHANG Yu-hua,DUAN Ju-long,LI Xiang-min,QIN Zhong.SYNTHESIS OF PERILLALDEHYDE BY OXIDATION AND ISOMERIZATION OF MYRTENOL[J].Journal of Nanchang University(Natural Science),2004,28(2):161-162,166. | |
| Authors: | NIE Li-juan ZHANG Yu-hua DUAN Ju-long LI Xiang-min QIN Zhong |
| Institution: | NIE Li-juan~1,ZHANG Yu-hua~2,DUAN Ju-long~3,LI Xiang-min~1,QIN Zhong~1 |
| Abstract: | Perillaldehyde is synthesized by oxidation and isomerization of myrtenol on the catalytic action; Better catalyst is selected; Effect of temperature, vacuum, feed speed and quantity of oxygen on the reaction are investigated; Purifying method of product is probed; Yield>48%; Experiment proved this synthesis process is simple and easy to industrialization. |
| Keywords: | myrtenol perillaldehyde oxidition isomerization |
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