| N,N′-联苄基-2-苯基四氢咪唑的合成 |
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| 引用本文： | 董怀民,余勃,姜伟,肖志斌,陆豫.N,N′-联苄基-2-苯基四氢咪唑的合成[J].南昌大学学报(理科版),2009,33(6). |
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| 作者姓名： | 董怀民 余勃 姜伟 肖志斌 陆豫 |
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| 作者单位： | 1. 南昌大学化学系,江西,南昌,330031;南昌大学中德联合研究院,江西,南昌,330047
2. 南昌大学中德联合研究院,江西,南昌,330047 |
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| 摘 要： | 以苯甲醛和乙二胺为原料,经缩合、催化加氢两步法合成标题产物,产物通过质谱、红外光谱、核磁共振氢谱及元素分析,对其结构进行确证.与传统的方法相比产率有所提高,而且反应条件温和,缩短了时间,简化了操作步骤.
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| 关 键 词： | Schiff碱 四氢咪唑 缩合反应 合成 |
Synthesis of N,N'-Dibenzyl-2-phenyl-tetrahydroimidazole |
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| Dong Huai-min,YU Bo,JIANG Wei,XIAO Zhi-bin,Lu Yu.Synthesis of N,N'-Dibenzyl-2-phenyl-tetrahydroimidazole[J].Journal of Nanchang University(Natural Science),2009,33(6). |
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| Authors: | Dong Huai-min YU Bo JIANG Wei XIAO Zhi-bin Lu Yu |
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| Abstract: | Ethylenediamine was reacted with benzaldehyde to prepare diSchiff bases,then the diSchiff bases and benzaldehyde were hydrogenated to get product by Pd/C catalyst.The structures of these product was verified by MS,IR,1H NMR spectrometry and elemental analysis.Compared with traditional methods,the yield was increased,the reaction condition was mild,the reaction time was shortened and the preparation process was simpler and convenient. |
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| Keywords: | schiff base tetrahydroimidazole condensation synthesis |
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