Synthesis of 1,3- and 1,4-bis-methoxy- and ethoxy-4-(m-carborane-C-methanoyloxy)phenylmethylene- and phenylmethyl]phenylenediamines |
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| Authors: | E A Dikusar V I Potkin N G Kozlov A P Kadutskii A P Yuvchenko M P Bey A V Shchurivskaya |
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| Institution: | (1) Institute of Physical Organic Chemistry, Belarus National Academy of Sciences, ul. Surganova 13, Minsk, 220072, Belarus;(2) Institute of Chemistry of New Materials, Belarus National Academy of Sciences, Minsk, Belarus;(3) Aleksandrov Republican Scientific and Practical Center of Oncology and Medical Radiology, Minsk district, Lesnoe 2, Belarus |
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| Abstract: | 1,3- and 1,4-bis3-methoxy and ethoxy-4-(m-carborane-C-methanoyloxy)phenylmethylene]phenylenediamines were synthesized from the vanillin and vanillal m-carborane-C-carboxylates by the reaction with 1,3- and 1,4-phenylenediamines in anhydrous methanol. Reduction of the title compounds with NaBH(OAc)3] in benzene yielded 1,3- and 1,4-bis3-methoxy- and ethoxy-4-(m-carborane-C-methanoyloxy)phenylmethyl] phenylenediamines. |
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