New human hair certified reference material for methylmercury and trace elements |
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Authors: | Jun Yoshinaga Masatoshi Morita and Kensaku Okamoto |
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Institution: | (1) National Institute for Environmental Studies, 16-2 Onogawa, Tsukuba, 305 Ibaraki, Japan;(2) Faculty of Pharmaceutical Sciences, University of Tokushima, 1-78 Shomachi, 770 Tokushima, Japan |
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Abstract: | A new human hair certified reference material (NIES CRM No. 13) for mercury speciation and trace element analysis was prepared
at the National Institute for Environmental Studies (NIES), Environmental Agency of Japan. Scalp hair from Japanese males,
which is identical with the original material for the previous human hair CRM (NIES CRM No. 5), was used. Special attention
was paid to reduce contamination from a grinding vessel during the preparation procedure. A newly-prepared ceramic/Teflon
disc mill was used for cryogenic grinding of the hair. 1, 000 bottles (3 g each) were produced after sieving and blending
of the hair powder. Certified values for total mercury and methylmercury, as well as other trace elements of toxicological
and nutritional significance (antimony, cadmium, copper, lead, selenium, and zinc), were determined based on analyses from
extensive collaborations. Reference values for 12 elements (aluminium, arsenic, barium, calcium, cobalt, iron, magnesium,
manganese, silver, sodium, sulfur and vanadium) were also given. |
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