| 基于深孔改进电极发射光谱法同时测定地球化学样品中微量银、锡、硼 |
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| 引用本文： | 彭君.基于深孔改进电极发射光谱法同时测定地球化学样品中微量银、锡、硼[J].中国无机分析化学,2018,8(2):22-24. |
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| 作者姓名： | 彭君 |
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| 作者单位： | 国土资源部长沙矿产资源监督检测中心;楚雄师范学院; |
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| 摘 要： | 采用深孔改进电极,一米平面光栅交流电弧摄谱法同时测定地球化学样品中微量银、锡、硼的含量。以三氧化二铝、硫酸钾、氟化钠和碳粉作缓冲剂,锗作内标。方法检出限为:银0.015μg/g、锡0.32μg/g、硼1.0μg/g,相对标准偏差(RSD)为5.8%~7.5%。实验用国家一级标准物质进行验证,方法的测定值与标准值相符。
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| 关 键 词： | 喷溅 熔球 深孔电极 钻孔 发射光谱 |
| 收稿时间： | 2017/7/25 0:00:00 |
| 修稿时间： | 2018/2/28 0:00:00 |
Simultaneous Determination of Trace Silver, Tin and Boron Based on Deep Hole Electrode in Geochemical Samples by Emission Spectrometry |
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| Peng Jun.Simultaneous Determination of Trace Silver, Tin and Boron Based on Deep Hole Electrode in Geochemical Samples by Emission Spectrometry[J].Chinese Journal of Inorganic Analytical Chemistry,2018,8(2):22-24. |
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| Authors: | Peng Jun |
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| Institution: | The ministry of land and resources of changsha mineral resources supervision and inspection center,Changsha,Hunan |
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| Abstract: | In this work, the effect of the molten splash ball was solved via the deep electrodes, drilling, and overlapping spectra of the emission spectrum when the spectrum of the sample taken from the molten splash ball, to test the quality of the impact brought by two-electrode spectrographic ensure the qualification of the samples tested at 95% the above. This way can improve the test sample pass rate, and low detection limit, high sensitivity, good accuracy, high accuracy and other technical indicators. |
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| Keywords: | Spatter molten globule deep-hole electrode perforate emission spectrometry |
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