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热重分析法测定矿产品中的吸附水及烧失减量
引用本文:管 嵩,丁仕兵,刘冲伟,冯丽丽.热重分析法测定矿产品中的吸附水及烧失减量[J].中国无机分析化学,2013,3(4):20-23.
作者姓名:管 嵩  丁仕兵  刘冲伟  冯丽丽
作者单位:山东出入境检验检疫局 化工矿产品检测中心 山东 青岛;黄岛出入境检验检疫局 山东 青岛,山东出入境检验检疫局 化工矿产品检测中心 山东 青岛,黄岛出入境检验检疫局 山东 青岛,山东出入境检验检疫局 化工矿产品检测中心 山东 青岛
基金项目:直属局非标方法研究项目(SFB/T 0151)资助
摘    要:采用热重分析法(TGA)测量矿产品中的吸附水及烧失减量,验证了方法的准确性及精密度。对多种矿产品样品采用TGA法和常规马弗炉加热法进行测量,对比结果表明,这两种方法没有显著性差异。TGA法具有方便快捷、准确可靠等优点,是矿产品吸附水及烧失减量检验的首选。

关 键 词:矿产品  吸附水  烧失减量  马弗炉
收稿时间:6/7/2013 12:00:00 AM
修稿时间:7/2/2013 12:00:00 AM

Determination of Absorbed Water and Loss on Ignition in Mineral Products by Thermogravimetric Method
GUAN Song,DING Shibing,LIU Chongwei and FENG Lili.Determination of Absorbed Water and Loss on Ignition in Mineral Products by Thermogravimetric Method[J].Chinese Journal of Inorganic Analytical Chemistry,2013,3(4):20-23.
Authors:GUAN Song  DING Shibing  LIU Chongwei and FENG Lili
Institution:Chemical Mineral Inspection Center of Shandong Entry-exit Inspection and Quarantine Bureau Shandong Qingdao Huangdao Entry-exit Inspection and Quarantine Bureau Shandong Qingdao,Chemical Mineral Inspection Center of Shandong Entry-exit Inspection and Quarantine Bureau Shandong Qingdao Huangdao Entry-exit Inspection and Quarantine Bureau Shandong Qingdao,Huangdao Entry-exit Inspection and Quarantine Bureau Shandong Qingdao,Chemical Mineral Inspection Center of Shandong Entry-exit Inspection and Quarantine Bureau Shandong Qingdao Huangdao Entry-exit Inspection and Quarantine Bureau Shandong Qingdao
Abstract:The absorbed water and loss on ignition in mineral products were studied by thermogravimetric analysis(TGA)method.The accuracy and precision of the method were validated.Several mineral products were tested by TGA and common muffle furnace burning method.By comparison,it concluded that there was no significant difference in the analysis results between the two methods.But the TGA method has some advantages such as convenience,higher accuracy and reliability,thus it is the preferred method that should be used for the determination of absorbed water and loss on ignition in mineral products.
Keywords:Thermogravimetric Method  Mineral Products  Higroscopic Moisture  Loss on Ignition  Muffle Furnace
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