| Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono（6A-N- 1-（2-hydroxyl）- phenylethylimino-6A-deoxy）-β-cyclodextrin and covalently bonded silica gel |
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| 作者姓名： | Xiao Ping Chen Zhi Ming Zhou Hao Yuan Zi Hui Meng |
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| 作者单位： | School of Chemical Engineering and the Environment, Beijing Institute of Technology, Beijing[4_TD$DIF] 100081, China |
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| 基金项目： | Financial support from the National Natural Science Foundation of China （No. 20572009） is gratefully acknowledged. |
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| 摘 要： | A novel chiral stationary phase （CSP） was prepared by immobilizing mono（6A-N-1-（2-hydroxyl）-phenylethylimino-6A- deoxy）-β-cyclodextrin onto the surface of silica gel via a longer spacer. This chiral stationary phase exhibited good enantioselectivity for a variety of chiral compounds under reversed-phase conditions.
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| 关 键 词： | 环式糊精 手性固定相 二茂铁 合成 |
Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono（6A-N- 1-（2-hydroxyl）- phenylethylimino-6A-deoxy）-β-cyclodextrin and covalently bonded silica gel |
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| Xiao Ping Chen Zhi Ming Zhou Hao Yuan Zi Hui Meng.Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono（6A-N- 1-（2-hydroxyl）- phenylethylimino-6A-deoxy）-β-cyclodextrin and covalently bonded silica gel[J].Chinese Chemical Letters,2008,19(7):797-800. |
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| Authors: | Xiao Ping Chen Zhi Ming Zhou Hao Yuan Zi Hui Meng |
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| Institution: | School of Chemical Engineering and the Environment, Beijing Institute of Technology, Beijing[4_TD$DIF] 100081, China |
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| Abstract: | A novel chiral stationary phase (CSP) was prepared by immobilizing mono(6A-N-1-(2-hydroxyl)-phenylethylimino-6A-deoxy)-β-cyclodextrin onto the surface of silica gel via a longer spacer.This chiral stationary phase exhibited good enantios electivity for a variety of chiral compounds under reversed-phase conditions. |
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| Keywords: | Cyclodextrin Enandoseparation Chiral stationary phase Ferrocene derivatives |
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