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煤沥青水浆的制备及影响规律的研究
引用本文:李兴,王灿,常宏宏,魏文珑,王志忠.煤沥青水浆的制备及影响规律的研究[J].燃料化学学报,2011,39(7):501-506.
作者姓名:李兴  王灿  常宏宏  魏文珑  王志忠
作者单位:College of Chemistry and Chemical Engineering, Taiyuan University of Technology, Taiyuan 030024, China
基金项目:国家自然科学基金,山西省高校科学研究开发项目,煤转化国家重点实验室开放基金
摘    要:以中温煤沥青为原料,经冷冻粉碎后制得具有一定粒径级配的煤沥青粉,加入适量分散剂和水在高速搅拌下制备煤沥青水浆.结果表明,JL-C01中裂乳化剂是制备煤沥青水浆的优良分散剂,在此基础上进一步考察了分散剂用量及浆体浓度对煤沥青成浆性、煤沥青水浆流变性及稳定性的影响.结果表明,最大成浆浓度为70%;在分散剂用量相同的条件下,...

关 键 词:煤沥青  煤沥青水浆  成浆性  流变性  稳定性
收稿时间:2010-09-03

Preparation and influence factors of coal pitch water slurry
LI Xing,WANG Can,CHANG Hong-hong,WEI Wen-long,WANG Zhi-zhong.Preparation and influence factors of coal pitch water slurry[J].Journal of Fuel Chemistry and Technology,2011,39(7):501-506.
Authors:LI Xing  WANG Can  CHANG Hong-hong  WEI Wen-long  WANG Zhi-zhong
Abstract:The medium temperature coal tar pitch was used as the raw material to prepare coal tar pitch powder with certain particle size distribution by freezing and then pulverizing. By adding proper amount of dispersant and water, the coal tar pitch powder was made into the coal pitch water slurry (CPWS) at high agitating speed. The screening experiments show that the JL-C01 emulsifier has the best dispersion effect. The effect of the dispersant dosage and slurry concentration on the slurry-ability, rheological behavior and static stability of CPWS were investigated. The maximum slurry-ability concentration is 70%. The apparent viscosity of CPWS firstly decreases and then increases with increasing shearing rate when the dispersant dosage is same. For different slurry concentrations, the apparent viscosity of CPWS presents a decreasing tendency with increasing shearing rate. Under the same shearing rate, the apparent viscosity goes up as the slurry concentration increases. The CPWS is a pseudo-plastic fluid. The best rheological behavior is obtained when the slurry concentration is 69%. When the slurry concentration is 70%, the slurry maintains stable for 21d. Referring to coal water slurry criterion GB/T18856-2002, the combustion analysis of CPWS was made. The low heat value, ash, and the volatile matter all meet the first grade standard for coal water slurry. In addition, the sulfur content achieves the second grade standard.
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